The crystal structure described by DyC5H9(NO4)2 crystallizes in the monoclinic C2 space group. Dy(1) is bonded in a 8-coordinate geometry to two equivalent O(1), two equivalent O(2), two equivalent O(3), and two equivalent O(4) atoms. There are three inequivalent C sites. In the first C site, C(1) is bonded in a trigonal planar geometry to one H(3), one O(1), and one O(2) atom. In the second C site, C(2) is bonded in a trigonal planar geometry to one H(4) and two equivalent O(3) atoms. In the third C site, C(3) is bonded in a trigonal planar geometry to one N(1), one H(5), and one O(4) atom. N(1) is bonded in a trigonal planar geometry to one C(3), one H(1), and one H(2) atom. There are five inequivalent H sites. In the first H site, H(1) is bonded in a single-bond geometry to one N(1) atom. In the second H site, H(2) is bonded in a single-bond geometry to one N(1) atom. In the third H site, H(3) is bonded in a single-bond geometry to one C(1) atom. In the fourth H site, H(4) is bonded in a single-bond geometry to one C(2) atom. In the fifth H site, H(5) is bonded in a single-bond geometry to one C(3) atom. There are four inequivalent O sites. In the first O site, O(1) is bonded in a distorted single-bond geometry to one Dy(1) and one C(1) atom. In the second O site, O(2) is bonded in a distorted bent 150 degrees geometry to one Dy(1) and one C(1) atom. In the third O site, O(3) is bonded in a distorted single-bond geometry to one Dy(1) and one C(2) atom. In the fourth O site, O(4) is bonded in a distorted single-bond geometry to one Dy(1) and one C(3) atom. is represented by the Crystallographic Information File (CIF) [CIF]
data_DyH9C5(NO4)2
_symmetry_space_group_name_H-M   'P 1'
_cell_length_a   6.705
_cell_length_b   6.705
_cell_length_c   6.654
_cell_angle_alpha   73.935
_cell_angle_beta   73.935
_cell_angle_gamma   65.012
_symmetry_Int_Tables_number   1
_cell_volume   256.086
_cell_formula_units_Z   1
loop_
 _symmetry_equiv_pos_site_id
 _symmetry_equiv_pos_as_xyz
  1  'x, y, z'
loop_
 _atom_site_type_symbol
 _atom_site_label
 _atom_site_symmetry_multiplicity
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_occupancy
  Dy  Dy0  1  0.002  0.998  0.000  1.0
  H  H1  1  0.816  0.654  0.417  1.0
  H  H2  1  0.346  0.184  0.583  1.0
  H  H3  1  0.524  0.740  0.523  1.0
  H  H4  1  0.260  0.476  0.477  1.0
  H  H5  1  0.164  0.462  0.874  1.0
  H  H6  1  0.538  0.836  0.126  1.0
  H  H7  1  0.916  0.084  0.500  1.0
  H  H8  1  0.554  0.465  0.803  1.0
  H  H9  1  0.535  0.446  0.197  1.0
  C  C10  1  0.060  0.467  0.036  1.0
  C  C11  1  0.533  0.940  0.964  1.0
  C  C12  1  0.069  0.931  0.500  1.0
  C  C13  1  0.713  0.470  0.700  1.0
  C  C14  1  0.530  0.287  0.300  1.0
  N  N15  1  0.685  0.636  0.536  1.0
  N  N16  1  0.364  0.315  0.464  1.0
  O  O17  1  0.990  0.311  0.126  1.0
  O  O18  1  0.689  0.010  0.874  1.0
  O  O19  1  0.019  0.635  0.117  1.0
  O  O20  1  0.365  0.981  0.883  1.0
  O  O21  1  0.158  0.854  0.666  1.0
  O  O22  1  0.146  0.842  0.334  1.0
  O  O23  1  0.899  0.328  0.742  1.0
  O  O24  1  0.672  0.101  0.258  1.0
[/CIF]
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The crystal structure described by DyC5H9(NO4)2 crystallizes in the monoclinic C2 space group. Dy(1) is bonded in a 8-coordinate geometry to two equivalent O(1), two equivalent O(2), two equivalent O(3), and two equivalent O(4) atoms. There are three inequivalent C sites. In the first C site, C(1) is bonded in a trigonal planar geometry to one H(3), one O(1), and one O(2) atom. In the second C site, C(2) is bonded in a trigonal planar geometry to one H(4) and two equivalent O(3) atoms. In the third C site, C(3) is bonded in a trigonal planar geometry to one N(1), one H(5), and one O(4) atom. N(1) is bonded in a trigonal planar geometry to one C(3), one H(1), and one H(2) atom. There are five inequivalent H sites. In the first H site, H(1) is bonded in a single-bond geometry to one N(1) atom. In the second H site, H(2) is bonded in a single-bond geometry to one N(1) atom. In the third H site, H(3) is bonded in a single-bond geometry to one C(1) atom. In the fourth H site, H(4) is bonded in a single-bond geometry to one C(2) atom. In the fifth H site, H(5) is bonded in a single-bond geometry to one C(3) atom. There are four inequivalent O sites. In the first O site, O(1) is bonded in a distorted single-bond geometry to one Dy(1) and one C(1) atom. In the second O site, O(2) is bonded in a distorted bent 150 degrees geometry to one Dy(1) and one C(1) atom. In the third O site, O(3) is bonded in a distorted single-bond geometry to one Dy(1) and one C(2) atom. In the fourth O site, O(4) is bonded in a distorted single-bond geometry to one Dy(1) and one C(3) atom. is represented by the Crystallographic Information File (CIF) [CIF]
data_DyH9C5(NO4)2
_symmetry_space_group_name_H-M   'P 1'
_cell_length_a   6.705
_cell_length_b   6.705
_cell_length_c   6.654
_cell_angle_alpha   73.935
_cell_angle_beta   73.935
_cell_angle_gamma   65.012
_symmetry_Int_Tables_number   1
_cell_volume   256.086
_cell_formula_units_Z   1
loop_
 _symmetry_equiv_pos_site_id
 _symmetry_equiv_pos_as_xyz
  1  'x, y, z'
loop_
 _atom_site_type_symbol
 _atom_site_label
 _atom_site_symmetry_multiplicity
 _atom_site_fract_x
 _atom_site_fract_y
 _atom_site_fract_z
 _atom_site_occupancy
  Dy  Dy0  1  0.002  0.998  0.000  1.0
  H  H1  1  0.816  0.654  0.417  1.0
  H  H2  1  0.346  0.184  0.583  1.0
  H  H3  1  0.524  0.740  0.523  1.0
  H  H4  1  0.260  0.476  0.477  1.0
  H  H5  1  0.164  0.462  0.874  1.0
  H  H6  1  0.538  0.836  0.126  1.0
  H  H7  1  0.916  0.084  0.500  1.0
  H  H8  1  0.554  0.465  0.803  1.0
  H  H9  1  0.535  0.446  0.197  1.0
  C  C10  1  0.060  0.467  0.036  1.0
  C  C11  1  0.533  0.940  0.964  1.0
  C  C12  1  0.069  0.931  0.500  1.0
  C  C13  1  0.713  0.470  0.700  1.0
  C  C14  1  0.530  0.287  0.300  1.0
  N  N15  1  0.685  0.636  0.536  1.0
  N  N16  1  0.364  0.315  0.464  1.0
  O  O17  1  0.990  0.311  0.126  1.0
  O  O18  1  0.689  0.010  0.874  1.0
  O  O19  1  0.019  0.635  0.117  1.0
  O  O20  1  0.365  0.981  0.883  1.0
  O  O21  1  0.158  0.854  0.666  1.0
  O  O22  1  0.146  0.842  0.334  1.0
  O  O23  1  0.899  0.328  0.742  1.0
  O  O24  1  0.672  0.101  0.258  1.0
[/CIF]
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