extractions and
                expelled seeds,
                with not more
                than 10 percent
                of oil and when
                the amount of
                moisture is
                higher than 11
                percent, with not
                more than 20
                percent of oil
                and moisture
                combined.
I............  Seed cake with             4.2  UN1386             III............  None...........  B136, IB8, IP3,     None...........  213............  241...........  Forbidden.....  Forbidden.....  E.............  13, 25
                more than 1.5                                                                        IP7, N7.
                percent oil and
                not more than 11
                percent moisture.
I............  Seed cake with not         4.2  UN2217             III............  None...........  B136, IB8, IP3,     None...........  213............  241...........  Forbidden.....  Forbidden.....  A.............  13, 25, 120
                more than 1.5                                                                        IP7, N7.
                percent oil and
                not more than 11
                percent moisture.

                                                                                * * * * * * *
               Selenic acid......           8  UN1905             I..............  8..............  IB7, IP1, N34, T6,  None...........  211............  242...........  Forbidden.....  25 kg.........  A.............  53, 58
                                                                                TP33.

                                                                                * * * * * * *
               Selenium                     8  UN2879             I..............  8, 6.1.........  A7, N34, T10, TP2,  None...........  201............  243...........  0.5 L.........  2.5 L.........  E.............  40, 53, 58
                oxychloride.                                                                         TP13.

                                                                                * * * * * * *
               Silicon                      8  UN1818             II.............  8..............  A3, B2, B6, T10,    None...........  202............  242...........  Forbidden.....  30 L..........  C.............  40, 53, 58
                tetrachloride.                                                                       TP2, TP7, TP13.

                                                                                * * * * * * *
               Sludge, acid......           8  UN1906             II.............  8..............  A3, A7, B2, IB2,    None...........  202............  242...........  Forbidden.....  30 L..........  C.............  14, 53, 58
                                                                                N34, T8, TP2,
                                                                                TP28.

                                                                                * * * * * * *
               Sodium............         4.3  UN1428             I..............  4.3............  A7, A8, A19, A20,   151............  211............  244...........  Forbidden.....  15 kg.........  D.............  13, 52, 148
                                                                                B9, B48, B68,
                                                                                IB4, IP1, N34,
                                                                                T9, TP7, TP33,
                                                                                TP46, W31.

                                                                                * * * * * * *
               Sodium borohydride         4.3  UN1426             I..............  4.3............  N40, W31..........  None...........  211............  242...........  Forbidden.....  15 kg.........  E.............  13, 52, 148

                                                                                * * * * * * *
               Sodium hydride....         4.3  UN1427             I..............  4.3............  A19, N40, W31.....  None...........  211............  242...........  Forbidden.....  15 kg.........  E.............  13, 52, 148
               Sodium                       8  UN2439             II.............  8..............  IB8, IP2, IP4, N3,  154............  212............  240...........  15 kg.........  50 kg.........  A.............  12, 25, 40,
                hydrogendifluorid                                                                    N34, T3, TP33.                                                                                52, 53, 58
                e.

                                                                                * * * * * * *
               Sodium phosphide..         4.3  UN1432             I..............  4.3, 6.1.......  A19, N40, W31.....  None...........  211............  None..........  Forbidden.....  15 kg.........  E.............  13, 40, 52,
                                                                                85, 148

                                                                                * * * * * * *
               Sounding devices,         1.2F  UN0204             ...............  1.2F...........  ..................  None...........  62.............  62............  Forbidden.....  Forbidden.....  03............  25
                explosive.
               Sounding devices,         1.1F  UN0296             ...............  1.1F...........  ..................  None...........  62.............  62............  Forbidden.....  Forbidden.....  03............  25
                explosive.
               Sounding devices,         1.1D  UN0374             ...............  1.1D...........  ..................  None...........  62.............  62............  Forbidden.....  Forbidden.....  03............  25
                explosive.
               Sounding devices,         1.2D  UN0375             ...............  1.2D...........  ..................  None...........  62.............  62............  Forbidden.....  Forbidden.....  03............  25
                explosive.

                                                                                * * * * * * *
               Stannic chloride,            8  UN1827             II.............  8..............  B2, IB2, T7, TP2..  154............  202............  242...........  1 L...........  30 L..........  C.............  53, 58
                anhydrous.
               Stannic chloride             8  UN2440             III............  8..............  IB8, IP3, T1, TP33  154............  213............  240...........  25 kg.........  100 kg........  A.............  53, 58
                pentahydrate.
               Stannic phosphide.         4.3  UN1433             I..............  4.3, 6.1.......  A19, N40, W31.....  None...........  211............  242...........  Forbidden.....  15 kg.........  E.............  13, 40, 52,
                                                                                85, 148

                                                                                * * * * * * *
               Strontium                  4.3  UN2013             I..............  4.3, 6.1.......  A19, N40, W31.....  None...........  211............  None..........  Forbidden.....  15 kg.........  E.............  13, 40, 52,
                phosphide.                                                                                85, 148

                                                                                * * * * * * *
G............  Substances,               1.4S  UN0481             ...............  1.4S...........  101, 347..........  None...........  62.............  None..........  25 kg.........  75 kg.........  01............  25
                explosive, n.o.s.

                                                                                * * * * * * *
               Sulfamic acid.....           8  UN2967             III............  8..............  IB8, IP3, T1, TP33  154............  213............  240...........  25 kg.........  100 kg........  A.............  53, 58

                                                                                * * * * * * *
               Sulfur chlorides..           8  UN1828             I..............  8..............  5, A7, A10, B10,    None...........  201............  243...........  Forbidden.....  2.5 L.........  C.............  40, 53, 58
                                                                                B77, N34, T20,
                                                                                TP2.

                                                                                * * * * * * *
+............  Sulfur trioxide,             8  UN1829             I..............  8, 6.1.........  2, 387, B9, B14,    None...........  227............  244...........  Forbidden.....  Forbidden.....  A.............  25, 40, 53, 58
                stabilized.                                                                          B32, B49, B77,
                                                                                N34, T20, TP4,
                                                                                TP13, TP25, TP26,
                                                                                TP38, TP45.

                                                                                * * * * * * *
               Sulfuric acid,               8  UN1831             I..............  8..............  A7, N34, T20,       None...........  201............  243...........  Forbidden.....  2.5 L.........  C.............  14, 40, 53, 58
                fuming with less                                                                     TP2,TP13.
                than 30 percent
                free sulfur
                trioxide.
               Sulfuric acid,               8  UN1831             I..............  8, 6.1.........  2, B9, B14, B32,    None...........  227............  244...........  Forbidden.....  Forbidden.....  C.............  53, 58
                fuming with 30                                                                       B77, B84, N34,
                percent or more                                                                      T20, TP2, TP12,
                free sulfur                                                                          TP13.
                trioxide.
               Sulfuric acid,               8  UN1832             II.............  8..............  A3, A7, B2, B83,    None...........  202............  242...........  Forbidden.....  30 L..........  C.............  14, 53, 58
                spent.                                                                               B84, IB2, N34,
                                                                                T8, TP2.
               Sulfuric acid with           8  UN1830             II.............  8..............  A3, A7, B3, B83,    154............  202............  242...........  1 L...........  30 L..........  C.............  14, 53, 58
                more than 51                                                                         B84, IB2, N34,
                percent acid.                                                                        T8, TP2.
               Sulfuric acid with           8  UN2796             II.............  8..............  386, A3, A7, B2,    154............  202............  242...........  1 L...........  30 L..........  B.............  53, 58
                not more than 51%                                                                    B15, IB2, N6,
                acid.                                                                                N34, T8, TP2.

                                                                                * * * * * * *
               Sulfurous acid....           8  UN1833             II.............  8..............  B3, IB2, T7, TP2..  154............  202............  242...........  1 L...........  30 L..........  B.............  40, 53, 58
+............  Sulfuryl chloride.         6.1  UN1834             I..............  6.1, 8.........  1, B6, B9, B10,     None...........  226............  244...........  Forbidden.....  Forbidden.....  D.............  40, 53, 58
                                                                                B14, B30, B77,
                                                                                N34, T22, TP2,
                                                                                TP13, TP38, TP44.

                                                                                * * * * * * *
               Tetrahydrophthalic           8  UN2698             III............  8..............  IB8, IP3, T1, TP33  154............  213............  240...........  25 kg.........  100 kg........  A.............  53, 58
                anhydrides with
                more than 0.05
                percent of maleic
                anhydride.

                                                                                * * * * * * *
               Thioglycolic acid.           8  UN1940             II.............  8..............  A7, B2, IB2, N34,   154............  202............  242...........  1 L...........  30 L..........  A.............  53, 58
                                                                                T7, TP2.

                                                                                * * * * * * *
               Thionyl chloride..           8  UN1836             I..............  8..............  B6, B10, N34, T10,  None...........  201............  243...........  Forbidden.....  Forbidden.....  C.............  40, 53, 58
                                                                                TP2, TP13.

                                                                                * * * * * * *
               Thiophosphoryl               8  UN1837             II.............  8..............  A3, A7, B2, B8,     None...........  202............  242...........  Forbidden.....  30 L..........  C.............  40, 53, 58
                chloride.                                                                            B25, IB2, N34,
                                                                                T7, TP2.

                                                                                * * * * * * *
+............  Titanium                   6.1  UN1838             I..............  6.1, 8.........  2, B7, B9, B14,     None...........  227............  244...........  Forbidden.....  Forbidden.....  D.............  40, 53, 58
                tetrachloride.                                                                       B32, B77, T20,
                                                                                TP2, TP13, TP38,
                                                                                TP45.
               Titanium                     8  UN2869             II.............  8..............  A7, IB8, IP2, IP4,  154............  212............  240...........  15 kg.........  50 kg.........  A.............  40, 53, 58
                trichloride                                                                          N34, T3, TP33.
                mixtures.
                                                                  III............  8..............  A7, IB8, IP3, N34,  154............  213............  240...........  25 kg.........  100 kg........  A.............  40, 53, 58
                                                                                T1, TP33.

                                                                                * * * * * * *
               Torpedoes with            1.1E  UN0329             ...............  1.1E...........  ..................  ...............  62.............  62............  Forbidden.....  Forbidden.....  03............  25
                bursting charge.
               Torpedoes with            1.1F  UN0330             ...............  1.1F...........  ..................  ...............  62.............  None..........  Forbidden.....  Forbidden.....  03............  25
                bursting charge.
               Torpedoes with            1.1D  UN0451             ...............  1.1D...........  ..................  ...............  62.............  62............  Forbidden.....  Forbidden.....  03............  25
                bursting charge.

                                                                                * * * * * * *
               Triallylamine.....           3  UN2610             III............  3, 8...........  B1, IB3, T4, TP1..  None...........  203............  242...........  5 L...........  60 L..........  A.............  40, 52

                                                                                * * * * * * *
               Trichloroacetic              8  UN1839             II.............  8..............  A7, IB8, IP2, IP4,  154............  212............  240...........  15 kg.........  50 kg.........  A.............  53, 58
                acid.                                                                                N34, T3, TP33.
               Trichloroacetic              8  UN2564             II.............  8..............  A3, A7, B2, IB2,    154............  202............  242...........  1 L...........  30 L..........  B.............  53, 58
                acid, solution.                                                                      N34, T7, TP2.
               ..................  ..........  .................  III............  8..............  A3, A7, IB3, N34,   154............  203............  241...........  5 L...........  60 L..........  B.............  8, 53, 58
                                                                                T4, TP1.
+............  Trichloroacetyl              8  UN2442             II.............  8, 6.1.........  2, B9, B14, B32,    None...........  227............  244...........  Forbidden.....  Forbidden.....  D.............  40, 53, 58
                chloride.                                                                            N34, T20, TP2,
                                                                                TP38, TP45.

                                                                                * * * * * * *
               Trichlorosilane...         4.3  UN1295             I..............  4.3, 3, 8......  N34, T14, TP2,      None...........  201............  244...........  Forbidden.....  Forbidden.....  D.............  21, 40, 49,
                                                                                TP7, TP13, W31.                                                                                53, 58, 100

                                                                                * * * * * * *
               Trifluoroacetic              8  UN2699             I..............  8..............  A7, B4, N3, N34,    None...........  201............  243...........  0.5 L.........  2.5 L.........  B.............  12, 25, 40,
                acid.                                                                                N36, T10, TP2.                                                                                53, 58

                                                                                * * * * * * *
               Trimethylacetyl            6.1  UN2438             I..............  6.1, 8, 3......  2, B3, B9, B14,     None...........  227............  244...........  Forbidden.....  Forbidden.....  D.............  21, 25, 40,
                chloride.                                                                            B32, N34, T20,                                                                                53, 58, 100
                                                                                TP2, TP13, TP38,
                                                                                TP45.
               Trimethylamine,            2.1  UN1083             ...............  2.1............  N87, T50..........  306............  304............  314, 315......  Forbidden.....  150 kg........  B.............  40, 52
                anhydrous.
               Trimethylamine,              3  UN1297             I..............  3, 8...........  T11, TP1..........  None...........  201............  243...........  0.5 L.........  2.5 L.........  D.............  40, 52, 135
                aqueous solutions
                with not more
                than 50 percent
                trimethylamine by
                mass.
                                                                  II.............  3, 8...........  B1, IB2, T7, TP1..  150............  202............  243...........  1 L...........  5 L...........  B.............  40, 41, 52
                                                                  III............  3, 8...........  B1, IB3, T7, TP1..  150............  203............  242...........  5 L...........  60 L..........  A.............  40, 41, 52

                                                                                * * * * * * *
               Trimethylchlorosil           3  UN1298             II.............  3, 8...........  A3, A7, B77, N34,   None...........  206............  243...........  Forbidden.....  5 L...........  E.............  40, 53, 58
                ane.                                                                                T10, TP2, TP7,
                                                                                TP13.
               Trimethylcyclohexy           8  UN2326             III............  8..............  IB3, T4, TP1......  154............  203............  241...........  5 L...........  60 L..........  A.............  52
                lamine.

                                                                                * * * * * * *
               Trimethylhexamethy           8  UN2327             III............  8..............  IB3, T4, TP1......  154............  203............  241...........  5 L...........  60 L..........  A.............  52
                lenediamines.

                                                                                * * * * * * *
               Tripropylamine....           3  UN2260             III............  3, 8...........  B1, IB3, T4, TP1..  150............  203............  242...........  5 L...........  60 L..........  A.............  40, 52

                                                                                * * * * * * *
               Uranium                    6.1  UN3507             I..............  6.1, 7, 8......  369...............  420............  None...........  None..........  Less than .1    Less than .1    A.............  132, 152
                hexafluoride,                                                                                kg.             kg.
                radioactive
                material,
                excepted package,
                less than 0.1 kg
                per package, non-
                fissile or
                fissile-excepted.

                                                                                * * * * * * *
               Valeryl chloride..           8  UN2502             II.............  8, 3...........  A3, A7, B2, IB2,    154............  202............  243...........  1 L...........  30 L..........  C.............  40, 53, 58
                                                                                N34, T7, TP2.

                                                                                * * * * * * *
               Vanadium                     8  UN2443             II.............  8..............  A3, A7, B2, B16,    154............  202............  242...........  Forbidden.....  30 L..........  C.............  40, 53, 58
                oxytrichloride.                                                                      IB2, N34, T7, TP2.

                                                                                * * * * * * *
               Vanadium                     8  UN2444             I..............  8..............  A7, B4, N34, T10,   None...........  201............  243...........  Forbidden.....  2.5 L.........  C.............  40, 53, 58
                tetrachloride.                                                                       TP2.
               Vanadium                     8  UN2475             III............  8..............  IB8, IP3, T1, TP33  154............  213............  240...........  25 kg.........  100 kg........  A.............  40, 53, 58
                trichloride.

                                                                                * * * * * * *
               Vinyltrichlorosila           3  UN1305             II.............  3, 8...........  A3, A7, B6, N34,    None...........  206............  243...........  Forbidden.....  5 L...........  B.............  40, 53, 58
                ne.                                                                                T10, TP2, TP7,
                                                                                TP13.

                                                                                * * * * * * *
               Warheads, rocket          1.4F  UN0371             ...............  1.4F...........  ..................  None...........  62.............  None..........  Forbidden.....  Forbidden.....  03............  25
                with burster or
                expelling charge.
               Warheads, rocket          1.1D  UN0286             ...............  1.1D...........  ..................  None...........  62.............  62............  Forbidden.....  Forbidden.....  03............  25
                with bursting
                charge.
               Warheads, rocket          1.2D  UN0287             ...............  1.2D...........  ..................  None...........  62.............  62............  Forbidden.....  Forbidden.....  03............  25
                with bursting
                charge.
               Warheads, rocket          1.1F  UN0369             ...............  1.1F...........  ..................  None...........  62.............  None..........  Forbidden.....  Forbidden.....  03............  25
                with bursting
                charge.
               Warheads, torpedo         1.1D  UN0221             ...............  1.1D...........  ..................  None...........  62.............  62............  Forbidden.....  Forbidden.....  03............  25
                with bursting
                charge.

                                                                                * * * * * * *
G............  Water-reactive             4.3  UN2813             I..............  4.3............  IB4, N40, T9, TP7,  None...........  211............  242...........  Forbidden.....  15 kg.........  E.............  13, 40, 148
                solid, n.o.s.                                                                        TP33, W31.
                                                                  II.............  4.3............  B132, IB7, IP2,     151............  212............  242...........  15 kg.........  50 kg.........  E.............  13, 40, 148
                                                                                IP21, T3, TP33,
                                                                                W31, W40.
                                                                  III............  4.3............  B132, IB8, IP21,    151............  213............  241...........  25 kg.........  100 kg........  E.............  13, 40, 148
                                                                                T1, TP33, W31.

                                                                                * * * * * * *
               Zinc ashes........         4.3  UN1435             III............  4.3............  A1, A19, B136,      151............  213............  241...........  25 kg.........  100 kg........  A.............  13, 148
                                                                                IB8, IP4, T1,
                                                                                TP33, W100.

                                                                                * * * * * * *
               Zinc chloride,               8  UN2331             III............  8..............  IB8, IP3, T1, TP33  None...........  213............  240...........  25 kg.........  100 kg........  A.............  53, 58
                anhydrous.
               Zinc chloride,               8  UN1840             III............  8..............  IB3, T4, TP2......  154............  203............  241...........  5 L...........  60 L..........  A.............  53, 58
                solution.

                                                                                * * * * * * *
               Zinc phosphide....         4.3  UN1714             I..............  4.3, 6.1.......  A19, N40, W31.....  None...........  211............  None..........  Forbidden.....  15 kg.........  E.............  13, 40, 52,
                                                                                85, 148

                                                                                * * * * * * *
               Zirconium                    8  UN2503             III............  8..............  IB8, IP3, T1, TP33  154............  213............  240...........  25 kg.........  100 kg........  A.............  53, 58
                tetrachloride.
----------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------------

* * * * *

Appendix B to Sec.  172.101--List of Marine Pollutants

* * * * *

                        List of Marine Pollutants
------------------------------------------------------------------------
           S. M. P. (1)                     Marine pollutant (2)
------------------------------------------------------------------------

                                * * * * *
                                    Dodecene (except 1-dodecene).

                                * * * * *
------------------------------------------------------------------------

* * * * *

0
7. In Sec.  172.102:
0
a. In paragraph (c)(1):
0
i. Special provisions 132, 150, 238, the first sentence of special
provision 369, and special provision 387 are revised;
0
ii. Special provisions 325, 388, 389, and 391 are added; and
0
iii. Special provisions 421 and 422 are revised;
0
b. In paragraph (c)(2), special provisions A56 and A105 are revised;
0
c. In paragraph (c)(3), special provision B136 is added;
0
d. In paragraph (c)(8)(ii), special provision TP10 is revised; and
0
e. In paragraph (c)(9), special provision W32 is removed.
    The additions and revisions read as follows:

Sec.  172.102  Special Provisions.

* * * * *
    (c) * * *
    (1) * * *
    132 This description may only be used for ammonium nitrate-based
compound fertilizers. They must be classified in accordance with the
procedure as set out in the Manual of Tests and Criteria, part III,
section 39 (IBR, see Sec.  171.7 of this subchapter). Fertilizers
meeting the criteria for this identification number are only subject to
the requirements of this subchapter when offered for transportation and
transported by air or vessel.
* * * * *
    150 This description may only be used for ammonium nitrate-based
fertilizers. They must be classified in accordance with the procedure
as set out in the Manual of Tests and Criteria, part III, section 39
(IBR, see Sec.  171.7 of this subchapter).
* * * * *
    238 Neutron radiation detectors: Neutron radiation detectors
containing non-pressurized boron trifluoride gas in excess of 1 gram
(0.035 ounces) and radiation detection systems containing such neutron
radiation detectors as components may be transported by highway, rail,
vessel, or cargo aircraft in accordance with the following:
    a. Each radiation detector must meet the following conditions:
    (1) The pressure in each neutron radiation detector must not exceed
105 kPa absolute at 20 [deg]C (68 [deg]F);
    (2) The amount of gas must not exceed 13 grams (0.45 ounces) per
detector; and
    (3) Each neutron radiation detector must be of welded metal
construction with brazed metal to ceramic feed through assemblies.
These detectors must have a minimum burst pressure of 1800 kPa as
demonstrated by design type qualification testing; and
    (4) Each detector must be tested to a 1 x 10-10 cm\3\/s
leaktightness standard before filling.
    b. Radiation detectors transported as individual components must be
transported as follows:
    (1) They must be packed in a sealed intermediate plastic liner with
sufficient absorbent or adsorbent material to absorb or adsorb the
entire gas contents.
    (2) They must be packed in strong outer packagings and the
completed package must be capable of withstanding a 1.8 meter (5.9
feet) drop without leakage of gas contents from detectors.
    (3) The total amount of gas from all detectors per outer packaging
must not exceed 52 grams (1.83 ounces).
    c. Completed neutron radiation detection systems containing
detectors meeting the conditions of paragraph a of this special
provision must be transported as follows:
    (1) The detectors must be contained in a strong sealed outer
casing;
    (2) The casing must contain include sufficient absorbent or
adsorbent material to absorb or adsorb the entire gas contents;
    (3) The completed system must be packed in strong outer packagings
capable of withstanding a 1.8 meter (5.9 feet) drop test without
leakage unless a system's outer casing affords equivalent protection.
    d. Except for transportation by aircraft, neutron radiation
detectors and radiation detection systems containing such detectors
transported in accordance with paragraph a of this special provision
are not subject to the labeling and placarding requirements of part 172
of this subchapter.
    e. When transported by highway, rail, vessel, or as cargo on an
aircraft, neutron radiation detectors containing not more than 1 gram
of boron trifluoride, including those with solder glass joints are not
subject to any other requirements of this subchapter provided they meet
the requirements in paragraph a of this special provision and are
packed in accordance with paragraph b of this special provision.
Radiation detection systems containing such detectors are not subject
to any other requirements of this subchapter provided they are packed
in accordance with paragraph c of this special provision.
* * * * *
    325 In the case of non-fissile or fissile-excepted uranium
hexafluoride, the material must be classified under UN 2978.
* * * * *
    369 In accordance with Sec.  173.2a of this subchapter, this
radioactive material in an excepted package possessing toxic and
corrosive properties is classified in Division 6.1 with radioactivity
and corrosive subsidiary risks. * * *
* * * * *
    387 When materials are stabilized by temperature control, the
provisions of Sec.  173.21(f) of this subchapter apply. When chemical
stabilization is employed, the person offering the material for
transport shall ensure that the level of stabilization is sufficient to
prevent the material as packaged from dangerous polymerization at 50
[deg]C (122 [deg]F). If chemical stabilization becomes ineffective at
lower temperatures within the anticipated duration of transport,
temperature control is required and is forbidden by aircraft. In making
this determination factors to be taken into consideration include, but
are not limited to, the capacity and geometry of the packaging and the
effect of any insulation present, the temperature of the material when
offered for transport, the duration of the journey, and the ambient
temperature conditions typically encountered in the journey
(considering also the season of year), the effectiveness and other
properties of the stabilizer employed, applicable operational controls
imposed by regulation (e.g., requirements to protect from sources of
heat, including other cargo carried at a temperature above ambient) and
any other relevant factors. The provisions of this special provision
will be effective until January 2, 2023, unless we terminate them
earlier or extend them beyond that date by notice of a final rule in
the Federal Register.
    388 a. Lithium batteries containing both primary lithium metal
cells and rechargeable lithium ion cells that are not designed to be
externally charged, must meet the following conditions:

    i. The rechargeable lithium ion cells can only be charged from the
primary lithium metal cells;
    ii. Overcharge of the rechargeable lithium ion cells is precluded
by design;
    iii. The battery has been tested as a primary lithium battery; and
    iv. Component cells of the battery must be of a type proved to meet
the respective testing requirements of the Manual of Tests and
Criteria, part III, subsection 38.3 (IBR, see Sec.  171.7 of this
subchapter).
    b. Lithium batteries conforming to paragraph a. of this special
provision must be assigned to UN Nos. 3090 or 3091, as appropriate.
When such batteries are transported in accordance with Sec.
173.185(c), the total lithium content of all lithium metal cells
contained in the battery must not exceed 1.5 g and the total capacity
of all lithium ion cells contained in the battery must not exceed 10
Wh.
    389 This entry only applies to lithium ion batteries or lithium
metal batteries installed in a cargo transport unit and designed only
to provide power external to the cargo transport unit. The lithium
batteries must meet the requirements of Sec.  173.185(a) and contain
the necessary systems to prevent overcharge and over discharge between
the batteries. The batteries must be securely attached to the interior
structure of the cargo transport unit (e.g., by means of placement in
racks, cabinets, etc.) in such a manner as to prevent short circuits,
accidental operation, and significant movement relative to the cargo
transport unit under the shocks, loadings, and vibrations normally
incident to transport. Hazardous materials necessary for the safe and
proper operation of the cargo transport unit (e.g., fire extinguishing
systems and air conditioning systems), must be properly secured to or
installed in the cargo transport unit and are not otherwise subject to
this subchapter. Hazardous materials not necessary for the safe and
proper operation of the cargo transport unit must not be transported
within the cargo transport unit. The batteries inside the cargo
transport unit are not subject to marking or labelling requirements of
part 172 subparts D and E of this subchapter. The cargo transport unit
shall display the UN number in a manner in accordance with Sec.
172.332 of this subchapter and be placarded on two opposing sides. For
transportation by aircraft, cargo transport units may only be offered
for transportation and transported under conditions approved by the
Associate Administrator.
    391 Except for articles being transported by motor vehicle as a
material of trade in accordance with Sec.  173.6 of this subchapter,
articles containing hazardous materials of Division 2.3, or Division
4.2, or Division 4.3, or Division 5.1, or Division 5.2, or Division 6.1
(substances with an inhalation toxicity of Packing Group I) and
articles containing more than one of the following hazards: (1) Gases
of Class 2; (2) Liquid desensitized explosives of Class 3; or (3) Self-
reactive substances and solid desensitized explosives of Division 4.1,
may only be offered for transportation and transported under conditions
approved by the Associate Administrator.
* * * * *
    421 This entry will no longer be effective on January 2, 2023,
unless we terminate it earlier or extend it beyond that date by notice
of a final rule in the Federal Register.
    422 When labelling is required, the label to be used must be the
label shown in Sec.  172.447. When a placard is displayed, the placard
must be the placard shown in Sec.  172.560.
    (2) * * *
    A56 Radioactive material with a subsidiary hazard of Division 4.2,
Packing Group I, must be transported in Type B packages when offered
for transportation by aircraft. Where the subsidiary hazard material is
``Forbidden'' in column (9A) or (9B) of the Sec.  172.101 Table, the
radioactive material may only be offered for transportation and
transported by aircraft under conditions approved by the Associate
Administrator.
* * * * *
    A105 a. This entry applies to machinery or apparatus containing
hazardous materials as a residue or as an integral element of the
machinery or apparatus. It must not be used for machinery or apparatus
for which a proper shipping name already exists in the Sec.  172.101
Table.
    b. Where the quantity of hazardous materials contained as an
integral element in machinery or apparatus exceeds the limits permitted
by Sec.  173.222(c)(2), and the hazardous materials meet the provisions
of Sec.  173.222(c), the machinery or apparatus may be transported by
aircraft only with the prior approval of the Associate Administrator.
* * * * *
    (3) * * *
    B136 Non-specification closed bulk bins are authorized.
* * * * *
    (8) * * *
    (ii) * * *
    TP10 A lead lining, not less than 5 mm thick, which shall be tested
annually, or another suitable lining material approved by the competent
authority, is required. A portable tank may be offered for transport
after the date of expiry of the last lining inspection for a period not
to exceed three months for purposes of performing the next required
test or inspection, after emptying but before cleaning.
* * * * *

0
8. In Sec.  172.203, paragraph (o) is revised to read as follows:

Sec.  172.203  Additional description requirements.

* * * * *
    (o) Organic peroxides, polymerizing substances, and self-reactive
materials. The description on a shipping paper for a Division 4.1
(polymerizing substance and self-reactive) material or a Division 5.2
(organic peroxide) material must include the following additional
information, as appropriate:
    (1) If notification or competent authority approval is required,
the shipping paper must contain a statement of approval of the
classification and conditions of transport.
    (2) For Division 4.1 (polymerizing substance and self-reactive) and
Division 5.2 (organic peroxide) materials that require temperature
control during transport, the words ``TEMPERATURE CONTROLLED'' must be
added as part of the proper shipping name, unless already part of the
proper shipping name. The control and emergency temperature must be
included on the shipping paper.
    (3) The word ``SAMPLE'' must be included in association with the
basic description when a sample of a Division 4.1 (self-reactive)
material (see Sec.  173.224(c)(3) of this subchapter) or Division 5.2
(organic peroxide) material (see Sec.  173.225(b)(2) of this
subchapter) is offered for transportation.
* * * * *

0
9. In Sec.  172.407, paragraph (c)(1) is revised to read as follows:

Sec.  172.407  Label specifications.

* * * * *
    (c) * * *
    (1) Each diamond (square-on-point) label prescribed in this subpart
must be at least 100 mm (3.9 inches) on each side with each side having
a solid line inner border approximately 5 mm (.2 inches) inside and
parallel to the edge. The 5 mm (.2 inches) measurement is from the
outside edge of the label to the outside of the solid line forming the
inner border.
    (i) If the size of the package so requires, the dimensions of the
label

and its features may be reduced proportionally provided the symbol and
other elements of the label remain clearly visible.
    (ii) Where dimensions are not specified, all features shall be in
approximate proportion to those shown in Sec. Sec.  172.411 through
172.448 of this subpart, as appropriate.
    (iii) [Reserved]
    (iv) For domestic transportation, a packaging labeled prior to
January 1, 2017, and in conformance with the requirements of this
paragraph in effect on December 31, 2014, may continue in service until
the end of its useful life.
* * * * *

0
10. In, Sec.  172.514 paragraphs (a) and (c)(3) are revised and
paragraph (d) is added to read as follows:

Sec.  172.514  Bulk packagings.

    (a) Except as provided in paragraphs (c) and (d) of this section,
each person who offers for transportation a bulk packaging which
contains a hazardous material, shall affix the placards specified for
the material in Sec. Sec.  172.504 and 172.505.
* * * * *
    (c) * * *
    (3) A bulk packaging other than a portable tank, cargo tank,
flexible bulk container, or tank car (e.g., a bulk bag or box) with a
volumetric capacity of less than 18 cubic meters (640 cubic feet);
* * * * *
    (d) A flexible bulk container may be placarded in two opposing
positions.

0
11. In Sec.  172.604, paragraph (d)(2) is revised to read as follows:

Sec.  172.604  Emergency response telephone number.

* * * * *
    (d) * * *
    (2) Materials properly described under the following shipping
names:
    (i) Battery powered equipment.
    (ii) Battery powered vehicle.
    (iii) Carbon dioxide, solid.
    (iv) Castor bean.
    (v) Castor flake.
    (vi) Castor meal.
    (vii) Castor pomace.
    (viii) Consumer commodity.
    (ix) Dry ice.
    (x) Engine, fuel cell, flammable gas powered.
    (xi) Engine, fuel cell, flammable liquid powered.
    (xii) Engine, internal combustion.
    (xiii) Engine, internal combustion, flammable gas powered.
    (xiv) Engine, internal combustion, flammable liquid powered.
    (xv) Fish meal, stabilized.
    (xvi) Fish scrap, stabilized.
    (xvii) Krill Meal, PG III.
    (xviii) Machinery, internal combustion.
    (xix) Machinery, fuel cell, flammable gas powered.
    (xx) Machinery, fuel cell, flammable liquid powered.
    (xxi) Machinery, internal combustion, flammable gas powered.
    (xxii) Machinery, internal combustion, flammable liquid powered.
    (xxiii) Refrigerating machine.
    (xxiv) Vehicle, flammable gas powered.
    (xxv) Vehicle, flammable liquid powered.
    (xxvi) Wheelchair, electric.
* * * * *

0
12. In Sec.  172.800, paragraph (b)(15) is revised to read as follows:

Sec.  172.800  Purpose and applicability.

* * * * *
    (b) * * *
    (15) International Atomic Energy Agency Code of Conduct (IBR, see
Sec.  171.7) Category 1 and 2 materials, Nuclear Regulatory Commission,
Category 1 and Category 2 radioactive materials as listed in Table 1,
Appendix A to 10 CFR part 37, and Highway Route Controlled quantities
as defined in 49 CFR 173.403.
* * * * *

PART 173--SHIPPERS--GENERAL REQUIREMENTS FOR SHIPMENTS AND
PACKAGINGS

0
13. The authority citation for part 173 continues to read as follows:

    Authority: 49 U.S.C. 5101-5128, 44701; 49 CFR 1.81, 1.96 and
1.97.

0
14. In Sec.  173.2a, revise paragraph (a) introductory text to read as
follows:

Sec.  173.2a  Classification of a material having more than one hazard.

    (a) Classification of a material having more than one hazard.
Except as provided in paragraph (c) of this section, a material not
specifically listed in the Sec.  172.101 Table or assigned to an entry
of articles containing hazardous materials (UN3537 to UN3548) that
meets the definition of more than one hazard class or division as
defined in this part, shall be classed according to the highest
applicable hazard class of the following hazard classes, which are
listed in descending order of hazard:
* * * * *

0
15. In Sec.  173.6, paragraph (a)(7) is added and paragraph (b)(3) is
revised to read as follows:

Sec.  173.6  Materials of trade exceptions.

* * * * *
    (a) * * *
    (7) For a material or article for which Column (5) of the Hazardous
Materials Table in Sec.  172.101 of this subchapter does not indicate a
packing group. Authorized amounts are:
    (i) For Classes or Divisions indicated in paragraph (a)(1) of this
section, the amounts shown in paragraph (a)(1)(ii).
    (ii) For Division 4.3, the amounts shown in paragraph (a)(3) of
this section.
    (b) * * *
    (3) Outer packagings are not required for receptacles (e.g., cans
and bottles) or articles that are secured against shifting in cages,
carts, bins, boxes, or compartments or by other means.
* * * * *

0
16. In Sec.  173.21, revise paragraph (f) introductory text and
paragraph (f)(1) to read as follows:

Sec.  173.21  Forbidden materials and packages.

* * * * *
    (f) A package containing a material which is likely to decompose
with a self-accelerated decomposition temperature (SADT) or polymerize
with a self-accelerated polymerization temperature (SAPT) of 50 [deg]C
(122 [deg]F) or less, with an evolution of a dangerous quantity of heat
or gas when decomposing or polymerizing, unless the material is
stabilized or inhibited in a manner to preclude such evolution. The
SADT and SAPT may be determined by any of the test methods described in
Part II of the UN Manual of Tests and Criteria (IBR, see Sec.  171.7 of
this subchapter).
    (1) A package meeting the criteria of paragraph (f) of this section
may be required to be shipped under controlled temperature conditions.
The control temperature and emergency temperature for a package shall
be as specified in the table in this paragraph (f)(1) based upon the
SADT or SAPT of the material. The control temperature is the
temperature above which a package of the material may not be offered
for transportation or transported. The emergency temperature is the
temperature at which, due to imminent danger, emergency measures must
be initiated.

                  Table 1 to Paragraph (f)(1)--Derivation of Control and Emergency Temperature
----------------------------------------------------------------------------------------------------------------
               SADT/SAPT \1\                        Control temperatures              Emergency temperature
----------------------------------------------------------------------------------------------------------------
SADT/SAPT <=20 [deg]C (68 [deg]F)..........  20 [deg]C (36 [deg]F) below SADT/  10 [deg]C (18 [deg]F) below SADT/
                                              SAPT.                              SAPT.
20 [deg]C (68 [deg]F) =1%
shall be taken into account, or <1% if these ingredients are still
relevant for

classifying the mixture to be corrosive to skin.
    (ii) To determine whether a mixture containing corrosive substances
must be considered a corrosive mixture and to assign a packing group,
the calculation method in the flow chart in Appendix I must be applied.
For this calculation method, generic concentration limits apply where
1% is used in the first step for the assessment of the packing group I
substances, and where 5% is used for the other steps respectively.
    (iii) When a specific concentration limit (SCL) is assigned to a
substance following its entry in the Hazardous Materials Table or in a
special provision, this limit shall be used instead of the generic
concentration limits (GCL).
    (iv) The following formula must be used for each step of the
calculation process. The criterion for a packing group is fulfilled
when the result of the calculation is >= 1. The generic concentration
limits to be used for the evaluation in each step of the calculation
method are those found in Appendix I of this part. Where applicable,
the generic concentration limit shall be substituted by the specific
concentration limit assigned to the substance(s) (SCLi), and the
adapted formula is a weighted average of the different concentration
limits assigned to the different substances in the mixture:
[GRAPHIC] [TIFF OMITTED] TR11MY20.001

PG xi = concentration of substance 1, 2 . . .i in the
mixture, assigned to packing group x (I, II or III)
GCL = generic concentration limit
SCLi = specific concentration limit assigned to substance
i

Note to Sec.  173.137: When an initial test on either a steel or
aluminum surface indicates the material being tested is corrosive, the
follow up test on the other surface is not required.

0
25. In Sec.  173.159, paragraphs (a)(2)(i) through (iii) and (d)(1) are
revised to read as follows:

Sec.  173.159  Batteries, wet.

    (a) * * *
    (2) * * *
    (i) Packaging each battery or each battery-powered device when
practicable, in fully enclosed inner packagings made of electrically
non-conductive material;
    (ii) Separating or packaging batteries and battery-powered devices
in a manner to prevent contact with other batteries, devices or
electrically conductive materials (e.g., metal) in the packagings; or
    (iii) Ensuring exposed terminals are protected with electrically
non-conductive caps, electrically non-conductive tape, or by other
appropriate means; and;
* * * * *
    (d) * * *
    (1) Electric storage batteries are firmly secured to skids or
pallets capable of withstanding the shocks normally incident to
transportation are authorized for transportation by rail, highway, or
vessel. The height of the completed unit must not exceed 1\1/2\ times
the width of the skid or pallet. The unit must be capable of
withstanding, without damage, a superimposed weight equal to two times
the weight of the unit or, if the weight of the unit exceeds 907 kg
(2,000 pounds), a superimposed weight of 1,814 kg (4,000 pounds).
Battery terminals must not be relied upon to support any part of the
superimposed weight and must not short out if an electrically
conductive material is placed in direct contact with them.
* * * * *

0
26. Revise Sec.  173.185 to read as follows:

Sec.  173.185  Lithium cells and batteries.

    As used in this section, consignment means one or more packages of
hazardous materials accepted by an operator from one shipper at one
time and at one address, receipted for in one lot and moving to one
consignee at one destination address. Equipment means the device or
apparatus for which the lithium cells or batteries will provide
electrical power for its operation. Lithium cell(s) or battery(ies)
includes both lithium metal and lithium ion chemistries. Medical device
means an instrument, apparatus, implement, machine, contrivance,
implant, or in vitro reagent, including any component, part, or
accessory thereof, which is intended for use in the diagnosis of
disease or other conditions, or in the cure, mitigation, treatment, or
prevention of disease, of a person.
    (a) Classification. (1) Each lithium cell or battery must be of the
type proven to meet the criteria in part III, sub-section 38.3 of the
UN Manual of Tests and Criteria (IBR; see Sec.  171.7 of this
subchapter). Lithium cells and batteries are subject to these tests
regardless of whether the cells used to construct the battery are of a
tested type. A single cell battery as defined in part III, sub-section
38.3 of the UN Manual of Tests and Criteria is considered a ``cell''
and must be offered for transportation in accordance with the
requirements for cells.
    (i) Cells and batteries manufactured according to a type meeting
the requirements of sub-section 38.3 of the UN Manual of Tests and
Criteria, Revision 3, Amendment 1 or any subsequent revision and
amendment applicable at the date of the type testing may continue to be
transported, unless otherwise provided in this subchapter.
    (ii) Cell and battery types only meeting the requirements of the UN
Manual of Tests and Criteria, Revision 3, are no longer valid. However,
cells and batteries manufactured in conformity with such types before
July 2003 may continue to be transported if all other applicable
requirements are fulfilled.
    (2) Each person who manufactures lithium cells or batteries must
create a record of satisfactory completion of the testing (e.g. test
report) required by this paragraph prior to offering the lithium cell
or battery for transport and must:
    (i) Maintain this record for as long as that design is offered for
transportation and for one year thereafter; and
    (ii) Make this record available to an authorized representative of
the Federal, state or local government upon request.
    (3) Beginning January 1, 2022 each manufacturer and subsequent
distributor of lithium cells or batteries manufactured on or after
January 1, 2008, must make available a test summary. The test summary
must include the following elements:
    (i) Name of cell, battery, or product manufacturer, as applicable;
    (ii) Cell, battery, or product manufacturer's contact information
to include address, telephone number, email address, and website for
more information;
    (iii) Name of the test laboratory, to include address, telephone
number, email address, and website for more information;
    (iv) A unique test report identification number;
    (v) Date of test report;

    (vi) Description of cell or battery to include at a minimum;
    (A) Lithium ion or lithium metal cell or battery;
    (B) Mass of cell or battery;
    (C) Watt-hour rating, or lithium content;
    (D) Physical description of the cell/battery; and
    (E) Cell or battery model number or, alternatively, if the test
summary is established for a product containing a cell or battery, the
product model number.
    (vii) List of tests conducted and results (i.e., pass/fail);
    (viii) Reference to assembled battery testing requirements (if
applicable);
    (ix) Reference to the revised edition of the UN Manual of Tests and
Criteria used and to amendments thereto, if any; and
    (x) Signature with name and title of signatory as an indication of
the validity of information provided.
    (4) Except for cells or batteries meeting the requirements of
paragraph (c) of this section, each lithium cell or battery must:
    (i) Incorporate a safety venting device or be designed to preclude
a violent rupture under conditions normally incident to transport;
    (ii) Be equipped with means of preventing external short circuits;
and
    (iii) Be equipped with a means of preventing dangerous reverse
current flow (e.g., diodes or fuses) if a battery contains cells, or a
series of cells that are connected in parallel.
    (b) Packaging. (1) Each package offered for transportation
containing lithium cells or batteries, including lithium cells or
batteries packed with, or contained in, equipment, must meet all
applicable requirements of subpart B of this part.
    (2) Lithium cells or batteries, including lithium cells or
batteries packed with, or contained in, equipment, must be packaged in
a manner to prevent:
    (i) Short circuits;
    (ii) Damage caused by movement or placement within the package; and
    (iii) Accidental activation of the equipment.
    (3) For packages containing lithium cells or batteries offered for
transportation:
    (i) The lithium cells or batteries must be placed in non-metallic
inner packagings that completely enclose the cells or batteries, and
separate the cells or batteries from contact with equipment, other
devices, or electrically conductive materials (e.g., metal) in the
packaging.
    (ii) The inner packagings containing lithium cells or batteries
must be placed in one of the following packagings meeting the
requirements of part 178, subparts L and M, of this subchapter at the
Packing Group II level:
    (A) Metal (4A, 4B, 4N), wooden (4C1, 4C2, 4D, 4F), fiberboard (4G),
or solid plastic (4H1, 4H2) box;
    (B) Metal (1A2, 1B2, 1N2), plywood (1D), fiber (1G), or plastic
(1H2) drum;
    (C) Metal (3A2, 3B2) or plastic (3H2) jerrican.
    (iii) When packed with equipment, lithium cells or batteries must:
    (A) Be placed in inner packagings that completely enclose the cell
or battery, then placed in an outer packaging. The completed package
for the cells or batteries must meet the Packing Group II performance
requirements as specified in paragraph (b)(3)(ii) of this section; or
    (B) Be placed in inner packagings that completely enclose the cell
or battery, then placed with equipment in a package that meets the
Packing Group II performance requirements as specified in paragraph
(b)(3)(ii) of this section.
    (4) When lithium cells or batteries are contained in equipment:
    (i) The outer packaging, when used, must be constructed of suitable
material of adequate strength and design in relation to the capacity
and intended use of the packaging, unless the lithium cells or
batteries are afforded equivalent protection by the equipment in which
they are contained;
    (ii) Equipment must be secured to prevent damage caused by movement
within the outer packaging and be packed so as to prevent accidental
operation during transport; and
    (iii) Any spare lithium cells or batteries packed with the
equipment must be packaged in accordance with paragraph (b)(3) of this
section.
    (5) Lithium batteries that weigh 12 kg (26.5 pounds) or more and
have a strong, impact-resistant outer casing and assemblies of such
batteries, may be packed in strong outer packagings; in protective
enclosures (for example, in fully enclosed or wooden slatted crates);
or on pallets or other handling devices, instead of packages meeting
the UN performance packaging requirements in paragraphs (b)(3)(ii) and
(b)(3)(iii) of this section. Batteries or battery assemblies must be
secured to prevent inadvertent movement, and the terminals may not
support the weight of other superimposed elements. Batteries or battery
assemblies packaged in accordance with this paragraph may be
transported by cargo aircraft if approved by the Associate
Administrator.
    (6) Except for transportation by aircraft, the following rigid
large packagings are authorized for a single battery, and for a single
item of equipment containing batteries, meeting provisions in
paragraphs (b)(1) and (2) of this section and the requirements of part
178, subparts P and Q, of this subchapter at the Packing Group II
level:
    (i) Metal (50A, 50B, 50N) metal packagings must be fitted with an
electrically non-conductive lining material (e.g., plastics) of
adequate strength for the intended use;
    (ii) Rigid plastic (50H);
    (iii) Wooden (50C, 50D, 50F);
    (iv) Rigid fiberboard (50G).
    (7) For transportation by aircraft, lithium cells and batteries
must not be packed in the same outer packaging with substances and
articles of Class 1 (explosives) other than Division 1.4S, Division 2.1
(flammable gases), Class 3 (flammable liquids), Division 4.1 (flammable
solids), or Division 5.1 (oxidizers).
    (c) Exceptions for smaller cells or batteries. Other than as
specifically stated below, a package containing lithium cells or
batteries, or lithium cells or batteries packed with, or contained in,
equipment, that meets the conditions of this paragraph is excepted from
the requirements in subparts C through H of part 172 of this subchapter
and the UN performance packaging requirements in paragraphs (b)(3)(ii)
and (iii) of this section under the following conditions and
limitations.
    (1) Size limits. (i) The Watt-hour (Wh) rating may not exceed 20 Wh
for a lithium ion cell or 100 Wh for a lithium ion battery. After
December 31, 2015, each lithium ion battery subject to this provision
must be marked with the Watt-hour rating on the outside case.
    (ii) The lithium content may not exceed 1 g for a lithium metal
cell or 2 g for a lithium metal battery.
    (iii) Except when lithium cells or batteries are packed with or
contained in equipment in quantities not exceeding 5 kg net weight, the
outer package that contains lithium cells or batteries must be
appropriately marked: ``PRIMARY LITHIUM BATTERIES--FORBIDDEN FOR
TRANSPORT ABOARD PASSENGER AIRCRAFT'', ``LITHIUM METAL BATTERIES--
FORBIDDEN FOR TRANSPORT ABOARD PASSENGER AIRCRAFT'', ``LITHIUM ION
BATTERIES--FORBIDDEN FOR TRANSPORT ABOARD PASSENGER AIRCRAFT'' or
labeled with a ``CARGO AIRCRAFT ONLY'' label specified in Sec.  172.448
of this subchapter.
    (iv) For transportation by highway or rail only, the lithium
content of the cell and battery may be increased to 5 g for a lithium
metal cell or 25 g for a lithium metal battery and 60 Wh for a lithium

ion cell or 300 Wh for a lithium ion battery, provided the outer
package is marked: ``LITHIUM BATTERIES--FORBIDDEN FOR TRANSPORT ABOARD
AIRCRAFT AND VESSEL.''
    (v) The marking specified in paragraphs (c)(1)(iii) and (iv) of
this section must have a background of contrasting color, and the
letters in the marking must be:
    (A) At least 6 mm (0.25 inch) in height on packages having a gross
weight of 30 kg (66 pounds) or less, except that smaller font may be
used as necessary when package dimensions so require.
    (B) At least 12 mm (0.5 inch) in height on packages having a gross
weight of more than 30 kg (66 pounds).
    (vi) Except when lithium cells or batteries are packed with, or
contained in, equipment, each package must not exceed 30 kg (66 pounds)
gross weight.
    (2) Packaging. Lithium cells and batteries must be packed in inner
packagings that completely enclose the cell or battery then placed in a
strong rigid outer package unless the cell or battery is contained in
equipment and is afforded equivalent protection by the equipment in
which it is contained. Except when lithium cells or batteries are
contained in equipment, each package of lithium cells or batteries, or
the completed package when packed with equipment, must be capable of
withstanding a 1.2 meter drop test, in any orientation, without damage
to the cells or batteries contained in the package, without shifting of
the contents that would allow battery-to-battery (or cell-to-cell)
contact, and without release of the contents of the package.
    (3) Hazard communication. Each package must display the lithium
battery mark except when a package contains button cell batteries
installed in equipment (including circuit boards), or no more than four
lithium cells or two lithium batteries contained in equipment, where
there are not more than two packages in the consignment.
    (i) The mark must indicate the UN number: ``UN3090'' for lithium
metal cells or batteries; or ``UN3480'' for lithium ion cells or
batteries. Where the lithium cells or batteries are contained in, or
packed with, equipment, the UN number ``UN3091'' or ``UN3481,'' as
appropriate, must be indicated. Where a package contains lithium cells
or batteries assigned to different UN numbers, all applicable UN
numbers must be indicated on one or more marks. The package must be of
such size that there is adequate space to affix the mark on one side
without the mark being folded.
[GRAPHIC] [TIFF OMITTED] TR11MY20.002

    (A) The mark must be in the form of a rectangle with hatched
edging. The mark must be not less than 120 mm (4.7 inches) wide by 110
mm (4.3 inches) high and the minimum width of the hatching must be 5 mm
(0.2 inches), except marks of 105 mm (4.1 inches) wide by 74 mm (2.9
inches) high may be used on a package containing lithium batteries when
the package is too small for the larger mark;
    (B) The symbols and letters must be black on white or suitable
contrasting background and the hatching must be red;
    (C) The ``*'' must be replaced by the appropriate UN number(s) and
the ``**'' must be replaced by a telephone number for additional
information; and
    (D) Where dimensions are not specified, all features shall be in
approximate proportion to those shown.
    (ii) [Reserved]
    (iii) When packages are placed in an overpack, the lithium battery
mark shall either be clearly visible through the overpack or be
reproduced on the outside of the overpack and the overpack shall be
marked with the word ``OVERPACK''. The lettering of the ``OVERPACK''
mark shall be at least 12 mm (0.47 inches) high.
    (4) Air transportation. (i) For transportation by aircraft, lithium
cells and batteries may not exceed the limits in the following Table 1
to paragraph (c)(4)(i). The limits on the maximum number of batteries
and maximum net quantity of batteries in the following table may not be
combined in the same package:

                                                             Table 1 to Paragraph (c)(4)(i)
--------------------------------------------------------------------------------------------------------------------------------------------------------
                                     Lithium metal       Lithium metal       Lithium metal                                                Lithium ion
                                     cells and/or        cells with a      batteries with a    Lithium ion cells   Lithium ion cells   batteries with a
                                   batteries with a     lithium content     lithium content    and/or batteries    with a watt-hour    watt-hour rating
            Contents                lithium content     more than 0.3 g     more than 0.3 g    with a watt-hour    rating more than    more than 2.7 Wh
                                   not more than 0.3   but not more than   but not more than    rating not more     2.7 Wh but not     but not more than
                                           g                  1 g                 2 g             than 2.7 Wh       more than 20 Wh         100 Wh
--------------------------------------------------------------------------------------------------------------------------------------------------------
Maximum number of cells/          No Limit..........  8 cells...........  2 batteries.......  No Limit..........  8 cells...........  2 batteries.
 batteries per package.
Maximum net quantity (mass) per   2.5 kg............  n/a...............  n/a...............  2.5 kg............  n/a...............  n/a.
 package.
--------------------------------------------------------------------------------------------------------------------------------------------------------

    (ii) Not more than one package prepared in accordance with this
paragraph (c)(4) may be placed into an overpack. When a package is
required to display the ``CARGO AIRCRAFT ONLY'' label, the paragraph
(c)(1)(iii) mark, or the paragraph (c)(3)(i) lithium battery mark and
the package is placed in an overpack, the appropriate label or mark
must either be clearly visible through the overpack, or the label or
mark must also be affixed on the outside of the overpack, and the
overpack must be marked with the word ``OVERPACK''. The lettering of
the ``OVERPACK'' mark shall be at least 12 mm (0.47 inches) high.
    (iii) A shipper is not permitted to offer for transport more than
one package prepared in accordance with the provisions of this
paragraph in any single consignment.
    (iv) Each shipment with packages required to display the paragraph
(c)(3)(i) lithium battery mark must include an indication on the air
waybill of compliance with this paragraph (c)(4) (or the applicable
ICAO Technical Instructions Packing Instruction), when an air waybill
is used.
    (v) Packages and overpacks of lithium batteries prepared in
accordance with this paragraph (c)(4) must be offered to the operator
separately from cargo which is not subject to the requirements of this
subchapter and must not be loaded into a unit load device before being
offered to the operator.
    (vi) For lithium batteries packed with, or contained in, equipment,
the number of batteries in each package is limited to the minimum
number required to power the piece of equipment, plus two spare sets,
and the total net quantity (mass) of the lithium cells or batteries in
the completed package must not exceed 5 kg. A ``set'' of cells or
batteries is the number of individual cells or batteries that are
required to power each piece of equipment.
    (vii) Each person who prepares a package for transport containing
lithium cells or batteries, including cells or batteries packed with,
or contained in, equipment in accordance with the conditions and
limitations of this paragraph (c)(4), must receive instruction on these
conditions and limitations, corresponding to their functions.
    (viii) Lithium cells and batteries must not be packed in the same
outer packaging with other hazardous materials. Packages prepared in
accordance with this paragraph (c)(4) must not be placed into an
overpack with packages containing hazardous materials and articles of
Class 1 (explosives) other than Division 1.4S, Division 2.1 (flammable
gases), Class 3 (flammable liquids), Division 4.1 (flammable solids) or
Division 5.1 (oxidizers).
    (5) For transportation by aircraft, a package that exceeds the
number or quantity (mass) limits in the table shown in paragraph
(c)(4)(i) of this section, the overpack limit described in paragraph
(c)(4)(ii) of this section, or the consignment limit described in
paragraph (c)(4)(iii) of this section is subject to all applicable
requirements of this subchapter, except that a package containing no
more than 2.5 kg lithium metal cells or batteries or 10 kg lithium ion
cells or batteries is not subject to the UN performance packaging
requirements in paragraph (b)(3)(ii) of this section when the package
displays both the lithium battery mark in paragraph (c)(3)(i) and the
Class 9 Lithium Battery label specified in Sec.  172.447 of this
subchapter. This paragraph does not apply to batteries or cells packed
with or contained in equipment.
    (d) Lithium cells or batteries shipped for disposal or recycling. A
lithium cell or battery, including a lithium cell or battery contained
in equipment, that is transported by motor vehicle to a permitted
storage facility or disposal site, or for purposes of recycling, is
excepted from the testing and record keeping requirements of paragraph
(a) and the UN performance packaging requirements in paragraphs
(b)(3)(ii), (b)(3)(iii) and (b)(6) of this section, when packed in a
strong outer packaging conforming to the applicable requirements of
subpart B of this part. A lithium cell or battery that meets the size,
packaging, and hazard communication conditions in paragraph (c)(1)-(3)
of this section is excepted from subparts C through H of part 172 of
this subchapter.
    (e) Low production runs and prototypes. Low production runs (i.e.,
annual production runs consisting of not more than 100 lithium cells or
batteries), prototype lithium cells or batteries transported for
purposes of testing, and equipment containing such cells or batteries
are excepted from the testing and record keeping requirements of
paragraph (a) of this section, provided:
    (1) Except as provided in paragraph (e)(5) of this section, each
cell or battery is individually packed in a non-metallic inner
packaging, inside an outer packaging, and is surrounded by cushioning
material that is non-combustible and electrically non-conductive, or
contained in equipment. Equipment must be constructed or packaged in a
manner as to prevent accidental operation during transport;
    (2) Appropriate measures shall be taken to minimize the effects of
vibration and shocks and prevent movement of the cells or batteries
within the package that may lead to damage and a dangerous condition
during transport. Cushioning material that is non-combustible and
electrically non-conductive may be used to meet this requirement;
    (3) The lithium cells or batteries are packed in inner packagings
or contained in equipment. The inner packaging or equipment is placed
in one of the following outer packagings that meet the requirements of
part 178, subparts L and M, of this subchapter at the Packing Group I
level. Cells and batteries, including equipment of different sizes,
shapes or masses must be placed into an outer packaging of a tested
design type listed in this section provided the total gross mass of the
package does not

exceed the gross mass for which the design type has been tested. A cell
or battery with a net mass of more than 30 kg is limited to one cell or
battery per outer packaging;
    (i) Metal (4A, 4B, 4N), wooden (4C1, 4C2, 4D, 4F), or solid plastic
(4H2) box;
    (ii) Metal (1A2, 1B2, 1N2), plywood (1D), or plastic (1H2) drum.
    (4) For a single battery, and for a single item of equipment
containing cells or batteries, the following rigid large packagings are
authorized:
    (i) Metal (50A, 50B, 50N) metal packagings must be fitted with an
electrically non-conductive lining material (e.g., plastics) of
adequate strength for the intended use;
    (ii) Rigid plastic (50H);
    (iii) Plywood (50D).
    (5) Lithium batteries, including lithium batteries contained in
equipment, that weigh 12 kg (26.5 pounds) or more and have a strong,
impact-resistant outer casing or assemblies of such batteries, may be
packed in strong outer packagings, in protective enclosures (for
example, in fully enclosed or wooden slatted crates), or on pallets or
other handling devices, instead of packages meeting the UN performance
packaging requirements in paragraphs (b)(3)(ii) and (iii) of this
section. The battery or battery assembly must be secured to prevent
inadvertent movement, and the terminals may not support the weight of
other superimposed elements;
    (6) Irrespective of the limit specified in column (9B) of the Sec.
172.101 Hazardous Materials Table, the battery or battery assembly
prepared for transport in accordance with this paragraph may have a
mass exceeding 35 kg gross weight when transported by cargo aircraft;
    (7) Batteries or battery assemblies packaged in accordance with
this paragraph are not permitted for transportation by passenger-
carrying aircraft, and may be transported by cargo aircraft only if
approved by the Associate Administrator prior to transportation; and
    (8) Shipping papers must include the following notation:
``Transport in accordance with Sec.  173.185(e).''
    (f) Damaged, defective, or recalled cells or batteries. Lithium
cells or batteries that have been damaged or identified by the
manufacturer as being defective for safety reasons, that have the
potential of producing a dangerous evolution of heat, fire, or short
circuit (e.g., those being returned to the manufacturer for safety
reasons) may be transported by highway, rail or vessel only, and must
be packaged as follows:
    (1) Each cell or battery must be placed in individual, non-metallic
inner packaging that completely encloses the cell or battery;
    (2) The inner packaging must be surrounded by cushioning material
that is non-combustible, electrically non-conductive, and absorbent;
and
    (3) Each inner packaging must be individually placed in one of the
following packagings meeting the applicable requirements of part 178,
subparts L, M, P, and Q of this subchapter at the Packing Group I
level:
    (i) Metal (4A, 4B, 4N), wooden (4C1, 4C2, 4D, 4F), or solid plastic
(4H2) box;
    (ii) Metal (1A2, 1B2, 1N2), plywood (1D), or plastic (1H2) drum; or
    (iii) For a single battery, and for a single item of equipment
containing cells or batteries, the following rigid large packagings are
authorized:
    (A) Metal (50A, 50B, 50N);
    (B) Rigid plastic (50H);
    (C) Plywood (50D); and
    (4) The outer package must be marked with an indication that the
package contains a ``Damaged/defective lithium ion battery'' and/or
``Damaged/defective lithium metal battery'' as appropriate. The marking
required by this paragraph must be in characters at least 12 mm (0.47
inches) high.
    (g) Limited exceptions to restrictions on air transportation of
medical device batteries. Irrespective of the quantity limitations
described in column 9A of the Sec.  172.101 Hazardous Materials Table
of this subchapter, up to two replacement lithium cells or batteries
specifically used for a medical device as defined in this section may
be transported as cargo on a passenger aircraft. Packages containing
these cells or batteries are not subject to the marking requirement in
paragraph (c)(1)(iii) of this section or the ``CARGO AIRCRAFT ONLY''
label required by Sec.  172.402(c) of this subchapter and may be
transported as cargo on a passenger aircraft when approved by the
Associate Administrator and provided the following conditions are met:
    (1) The intended destination of the cells or batteries is not
serviced daily by cargo aircraft if a cell or battery is required for
medically necessary care; and
    (2) Lithium ion cells or batteries for medical devices are excepted
from the state of charge limitations in Sec.  172.102, special
provision A100, of this subchapter, provided each cell or battery is:
    (i) Individually packed in an inner packaging that completely
encloses the cell or battery;
    (ii) Placed in a rigid outer packaging; and
    (iii) Protected to prevent short circuits.
    (h) Approval. A lithium cell or battery that does not conform to
the provisions of this subchapter may be transported only under
conditions approved by the Associate Administrator.

0
27. In Sec.  173.218, paragraph (c) is revised to read as follows:

Sec.  173.218  Fish meal or fish scrap.

* * * * *
    (c) When fish scrap or fish meal is offered for transportation by
vessel in bulk in freight containers, the fish scrap or fish meal shall
contain at least 50 ppm (mg/kg) of ethoxyquin, 100 ppm (mg/kg) of
butylated hydroxytoluene (BHT) or 250 ppm (mg/kg) of tocopherol based
antioxidant at the time of shipment.

0
28. In Sec.  173.220, paragraph (b)(2)(ii)(C) is added and paragraph
(d) is revised to read as follows:

Sec.  173.220  Internal combustion engines, vehicles, machinery
containing internal combustion engines, battery-powered equipment or
machinery, fuel cell-powered equipment or machinery.

* * * * *
    (b) * * *
    (2) * * *
    (ii) * * *
    (C) If a vehicle is powered by a flammable liquid and a flammable
gas internal combustion engine, the requirements of paragraphs (b)(1)
of this section must also be met.
* * * * *
    (d) Lithium batteries. Except as provided in Sec.  172.102, special
provision A101, of this subchapter, vehicles, engines, and machinery
powered by lithium metal batteries that are transported with these
batteries installed are forbidden aboard passenger-carrying aircraft.
Lithium batteries contained in vehicles, engines, or mechanical
equipment must be securely fastened in the battery holder of the
vehicle, engine, or mechanical equipment, and be protected in such a
manner as to prevent damage and short circuits (e.g., by the use of
non-conductive caps that cover the terminals entirely). Except for
vehicles, engines, or machinery transported by highway, rail, or vessel
with prototype or low production lithium batteries securely installed,
each lithium battery must be of a type that has successfully passed
each test in the UN Manual of Tests and Criteria (IBR, see Sec.  171.7
of this subchapter), as specified in Sec.  173.185, unless approved by
the Associate Administrator. Where a vehicle could possibly be handled
in other than an upright position, the vehicle must be

secured in a strong, rigid outer packaging. The vehicle must be secured
by means capable of restraining the vehicle in the outer packaging to
prevent any movement during transport which would change the
orientation or cause the vehicle to be damaged. Where the lithium
battery is removed from the vehicle and is packed separate from the
vehicle in the same outer packaging, the package must be consigned as
``UN 3481, Lithium ion batteries packed with equipment'' or ``UN 3091,
Lithium metal batteries packed with equipment'' and prepared in
accordance with the requirements specified in Sec.  173.185.
* * * * *

0
29. In Sec.  173.222, paragraphs (c) and (d) are revised to read as
follows:

Sec.  173.222  Dangerous goods in equipment, machinery or apparatus.

* * * * *
    (c)(1) Except for transportation by aircraft, the total net
quantity of hazardous materials contained in one item of machinery or
apparatus must not exceed the following:
    (i) In the case of solids or liquids, the limited quantity amount
specified in the corresponding section referenced in Column (8A) of the
Sec.  172.101 Table;
    (ii) 0.5 kg (1.1 pounds) in the case of Division 2.2 gases.
    (iii) When machinery or apparatus contains multiple hazardous
materials, the quantity of each hazardous material must not exceed the
quantity specified in the corresponding section referenced in Column
(8A) of the Sec.  172.101 Table, or for gases, paragraph (c)(1)(ii) of
this section.
    (2) For transportation by aircraft, the total net quantity of
hazardous materials contained in one item of machinery or apparatus
must not exceed the following:
    (i) 1 kg (2.2 pounds) in the case of solids;
    (ii) 0.5 L (0.1 gallons) in the case of liquids;
    (iii) 0.5 kg (1.1 pounds) in the case of Division 2.2 gases.
Division 2.2 gases with subsidiary risks and refrigerated liquefied
gases are not authorized;
    (iv) A total quantity of not more than the aggregate of that
permitted in paragraphs (c)(2)(i) through (iii) of this section, for
each category of material in the package, when a package contains
hazardous materials in two or more of the categories in paragraphs
(c)(2)(i) through (iii) of this section; and
    (d) Except for transportation by aircraft, when a package contains
hazardous materials in two or more of the categories listed in
paragraph (c)(1) of this section the total quantity required by Sec.
172.202(c) of this subchapter to be entered on the shipping paper must
be either the aggregate quantity, or the estimated quantity, of all
hazardous materials, expressed as net mass.

0
30. In Sec.  173.224, revise paragraph (b)(4), the table to paragraph
(b), and paragraph (c) to read as follows:

Sec.  173.224  Packaging and control and emergency temperatures for
self-reactive materials.

* * * * *
    (b) * * *
    (4) Packing method. Column 4 specifies the highest packing method
which is authorized for the self-reactive material. A packing method
corresponding to a smaller package size may be used, but a packing
method corresponding to a larger package size may not be used. The
Table of Packing Methods in Sec.  173.225(d) defines the packing
methods. Bulk packagings for Type F self-reactive substances are
authorized by Sec.  173.225(f) for IBCs and Sec.  173.225(h) for bulk
packagings other than IBCs. The formulations listed in Sec.  173.225(f)
for IBCs and in Sec.  173.225(g) for portable tanks may also be
transported packed in accordance with packing method OP8, with the same
control and emergency temperatures, if applicable. Additional bulk
packagings are authorized if approved by the Associate Administrator.
* * * * *

                                                              Self-Reactive Materials Table
--------------------------------------------------------------------------------------------------------------------------------------------------------
                                                                                Control
                    Self-reactive substance                      Identification     Concentration    Packing     temperature      Emergency      Notes
                                                                       No.               (%)          method      ([deg]C)       temperature
(1)                                                                          (2)               (3)        (4)             (5)             (6)        (7)
--------------------------------------------------------------------------------------------------------------------------------------------------------
Acetone-pyrogallol copolymer 2-diazo-1-naphthol-5-sulphonate..              3228               100        OP8  ..............  ..............  .........
Azodicarbonamide formulation type B, temperature controlled...              3232              <100        OP5  ..............  ..............          1
Azodicarbonamide formulation type C...........................              3224              <100        OP6  ..............  ..............  .........
Azodicarbonamide formulation type C, temperature controlled...              3234              <100        OP6  ..............  ..............          1
Azodicarbonamide formulation type D...........................              3226              <100        OP7  ..............  ..............  .........
Azodicarbonamide formulation type D, temperature controlled...              3236              <100        OP7  ..............  ..............          1
2,2'-Azodi(2,4-dimethyl-4-methoxyvaleronitrile)...............              3236               100        OP7              -5              +5  .........
2,2'-Azodi(2,4-dimethylvaleronitrile).........................              3236               100        OP7             +10             +15  .........
2,2'-Azodi(ethyl 2-methylpropionate)..........................              3235               100        OP7             +20             +25  .........
1,1-Azodi(hexahydrobenzonitrile)..............................              3226               100        OP7  ..............  ..............  .........
2,2-Azodi(isobutyronitrile)...................................              3234               100        OP6             +40             +45  .........
2,2'-Azodi(isobutyronitrile) as a water based paste...........              3224              <=50        OP6  ..............  ..............  .........
2,2-Azodi(2-methylbutyronitrile)..............................              3236               100        OP7             +35             +40  .........
Benzene-1,3-disulphonylhydrazide, as a paste..................              3226                52        OP7  ..............  ..............  .........
Benzene sulphohydrazide.......................................              3226               100        OP7  ..............  ..............  .........
4-(Benzyl(ethyl)amino)-3-ethoxybenzenediazonium zinc chloride.              3226               100        OP7  ..............  ..............  .........
4-(Benzyl(methyl)amino)-3-ethoxybenzenediazonium zinc chloride              3236               100        OP7             +40             +45  .........
3-Chloro-4-diethylaminobenzenediazonium zinc chloride.........              3226               100        OP7  ..............  ..............  .........
2-Diazo-1-Naphthol sulphonic acid ester mixture...............              3226              <100        OP7  ..............  ..............          4

2-Diazo-1-Naphthol-4-sulphonyl chloride.......................              3222               100        OP5  ..............  ..............  .........
2-Diazo-1-Naphthol-5-sulphonyl chloride.......................              3222               100        OP5  ..............  ..............  .........
2,5-Dibutoxy-4-(4-morpholinyl)-Benzenediazonium,                            3228               100        OP8  ..............  ..............  .........
 tetrachlorozincate (2:1).....................................
2,5-Diethoxy-4-morpholinobenzenediazonium zinc chloride.......              3236            67-100        OP7             +35             +40  .........
2,5-Diethoxy-4-morpholinobenzenediazonium zinc chloride.......              3236                66        OP7             +40             +45  .........
2,5-Diethoxy-4-morpholinobenzenediazonium tetrafluoroborate...              3236               100        OP7             +30             +35  .........
2,5-Diethoxy-4-(phenylsulphonyl)benzenediazonium zinc chloride              3236                67        OP7             +40             +45  .........
2,5-Diethoxy-4-(4-morpholinyl)-benzenediazonium sulphate......              3226               100        OP7  ..............  ..............  .........
Diethylene glycol bis(allyl carbonate) +                                    3237       >=88 + <=12        OP8             -10               0  .........
 Diisopropylperoxydicarbonate.................................
2,5-Dimethoxy-4-(4-methylphenylsulphony)benzenediazonium zinc               3236                79        OP7             +40             +45  .........
 chloride.....................................................
4-Dimethylamino-6-(2-dimethylaminoethoxy)toluene-2-diazonium                3236               100        OP7             +40             +45  .........
 zinc chloride................................................
4-(Dimethylamino)-benzenediazonium trichlorozincate (-1)......              3228               100        OP8  ..............  ..............  .........
N,N'-Dinitroso-N, N'-dimethyl-terephthalamide, as a paste.....              3224                72        OP6  ..............  ..............  .........
N,N'-Dinitrosopentamethylenetetramine.........................              3224                82        OP6  ..............  ..............          2
Diphenyloxide-4,4'-disulphohydrazide..........................              3226               100        OP7  ..............  ..............  .........
Diphenyloxide-4,4'-disulphonylhydrazide.......................              3226               100        OP7  ..............  ..............  .........
4-Dipropylaminobenzenediazonium zinc chloride.................              3226               100        OP7  ..............  ..............  .........
2-(N,N-Ethoxycarbonylphenylamino)-3-methoxy-4-(N-methyl-N-                  3236             63-92        OP7             +40             +45  .........
 cyclohexylamino)benzenediazonium zinc chloride...............
2-(N,N-Ethoxycarbonylphenylamino)-3-methoxy-4-(N-methyl-N-                  3236                62        OP7             +35             +40  .........
 cyclohexylamino)benzenediazonium zinc chloride...............
N-Formyl-2-(nitromethylene)-1,3-perhydrothiazine..............              3236               100        OP7             +45             +50  .........
2-(2-Hydroxyethoxy)-1-(pyrrolidin-1-yl)benzene-4-diazonium                  3236               100        OP7             +45             +50  .........
 zinc chloride................................................
3-(2-Hydroxyethoxy)-4-(pyrrolidin-1-yl)benzenediazonium zinc                3236               100        OP7             +40             +45  .........
 chloride.....................................................
2-(N,N-Methylaminoethylcarbonyl)-4-(3,4-dimethyl-                           3236                96        OP7             +45             +50  .........
 phenylsulphonyl)benzene diazonium zinc chloride..............
4-Methylbenzenesulphonylhydrazide.............................              3226               100        OP7  ..............  ..............  .........
3-Methyl-4-(pyrrolidin-1-yl)benzenediazonium tetrafluoroborate              3234                95        OP6             +45             +50  .........
4-Nitrosophenol...............................................              3236               100        OP7             +35             +40  .........
Phosphorothioic acid, O-[(cyanophenyl methylene) azanyl] O,O-               3227             82-91        OP8  ..............  ..............          5
 diethyl ester................................................                          (Z isomer)
Self-reactive liquid, sample..................................              3223  ................        OP2  ..............  ..............          3
Self-reactive liquid, sample, temperature control.............              3233  ................        OP2  ..............  ..............          3
Self-reactive solid, sample...................................              3224  ................        OP2  ..............  ..............          3
Self-reactive solid, sample, temperature control..............              3234  ................        OP2  ..............  ..............          3
Sodium 2-diazo-1-naphthol-4-sulphonate........................              3226               100        OP7  ..............  ..............  .........
Sodium 2-diazo-1-naphthol-5-sulphonate........................              3226               100        OP7  ..............  ..............  .........
Tetramine palladium (II) nitrate..............................              3234               100        OP6             +30             +35  .........
--------------------------------------------------------------------------------------------------------------------------------------------------------
Notes:
1. The emergency and control temperatures must be determined in accordance with Sec.   173.21(f).
2. With a compatible diluent having a boiling point of not less than 150 [deg]C.

3. Samples may only be offered for transportation under the provisions of paragraph (c)(3) of this section.
4. This entry applies to mixtures of esters of 2-diazo-1-naphthol-4-sulphonic acid and 2-diazo-1-naphthol-5-sulphonic acid.
5. This entry applies to the technical mixture in n-butanol within the specified concentration limits of the (Z) isomer.

    (c) New self-reactive materials, formulations and samples. (1)
Except as provided for samples in paragraph (c)(3) or (4) of this
section, no person may offer, accept for transportation, or transport a
self-reactive material which is not identified by technical name in the
Self-Reactive Materials Table of this section, or a formulation of one
or more self-reactive materials which are identified by technical name
in the table, unless the self-reactive material is assigned a generic
type and shipping description and is approved by the Associate
Administrator under the provisions of Sec.  173.124(a)(2)(iii).
    (2) Except as provided by an approval issued under Sec.
173.124(a)(2)(iii), intermediate bulk and bulk packagings are not
authorized.
    (3) Samples of new self-reactive materials or new formulations of
self-reactive materials identified in the Self-Reactive Materials Table
in paragraph (b) of this section, for which complete test data are not
available, and which are to be transported for further testing or
product evaluation, may be assigned an appropriate shipping description
for Self-reactive materials Type C, packaged and offered for
transportation under the following conditions:
    (i) Data available to the person offering the material for
transportation must indicate that the sample would pose a level of
hazard no greater than that of a self-reactive material Type B and that
the control temperature, if any, is sufficiently low to prevent any
dangerous decomposition and sufficiently high to prevent any dangerous
phase separation;
    (ii) The sample must be packaged in accordance with packing method
OP2;
    (iii) Packages of the self-reactive material may be offered for
transportation and transported in a quantity not to exceed 10 kg (22
pounds) per transport vehicle; and
    (iv) One of the following shipping descriptions must be assigned:
    (A) Self-reactive, liquid, type C, 4.1, UN 3223.
    (B) Self-reactive, solid, type C, 4.1, UN 3224.
    (C) Self-reactive, liquid, type C, temperature controlled, 4.1, UN
3233.
    (D) Self-reactive, solid, type C, temperature controlled, 4.1, UN
3234.
    (4) Samples of organic substances carrying functional groups listed
in tables A6.1 and/or A6.2 in Annex 6 (Screening Procedures) of the UN
Manual of Tests and Criteria (IBR, see Sec.  171.7 of this subchapter)
may be transported under UN 3224 or UN 3223, as applicable, of Division
4.1 provided that:
    (i) The samples do not contain any:
    (A) Known explosives;
    (B) Substances showing explosive effects in testing;
    (C) Compounds designed with the view of producing a practical
explosive or pyrotechnic effect;
    (D) Components consisting of synthetic precursors of intentional
explosives;
    (ii) For mixtures, complexes or salts of inorganic oxidizing
substances of Division 5.1 with organic material(s), the concentration
of the inorganic oxidizing substance is:
    (A) Less than 15 percent, by mass, if assigned to Packing Group I
or II; or
    (B) Less than 30 percent, by mass, if assigned to Packing Group
III;
    (iii) Available data does not allow a more precise classification;
    (iv) The sample is not packed together with other goods;
    (v) Must be packaged as follows:
    (A) The quantity per individual inner cavity does not exceed 0.01 g
for solids or 0.01 mL for liquids and the maximum net quantity per
outer packaging does not exceed 20 g for solids or 20 mL for liquids,
or in the case of mixed packing the sum of grams and mL does not exceed
20:
    (1) The samples are carried in microtiter plates or multi-titer
plates made of plastics, glass, porcelain or stoneware as an inner
packaging;
    (2) only combination packaging with outer packaging comprising
boxes (4A, 4B, 4N, 4C1, 4C2, 4D, 4F, 4G, 4H1 and 4H2) are permitted; or
    (B) The maximum content of each inner packaging does not exceed 1 g
for solids or 1 mL for liquids and the maximum net quantity per outer
packaging does not exceed 56 g for solids or 56 mL for liquids, or in
the case of mixed packing the sum of grams and mL does not exceed 56:
    (1) The individual substance is contained in an inner packaging of
glass or plastics of maximum capacity of 30 mL placed in an expandable
polyethylene foam matrix of at least 130 mm thickness having a density
of 18  1 g/L;
    (2) Within the foam carrier, inner packagings are segregated from
each other by a minimum distance of 40 mm and from the wall of the
outer packaging by a minimum distance of 70 mm. The package may contain
up to two layers of such foam matrices, each carrying up to twenty-
eight inner packagings;
    (3) The outer packaging consists only of corrugated fiberboard
boxes (4G) having minimum dimensions of 60 cm (length) by 40.5 cm
(width) by 30 cm (height) and minimum wall thickness of 1.3 cm.
    (vi) When dry ice or liquid nitrogen is optionally used as a
coolant for quality control measures, all applicable requirements of
this subchapter must be met. Interior supports must be provided to
secure the inner packagings in the original position after the ice or
dry ice has dissipated. If ice is used, the outside packaging or
overpack must be leakproof. If dry ice is used, the requirements in
Sec.  173.217 must be met. The inner and outer packagings must maintain
their integrity at the temperature of the refrigerant used as well as
the temperatures and the pressures which could result if refrigeration
were lost.

0
31. In Sec.  173.225, revise the table to paragraph (c), the heading of
the table to paragraph (d), paragraph (e), paragraph (g) introductory
text, and the heading to the table to paragraph (g) to read as follows:

Sec.  173.225  Packaging requirements and other provisions for organic
peroxides.

* * * * *
    (c) * * *
    (8) * * *

                                                     Table to Paragraph (c): Organic Peroxide Table
--------------------------------------------------------------------------------------------------------------------------------------------------------
                                                                       Diluent (mass %)                                  Temperature ( [deg]C)
         Technical name              ID No.      Concentration  ------------------------------   Water       Packing    -----------------------   Notes
                                                    (mass %)         A         B         I      (mass %)      method      Control   Emergency
--------------------------------------------------------------------------------------------------------------------------------------------------------
(1)                              (2)                        (3)      (4a)      (4b)      (4c)        (5)  (6)                (7a)         (7b)       (8)
--------------------------------------------------------------------------------------------------------------------------------------------------------
Acetyl acetone peroxide........  UN3105                    <=42      >=48  ........  ........        >=8  OP7            ........  ...........         2
Acetyl acetone peroxide [as a    UN3106                    <=32  ........  ........  ........  .........  OP7            ........  ...........        21
 paste].

Acetyl cyclohexanesulfonyl       UN3112                    <=82  ........  ........  ........       >=12  OP4                 -10            0  ........
 peroxide.
Acetyl cyclohexanesulfonyl       UN3115                    <=32  ........      >=68  ........  .........  OP7                 -10            0  ........
 peroxide.
tert-Amyl hydroperoxide........  UN3107                    <=88       >=6  ........  ........        >=6  OP8            ........  ...........  ........
tert-Amyl peroxyacetate........  UN3105                    <=62      >=38  ........  ........  .........  OP7            ........  ...........  ........
tert-Amyl peroxybenzoate.......  UN3103                   <=100  ........  ........  ........  .........  OP5            ........  ...........  ........
tert-Amyl peroxy-2-              UN3115                   <=100  ........  ........  ........  .........  OP7                  20           25  ........
 ethylhexanoate.
tert-Amyl peroxy-2-ethylhexyl    UN3105                   <=100  ........  ........  ........  .........  OP7            ........  ...........  ........
 carbonate.
tert-Amyl peroxy isopropyl       UN3103                    <=77      >=23  ........  ........  .........  OP5            ........  ...........  ........
 carbonate.
tert-Amyl peroxyneodecanoate...  UN3115                    <=77  ........      >=23  ........  .........  OP7                   0           10  ........
tert-Amyl peroxyneodecanoate...  UN3119                    <=47      >=53  ........  ........  .........  OP8                   0           10  ........
tert-Amyl peroxypivalate.......  UN3113                    <=77  ........      >=23  ........  .........  OP5                  10           15  ........
tert-Amyl peroxypivalate.......  UN3119                    <=32      >=68  ........  ........  .........  OP8                  10           15  ........
tert-Amyl peroxy-3,5,5-          UN3105                   <=100  ........  ........  ........  .........  OP7            ........  ...........  ........
 trimethylhexanoate.
tert-Butyl cumyl peroxide......  UN3109                 >42-100  ........  ........  ........  .........  OP8            ........  ...........         9
tert-Butyl cumyl peroxide......  UN3108                    <=52  ........  ........      >=48  .........  OP8            ........  ...........         9
n-Butyl-4,4-di-(tert-            UN3103                 >52-100  ........  ........  ........  .........  OP5            ........  ...........  ........
 butylperoxy)valerate.
n-Butyl-4,4-di-(tert-            UN3108                    <=52  ........  ........      >=48  .........  OP8            ........  ...........  ........
 butylperoxy)valerate.
tert-Butyl hydroperoxide.......  UN3103                  >79-90  ........  ........  ........       >=10  OP5            ........  ...........        13
tert-Butyl hydroperoxide.......  UN3105                    <=80      >=20  ........  ........  .........  OP7            ........  ...........     4, 13
tert-Butyl hydroperoxide.......  UN3107                    <=79  ........  ........  ........        >14  OP8            ........  ...........    13, 16
tert-Butyl hydroperoxide.......  UN3109                    <=72  ........  ........  ........       >=28  OP8            ........  ...........        13
tert-Butyl hydroperoxide [and]   UN3103                <82 + >9  ........  ........  ........        >=7  OP5            ........  ...........        13
 Di-tert-butylperoxide.
tert-Butyl monoperoxymaleate...  UN3102                 >52-100  ........  ........  ........  .........  OP5            ........  ...........  ........
tert-Butyl monoperoxymaleate...  UN3103                    <=52      >=48  ........  ........  .........  OP6            ........  ...........  ........
tert-Butyl monoperoxymaleate...  UN3108                    <=52  ........  ........      >=48  .........  OP8            ........  ...........  ........
tert-Butyl monoperoxymaleate     UN3108                    <=52  ........  ........  ........  .........  OP8            ........  ...........  ........
 [as a paste].
tert-Butyl peroxyacetate.......  UN3101                  >52-77      >=23  ........  ........  .........  OP5            ........  ...........  ........
tert-Butyl peroxyacetate.......  UN3103                  >32-52      >=48  ........  ........  .........  OP6            ........  ...........  ........
tert-Butyl peroxyacetate.......  UN3109                    <=32  ........      >=68  ........  .........  OP8            ........  ...........  ........
tert-Butyl peroxybenzoate......  UN3103                 >77-100  ........  ........  ........  .........  OP5            ........  ...........  ........
tert-Butyl peroxybenzoate......  UN3105                  >52-77      >=23  ........  ........  .........  OP7            ........  ...........         1
tert-Butyl peroxybenzoate......  UN3106                    <=52  ........  ........      >=48  .........  OP7            ........  ...........  ........
tert-Butyl peroxybenzoate......  UN3109                    <=32      >=68  ........  ........  .........  OP8            ........  ...........  ........
tert-Butyl peroxybutyl fumarate  UN3105                    <=52      >=48  ........  ........  .........  OP7            ........  ...........  ........
tert-Butyl peroxycrotonate.....  UN3105                    <=77      >=23  ........  ........  .........  OP7            ........  ...........  ........
tert-Butyl peroxydiethylacetate  UN3113                   <=100  ........  ........  ........  .........  OP5                  20           25  ........
tert-Butyl peroxy-2-             UN3113                 >52-100  ........  ........  ........  .........  OP6                  20           25  ........
 ethylhexanoate.
tert-Butyl peroxy-2-             UN3117                  >32-52  ........      >=48  ........  .........  OP8                  30           35  ........
 ethylhexanoate.
tert-Butyl peroxy-2-             UN3118                    <=52  ........  ........      >=48  .........  OP8                  20           25  ........
 ethylhexanoate.
tert-Butyl peroxy-2-             UN3119                    <=32  ........      >=68  ........  .........  OP8                  40           45  ........
 ethylhexanoate.
tert-Butyl peroxy-2-             UN3106             <=12 + <=14      >=14  ........      >=60  .........  OP7            ........  ...........  ........
 ethylhexanoate [and] 2,2-di-
 (tert-Butylperoxy)butane.
tert-Butyl peroxy-2-             UN3115             <=31 + <=36  ........      >=33  ........  .........  OP7                  35           40  ........
 ethylhexanoate [and] 2,2-di-
 (tert-Butylperoxy)butane.
tert-Butyl peroxy-2-             UN3105                   <=100  ........  ........  ........  .........  OP7            ........  ...........  ........
 ethylhexylcarbonate.
tert-Butyl peroxyisobutyrate...  UN3111                  >52-77  ........      >=23  ........  .........  OP5                  15           20  ........
tert-Butyl peroxyisobutyrate...  UN3115                    <=52  ........      >=48  ........  .........  OP7                  15           20  ........
tert-Butylperoxy                 UN3103                    <=77      >=23  ........  ........  .........  OP5            ........  ...........  ........
 isopropylcarbonate.
1-(2-tert-Butylperoxy            UN3105                    <=77      >=23  ........  ........  .........  OP7            ........  ...........  ........
 isopropyl)-3-
 isopropenylbenzene.
1-(2-tert-Butylperoxy            UN3108                    <=42  ........  ........      >=58  .........  OP8            ........  ...........  ........
 isopropyl)-3-
 isopropenylbenzene.
tert-Butyl peroxy-2-             UN3103                   <=100  ........  ........  ........  .........  OP5            ........  ...........  ........
 methylbenzoate.
tert-Butyl peroxyneodecanoate..  UN3115                 >77-100  ........  ........  ........  .........  OP7                  -5            5  ........
tert-Butyl peroxyneodecanoate..  UN3115                    <=77  ........      >=23  ........  .........  OP7                   0           10  ........
tert-Butyl peroxyneodecanoate    UN3119                    <=52  ........  ........  ........  .........  OP8                   0           10  ........
 [as a stable dispersion in
 water].
tert-Butyl peroxyneodecanoate    UN3118                    <=42  ........  ........  ........  .........  OP8                   0           10  ........
 [as a stable dispersion in
 water (frozen)].
tert-Butyl peroxyneodecanoate..  UN3119                    <=32      >=68  ........  ........  .........  OP8                   0           10  ........
tert-Butyl peroxyneoheptanoate.  UN3115                    <=77      >=23  ........  ........  .........  OP7                   0           10  ........
tert-Butyl peroxyneoheptanoate   UN3117                    <=42  ........  ........  ........  .........  OP8                   0           10  ........
 [as a stable dispersion in
 water].
tert-Butyl peroxypivalate......  UN3113                  >67-77      >=23  ........  ........  .........  OP5                   0           10  ........
tert-Butyl peroxypivalate......  UN3115                  >27-67  ........      >=33  ........  .........  OP7                   0           10  ........
tert-Butyl peroxypivalate......  UN3119                    <=27  ........      >=73  ........  .........  OP8                  30           35  ........
tert-Butylperoxy                 UN3106                   <=100  ........  ........  ........  .........  OP7            ........  ...........  ........
 stearylcarbonate.
tert-Butyl peroxy-3,5,5-         UN3105                 >37-100  ........  ........  ........  .........  OP7            ........  ...........  ........
 trimethylhexanoate.
tert-Butyl peroxy-3,5,5-         UN3106                    <=42  ........  ........      >=58  .........  OP7            ........  ...........  ........
 trimethlyhexanoate.
tert-Butyl peroxy-3,5,5-         UN3109                    <=37  ........      >=63  ........  .........  OP8            ........  ...........  ........
 trimethylhexanoate.
3-Chloroperoxybenzoic acid.....  UN3102                  >57-86  ........  ........      >=14  .........  OP1            ........  ...........  ........

3-Chloroperoxybenzoic acid.....  UN3106                    <=57  ........  ........       >=3       >=40  OP7            ........  ...........  ........
3-Chloroperoxybenzoic acid.....  UN3106                    <=77  ........  ........       >=6       >=17  OP7            ........  ...........  ........
Cumyl hydroperoxide............  UN3107                  >90-98      <=10  ........  ........  .........  OP8            ........  ...........        13
Cumyl hydroperoxide............  UN3109                    <=90      >=10  ........  ........  .........  OP8            ........  ...........    13, 15
Cumyl peroxyneodecanoate.......  UN3115                    <=87      >=13  ........  ........  .........  OP7                 -10            0  ........
Cumyl peroxyneodecanoate.......  UN3115                    <=77  ........      >=23  ........  .........  OP7                 -10            0  ........
Cumyl peroxyneodecanoate [as a   UN3119                    <=52  ........  ........  ........  .........  OP8                 -10            0  ........
 stable dispersion in water].
Cumyl peroxyneoheptanoate......  UN3115                    <=77      >=23  ........  ........  .........  OP7                 -10            0  ........
Cumyl peroxypivalate...........  UN3115                    <=77  ........      >=23  ........  .........  OP7                  -5            5  ........
Cyclohexanone peroxide(s)......  UN3104                    <=91  ........  ........  ........        >=9  OP6            ........  ...........        13
Cyclohexanone peroxide(s)......  UN3105                    <=72      >=28  ........  ........  .........  OP7            ........  ...........         5
Cyclohexanone peroxide(s) [as a  UN3106                    <=72  ........  ........  ........  .........  OP7            ........  ...........     5, 21
 paste].
Cyclohexanone peroxide(s)......  Exempt                    <=32  ........       >68  ........  .........  Exempt         ........  ...........        29
Diacetone alcohol peroxides....  UN3115                    <=57  ........      >=26  ........        >=8  OP7                  40           45         5
Diacetyl peroxide..............  UN3115                    <=27  ........      >=73  ........  .........  OP7                  20           25      8,13
Di-tert-amyl peroxide..........  UN3107                   <=100  ........  ........  ........  .........  OP8            ........  ...........  ........
([3R- (3R, 5aS, 6S, 8aS, 9R,     UN3106                   <=100  ........  ........  ........  .........  OP7            ........  ...........  ........
 10R, 12S, 12aR**)]-Decahydro-
 10-methoxy-3, 6, 9-trimethyl-
 3, 12-epoxy-12H-pyrano [4, 3-
 j]-1, 2-benzodioxepin).
2,2-Di-(tert-amylperoxy)-butane  UN3105                    <=57      >=43  ........  ........  .........  OP7            ........  ...........  ........
1,1-Di-(tert-                    UN3103                    <=82      >=18  ........  ........  .........  OP6            ........  ...........  ........
 amylperoxy)cyclohexane.
Dibenzoyl peroxide.............  UN3102                 >52-100  ........  ........      <=48  .........  OP2            ........  ...........         3
Dibenzoyl peroxide.............  UN3102                  >77-94  ........  ........  ........        >=6  OP4            ........  ...........         3
Dibenzoyl peroxide.............  UN3104                    <=77  ........  ........  ........       >=23  OP6            ........  ...........  ........
Dibenzoyl peroxide.............  UN3106                    <=62  ........  ........      >=28       >=10  OP7            ........  ...........  ........
Dibenzoyl peroxide [as a paste]  UN3106                  >52-62  ........  ........  ........  .........  OP7            ........  ...........        21
Dibenzoyl peroxide.............  UN3106                  >35-52  ........  ........      >=48  .........  OP7            ........  ...........  ........
Dibenzoyl peroxide.............  UN3107                  >36-42      >=18  ........  ........       <=40  OP8            ........  ...........  ........
Dibenzoyl peroxide [as a paste]  UN3108                  <=56.5  ........  ........  ........       >=15  OP8            ........  ...........  ........
Dibenzoyl peroxide [as a paste]  UN3108                    <=52  ........  ........  ........  .........  OP8            ........  ...........        21
Dibenzoyl peroxide [as a stable  UN3109                    <=42  ........  ........  ........  .........  OP8            ........  ...........  ........
 dispersion in water].
Dibenzoyl peroxide.............  Exempt                    <=35  ........  ........      >=65  .........  Exempt         ........  ...........        29
Di-(4-tert-                      UN3114                   <=100  ........  ........  ........  .........  OP6                  30           35  ........
 butylcyclohexyl)peroxydicarbon
 ate.
Di-(4-tert-                      UN3119                    <=42  ........  ........  ........  .........  OP8                  30           35  ........
 butylcyclohexyl)peroxydicarbon
 ate [as a stable dispersion in
 water].
Di-(4-tert-                      UN3116                    <=42  ........  ........  ........  .........  OP7                  35           40  ........
 butylcyclohexyl)peroxydicarbon
 ate [as a paste].
Di-tert-butyl peroxide.........  UN3107                 >52-100  ........  ........  ........  .........  OP8            ........  ...........  ........
Di-tert-butyl peroxide.........  UN3109                    <=52  ........      >=48  ........  .........  OP8            ........  ...........        24
Di-tert-butyl peroxyazelate....  UN3105                    <=52      >=48  ........  ........  .........  OP7            ........  ...........  ........
2,2-Di-(tert-butylperoxy)butane  UN3103                    <=52      >=48  ........  ........  .........  OP6            ........  ...........  ........
1,6-Di-(tert-                    UN3103                    <=72      >=28  ........  ........  .........  OP5            ........  ...........  ........
 butylperoxycarbonyloxy)hexane.
1,1-Di-(tert-                    UN3101                 >80-100  ........  ........  ........  .........  OP5            ........  ...........  ........
 butylperoxy)cyclohexane.
1,1-Di-(tert-                    UN3103                  >52-80      >=20  ........  ........  .........  OP5            ........  ...........  ........
 butylperoxy)cyclohexane.
1,1-Di-(tert-butylperoxy)-       UN3103                    <=72  ........      >=28  ........  .........  OP5            ........  ...........        30
 cyclohexane.
1,1-Di-(tert-                    UN3105                  >42-52      >=48  ........  ........  .........  OP7            ........  ...........  ........
 butylperoxy)cyclohexane.
1,1-Di-(tert-                    UN3106                    <=42      >=13  ........      >=45  .........  OP7            ........  ...........  ........
 butylperoxy)cyclohexane.
1,1-Di-(tert-                    UN3107                    <=27      >=25  ........  ........  .........  OP8            ........  ...........        22
 butylperoxy)cyclohexane.
1,1-Di-(tert-                    UN3109                    <=42      >=58  ........  ........  .........  OP8            ........  ...........  ........
 butylperoxy)cyclohexane.
1,1-Di-(tert-Butylperoxy)        UN3109                    <=37      >=63  ........  ........  .........  OP8            ........  ...........  ........
 cyclohexane.
1,1-Di-(tert-                    UN3109                    <=25      >=25      >=50  ........  .........  OP8            ........  ...........  ........
 butylperoxy)cyclohexane.
1,1-Di-(tert-                    UN3109                    <=13      >=13      >=74  ........  .........  OP8            ........  ...........  ........
 butylperoxy)cyclohexane.
1,1-Di-(tert-                    UN3105             <=43 + <=16      >=41  ........  ........  .........  OP7            ........  ...........  ........
 butylperoxy)cyclohexane + tert-
 Butyl peroxy-2-ethylhexanoate.
Di-n-butyl peroxydicarbonate...  UN3115                  >27-52  ........      >=48  ........  .........  OP7                 -15           -5  ........
Di-n-butyl peroxydicarbonate...  UN3117                    <=27  ........      >=73  ........  .........  OP8                 -10            0  ........
Di-n-butyl peroxydicarbonate     UN3118                    <=42  ........  ........  ........  .........  OP8                 -15           -5  ........
 [as a stable dispersion in
 water (frozen)].
Di-sec-butyl peroxydicarbonate.  UN3113                 >52-100  ........  ........  ........  .........  OP4                 -20          -10         6