[Federal Register Volume 81, Number 174 (Thursday, September 8, 2016)]
[Notices]
[Page 62192]
[FR Doc No: 2016-21519]

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SECURITIES AND EXCHANGE COMMISSION

[Release No. 34-78755; File No. SR-NYSEArca-2016-103]

Self-Regulatory Organizations; NYSE Arca Inc.; Notice of
Designation of a Longer Period for Commission Action on Proposed Rule
Change Amending Rules 2.17(c) and 2.23(i) To Extend the Time Within
Which OTP Holders and OTP Firms Must File a Uniform Termination Notice
for Securities Industry Registration (``U5'')

September 1, 2016.
    On July 14, 2016, NYSE Arca, Inc. filed with the Securities and
Exchange Commission (``Commission''), pursuant to Section 19(b)(1) of
the Securities Exchange Act of 1934 (``Act'') \1\ and Rule 19b-4
thereunder,\2\ a proposed rule change to amend Rules 2.17(c) and
2.23(i) to extend the time within which OTP Holders and OTP Firms must
file a U5. The proposed rule change was published for comment in the
Federal Register on July 27, 2016.\3\ The Commission received no
comments in response to the proposal. In response to a related proposed
rule change,\4\ however, the Commission received a comment letter and a
response to those comments from the proposing exchange.\5\
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    \1\ 15 U.S.C. 78s(b)(1).
    \2\ 17 CFR 240.19b-4.
    \3\ See Securities Exchange Act Release No. 78381 (July 21,
2016), 81 FR 49286.
    \4\ See Securities Exchange Act Release No. 78198 (June 30,
2016), 81 FR 44363.
    \5\ See letter from Judith Shaw, President, North American
Securities Administrators Association, Inc., to Brent J. Fields,
Secretary, Securities and Exchange Commission, dated August 3, 2016
(``NASAA Letter'') and letter from Elizabeth K. King, General
Counsel and Corporate Secretary, New York Stock Exchange to Brent J.
Fields, Secretary, SEC, dated August 12, 2016.
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    Section 19(b)(2) of the Act \6\ provides that within 45 days of the
publication of notice of the filing of a proposed rule change, or
within such longer period up to 90 days as the Commission may designate
if it finds such longer period to be appropriate and publishes its
reasons for so finding, or as to which the self-regulatory organization
consents, the Commission shall either approve the proposed rule change,
disapprove the proposed rule change, or institute proceedings to
determine whether the proposed rule change should be disapproved. The
45th day after publication of the notice for this proposed rule change
is September 10, 2016. The Commission is extending this 45-day time
period.
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    \6\ 15 U.S.C. 78s(b)(2).
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    The Commission finds it appropriate to designate a longer period
within which to take action on the proposed rule change so that it has
sufficient time to consider the issues raised in the NASAA Letter, as
well as those in the response from NYSE MKT LLC., in connection with
the proposed rule change. Accordingly, the Commission, pursuant to
Section 19(b)(2) of the Act,\7\ designates October 25, 2016, as the
date by which the Commission shall either approve or disapprove, or
institute proceedings to determine whether to disapprove, the proposed
rule change (File No. SR-NYSEArca-2016-103).
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    \7\ Id.

    For the Commission, by the Division of Trading and Markets,
pursuant to delegated authority.\8\
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    \8\ 17 CFR 200.30-3(a)(31).
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Robert W. Errett,
Deputy Secretary.
[FR Doc. 2016-21519 Filed 9-7-16; 8:45 am]
 BILLING CODE 8011-01-P


calibration check procedures on field analytical balances each day
that they are used. You must use National Institute of Standards and
Technology (NIST)-traceable weights at a mass approximately equal to
the weight of the sample plus container you will weigh.
    9.5 Glassware. Use class A volumetric glassware for titrations,
or calibrate your equipment against NIST-traceable glassware.
    9.6 Laboratory Analytical Balance Calibration Check. Check the
calibration of your laboratory analytical balance each day that you
weigh CPM samples. You must use NIST Class S weights at a mass
approximately equal to the weight of the sample plus container you
will weigh.
    9.7 Laboratory Reagent Blanks. You should run blanks of water,
acetone, and hexane used for field recovery and sample analysis.
Analyze at least one sample (150 ml minimum) of each lot of reagents
that you plan to use for sample recovery and analysis before you
begin testing. These blanks are not required by the test method, but
running blanks before field use is advisable to verify low blank
concentrations, thereby reducing the potential for a high field
blank on test samples.
    9.8 Field Reagent Blanks. You should run at least one field
reagent blank of water, acetone, and hexane you use for field
recovery. These blanks are not required by the test method, but
running independent field reagent blanks is advisable to verify that
low blank concentrations were maintained during field solvent use
and demonstrate that reagents have not been contaminated during
field tests.
    9.9 Field Train Proof Blank. If you are not baking glassware as
specified in Section 8.4, you must recover a minimum of one field
train proof blank for the sampling train used for testing each new
source category at a single facility. You must assemble the sampling
train as it will be used for testing. You must recover the field
train proof blank samples as described in Section <IP_ADDRESS> and
<IP_ADDRESS>.
    9.10 Field Train Recovery Blank. You must recover a minimum of
one field train blank for each source category tested at the
facility. You must recover the field train blank after the first or
second run of the test. You must assemble the sampling train as it
will be used for testing. Prior to the purge, you must add 100 ml of
water to the first impinger and record this data on Figure 4. You
must purge the assembled train as

described in Sections <IP_ADDRESS> and <IP_ADDRESS>. You must recover field
train blank samples as described in Section 8.5.4. From the field
sample weight, you will subtract the condensable particulate mass
you determine with this blank train or 0.002 g (2.0 mg), whichever
is less.

10.0 Calibration and Standardization

    Maintain a field log notebook of all condensable particulate
sampling and analysis calibrations. Include copies of the relevant
portions of the calibration and field logs in the final test report.
    10.1 Thermocouple Calibration. You must calibrate the
thermocouples using the procedures described in Section 10.3.1 of
Method 2 of appendix A-1 to part 60 or Alternative Method 2,
Thermocouple Calibration (ALT-011) (http://www.epa.gov/ttn/emc).
Calibrate each temperature sensor at a minimum of three points over
the anticipated range of use against a NIST-traceable thermometer.
Alternatively, a reference thermocouple and potentiometer calibrated
against NIST standards can be used.
    10.2 Ammonium Hydroxide. The 0.1 N NH4OH used for
titrations in this method is made as follows: Add 7 ml of
concentrated (14.8 M) NH4OH to l liter of water.
Standardize against standardized 0.1 N H2SO4,
and calculate the exact normality using a procedure parallel to that
described in Section 10.5 of Method 6 of appendix A-4 to 40 CFR part
60. Alternatively, purchase 0.1 N NH4OH that has been
standardized against a NIST reference material. Record the normality
on the CPM Work Table (see Figure 6 of Section 18).

11.0 Analytical Procedures

    11.1 Analytical Data Sheets. (a) Record the filterable
particulate field data on the appropriate (i.e., Method 5, 17, or
201A) analytical data sheets. Alternatively, data may be recorded
electronically using software applications such as the Electronic
Reporting Tool available at http://www.epa.gov/ttn/chief/ert/ert_tool.html. Record the condensable particulate data on the CPM Work
Table (see Figure 6 of Section 18).
    (b) Measure the liquid in all containers either volumetrically
to  1 ml or gravimetrically to  0.5 g.
Confirm on the filterable particulate analytical data sheet whether
leakage occurred during transport. If a noticeable amount of leakage
has occurred, either void the sample or use methods (subject to the
approval of the Administrator) to correct the final results.
    11.2 Condensable PM Analysis. See the flow chart in Figure 7 of
Section 18 for the steps to process and combine fractions from the
CPM train.
    11.2.1 Container 3, CPM Filter Sample. If the sample
was collected by Method 17 or Method 201A with a stack temperature
below 30 [deg]C (85 [deg]F) and the filter can be brought to a
constant weight, transfer the filter and any loose PM from the
sample container to a tared glass weighing dish. (See Section 3.0
for a definition of constant weight.) Desiccate the sample for 24
hours in a desiccator containing anhydrous calcium sulfate. Weigh to
a constant weigh and report the results to the nearest 0.1 mg. If
the filter cannot be brought to constant weight using this
procedure, you must follow the extraction and weighing procedures in
this section. (See Section 3.0 for a definition of constant weight.)
Extract the filter recovered from the low-temperature portion of the
train, and combine the extracts with the organic and inorganic
fractions resulting from the aqueous impinger sample recovery in
Containers 1 and 2, respectively. Extract the CPM filter as follows:
    <IP_ADDRESS> Extract the water soluble (aqueous or inorganic) CPM
from the CPM filter by folding the filter in quarters and placing it
into a 50-ml extraction tube. Add sufficient deionized, ultra-
filtered water to cover the filter (e.g., 10 ml of water). Place the
extractor tube into a sonication bath and extract the water-soluble
material for a minimum of two minutes. Combine the aqueous extract
with the contents of Container 1. Repeat this extraction
step twice for a total of three extractions.
    <IP_ADDRESS> Extract the organic soluble CPM from the CPM filter by
adding sufficient hexane to cover the filter (e.g., 10 ml of
hexane). Place the extractor tube into a sonication bath and extract
the organic soluble material for a minimum of two minutes. Combine
the organic extract with the contents of Container 2.
Repeat this extraction step twice for a total of three extractions.
    11.2.2 CPM Container 1, Aqueous Liquid Impinger
Contents. Analyze the water soluble CPM in Container 1 as described
in this section. Place the contents of Container 1 into a
separatory funnel. Add approximately 30 ml of hexane to the funnel,
mix well, and drain off the lower organic phase. Repeat this
procedure twice with 30 ml of hexane each time combining the organic
phase from each extraction. Each time, leave a small amount of the
organic/hexane phase in the separatory funnel, ensuring that no
water is collected in the organic phase. This extraction should
yield about 90 ml of organic extract. Combine the organic extract
from Container 1 with the organic train rinse in Container
2.
    <IP_ADDRESS> Determine the inorganic fraction weight. Transfer the
aqueous fraction from the extraction to a clean 500-ml or smaller
beaker. Evaporate to no less than 10 ml liquid on a hot plate or in
the oven at 105 [deg]C and allow to dry at room temperature (not to
exceed 30 [deg]C (85 [deg]F)). You must ensure that water and
volatile acids have completely evaporated before neutralizing
nonvolatile acids in the sample. Following evaporation, desiccate
the residue for 24 hours in a desiccator containing anhydrous
calcium sulfate. Weigh at intervals of at least six hours to a
constant weight. (See Section 3.0 for a definition of Constant
weight.) Report results to the nearest 0.1 mg on the CPM Work Table
(see Figure 6 of Section 18) and proceed directly to Section 11.2.3.
If the residue can not be weighed to constant weight, redissolve the
residue in 100 ml of deionized distilled ultra-filtered water that
contains 1 ppmw (1 mg/L) residual mass or less and continue to
Section <IP_ADDRESS>.
    <IP_ADDRESS> Use titration to neutralize acid in the sample and
remove water of hydration. If used, calibrate the pH meter with the
neutral and acid buffer solutions. Then titrate the sample with 0.1N
NH4OH to a pH of 7.0, as indicated by the pH meter or
colorimetric indicator. Record the volume of titrant used on the CPM
Work Table (see Figure 6 of Section 18).
    <IP_ADDRESS> Using a hot plate or an oven at 105 [deg]C, evaporate
the aqueous phase to approximately 10 ml. Quantitatively transfer
the beaker contents to a clean, 50-ml pre-tared weighing tin and
evaporate to dryness at room temperature (not to exceed 30 [deg]C
(85 [deg]F)) and pressure in a laboratory hood. Following
evaporation, desiccate the residue for 24 hours in a desiccator
containing anhydrous calcium sulfate. Weigh at intervals of at least
six hours to a constant weight. (See Section 3.0 for a definition of
Constant weight.) Report results to the nearest 0.1 mg on the CPM
Work Table (see Figure 6 of Section 18).
    <IP_ADDRESS> Calculate the correction factor to subtract the
NH4\+\ retained in the sample using Equation 1 in Section
12.
    11.2.3 CPM Container 2, Organic Fraction Weight
Determination. Analyze the organic soluble CPM in Container
2 as described in this section. Place the organic phase in
a clean glass beaker. Evaporate the organic extract at room
temperature (not to exceed 30 [deg]C (85 [deg]F)) and pressure in a
laboratory hood to not less than 10 ml. Quantitatively transfer the
beaker contents to a clean 50-ml pre-tared weighing tin and
evaporate to dryness at room temperature (not to exceed 30 [deg]C
(85 [deg]F)) and pressure in a laboratory hood. Following
evaporation, desiccate the organic fraction for 24 hours in a
desiccator containing anhydrous calcium sulfate. Weigh at intervals
of at least six hours to a constant weight (i.e., less than or equal
to 0.5 mg change from previous weighing), and report results to the
nearest 0.1 mg on the CPM Work Table (see Figure 6 of Section 18).
    11.2.4 CPM Container 4, Cold Impinger Water. If the
amount of water has not been determined in the field, note the level
of liquid in the container, and confirm on the filterable
particulate analytical data sheet whether leakage occurred during
transport. If a noticeable amount of leakage has occurred, either
void the sample or use methods (subject to the approval of the
Administrator) to correct the final results. Measure the liquid in
Container 4 either volumetrically to  1 ml or
gravimetrically to  0.5 g, and record the volume or
weight on the filterable particulate analytical data sheet of the
filterable PM test method.
    11.2.5 CPM Container 5, Silica Gel Absorbent. Weigh the
spent silica gel (or silica gel plus impinger) to the nearest 0.5 g
using a balance. This step may be conducted in the field. Record the
weight on the filterable particulate analytical data sheet of the
filterable PM test method.
    11.2.6 Container 6, Acetone Field Reagent Blank. Use
150 ml of acetone from the blank container used for this analysis.
Transfer 150 ml of the acetone to a clean 250-ml beaker. Evaporate
the acetone at room temperature (not to exceed 30 [deg]C (85
[deg]F)) and pressure in a laboratory hood to approximately 10 ml.
Quantitatively transfer

the beaker contents to a clean 50-ml pre-tared weighing tin, and
evaporate to dryness at room temperature (not to exceed 30 [deg]C
(85 [deg]F)) and pressure in a laboratory hood. Following
evaporation, desiccate the residue for 24 hours in a desiccator
containing anhydrous calcium sulfate. Weigh at intervals of at least
six hours to a constant weight (i.e., less than or equal to 0.5 mg
change from previous weighing), and report results to the nearest
0.1 mg on Figure 4 of Section 19.
    11.2.7 Water Field Reagent Blank, Container 7. Use 150
ml of the water from the blank container for this analysis. Transfer
the water to a clean 250-ml beaker, and evaporate to approximately
10 ml liquid in the oven at 105 [deg]C. Quantitatively transfer the
beaker contents to a clean 50 ml pre-tared weighing tin and
evaporate to dryness at room temperature (not to exceed 30 [deg]C
(85 [deg]F)) and pressure in a laboratory hood. Following
evaporation, desiccate the residue for 24 hours in a desiccator
containing anhydrous calcium sulfate. Weigh at intervals of at least
six hours to a constant weight (i.e., less than or equal to 0.5 mg
change from previous weighing) and report results to the nearest 0.1
mg on Figure 4 of Section 18.
    11.2.8 Hexane Field Reagent Blank, Container 8. Use 150
ml of hexane from the blank container for this analysis. Transfer
150 ml of the hexane to a clean 250-ml beaker. Evaporate the hexane
at room temperature (not to exceed 30 [deg]C (85 [deg]F)) and
pressure in a laboratory hood to approximately 10 ml. Quantitatively
transfer the beaker contents to a clean 50-ml pre-tared weighing tin
and evaporate to dryness at room temperature (not to exceed 30
[deg]C (85 [deg]F)) and pressure in a laboratory hood. Following
evaporation, desiccate the residue for 24 hours in a desiccator
containing anhydrous calcium sulfate. Weigh at intervals of at least
six hours to a constant weight (i.e., less than or equal to 0.5 mg
change from previous weighing), and report results to the nearest
0.1 mg on Figure 4 of Section 18.

12.0 Calculations and Data Analysis

    12.1 Nomenclature. Report results in International System of
Units (SI units) unless the regulatory authority for testing
specifies English units. The following nomenclature is used.

    [Delta]H@ = Pressure drop across orifice at flow rate
of 0.75 SCFM at standard conditions, inches of water column (Note:
Specific to each orifice and meter box).
17.03 = mg/milliequivalents for ammonium ion.
ACFM = Actual cubic feet per minute.
Ccpm = Concentration of the condensable PM in the stack
gas, dry basis, corrected to standard conditions, milligrams/dry
standard cubic foot.
mc = Mass of the NH4\+\ added to sample to
form ammonium sulfate, mg.
mcpm = Mass of the total condensable PM, mg.
mfb = Mass of total CPM in field train recovery blank,
mg.
mg = Milligrams.
mg/L = Milligrams per liter.
mi = Mass of inorganic CPM, mg.
mib = Mass of inorganic CPM in field train recovery
blank, mg.
mo = Mass of organic CPM, mg.
mob = Mass of organic CPM in field train blank, mg.
mr = Mass of dried sample from inorganic fraction, mg.
N = Normality of ammonium hydroxide titrant.
ppmv = Parts per million by volume.
ppmw = Parts per million by weight.
Vm(std) = Volume of gas sample measured by the dry gas
meter, corrected to standard conditions, dry standard cubic meter
(dscm) or dry standard cubic foot (dscf) as defined in Equation 5-1
of Method 5.
Vt = Volume of NH4OH titrant, ml.
Vp = Volume of water added during train purge.

    12.2 Calculations. Use the following equations to complete the
calculations required in this test method. Enter the appropriate
results from these calculations on the CPM Work Table (see Figure 6
of Section 18).
    12.2.1 Mass of ammonia correction. Correction for ammonia added
during titration of 100 ml aqueous CPM sample. This calculation
assumes no waters of hydration.
[GRAPHIC] [TIFF OMITTED] TR21DE10.058

    12.2.2 Mass of the Field Train Recovery Blank (mg). Per Section
9.10, the mass of the field train recovery blank, mfb,
shall not exceed 2.0 mg.
[GRAPHIC] [TIFF OMITTED] TR21DE10.059

    12.2.3 Mass of Inorganic CPM (mg).
    [GRAPHIC] [TIFF OMITTED] TR21DE10.060

    12.2.4 Total Mass of CPM (mg).
    [GRAPHIC] [TIFF OMITTED] TR21DE10.061

    12.2.5 Concentration of CPM (mg/dscf).
    [GRAPHIC] [TIFF OMITTED] TR21DE10.062

    12.3 Emissions Test Report. You must prepare a test report
following the guidance in EPA Guidance Document 043 (Preparation and
Review of Test Reports. December 1998).

13.0 Method Performance

    An EPA field evaluation of the revised Method 202 showed the
following precision in the results: approximately 4 mg for total
CPM, approximately 0.5 mg for organic CPM, and approximately 3.5 mg
for inorganic CPM.

14.0 Pollution Prevention

    [Reserved]

15.0 Waste Management

    Solvent and water are evaporated in a laboratory hood during
analysis. No liquid waste is generated in the performance of this
method. Organic solvents used to clean sampling equipment should be
managed as RCRA organic waste.

16.0 Alternative Procedures

    Alternative Method 2, Thermocouple Calibration (ALT-011) for the
thermocouple calibration can be found at http://www.epa.gov/ttn/emc/approalt.html.

17.0 References

    (1) Commonwealth of Pennsylvania, Department of Environmental
Resources. 1960. Chapter 139, Sampling and Testing (Title 25, Rules
and Regulations, part I, Department of Environmental Resources,
Subpart C, Protection of Natural Resources, Article III, Air
Resources). January 8, 1960.
    (2) DeWees, W.D. and K.C. Steinsberger. 1989. ``Method
Development and Evaluation of Draft Protocol for Measurement of
Condensable Particulate Emissions.'' Draft Report. November 17,
1989.
    (3) DeWees, W.D., K.C. Steinsberger, G.M. Plummer, L.T. Lay,
G.D. McAlister, and R.T. Shigehara. 1989. ``Laboratory and Field
Evaluation of EPA Method 5 Impinger Catch for Measuring Condensable
Matter from Stationary Sources.'' Paper presented at the 1989 EPA/
AWMA International Symposium on Measurement of Toxic and Related Air
Pollutants. Raleigh, North Carolina. May 1-5, 1989.
    (4) Electric Power Research Institute (EPRI). 2008. ``Laboratory
Comparison of Methods to Sample and Analyze Condensable PM.'' EPRI
Agreement EP-P24373/C11811 Condensable Particulate Methods: EPRI
Collaboration with EPA, October 2008.
    (5) Nothstein, Greg. Masters Thesis. University of Washington.
Department of Environmental Health. Seattle, Washington.
    (6) Richards, J., T. Holder, and D. Goshaw. 2005. ``Optimized
Method 202 Sampling Train to Minimize the Biases Associated with
Method 202 Measurement of Condensable PM Emissions.'' Paper
presented at Air & Waste Management Association Hazardous Waste
Combustion Specialty Conference. St. Louis, Missouri. November 2-3,
2005.
    (7) Texas Air Control Board, Laboratory Division. 1976.
``Determination of Particulate in Stack Gases Containing Sulfuric
Acid and/or Sulfur Dioxide.'' Laboratory Methods for Determination
of Air Pollutants. Modified December 3, 1976.
    (8) Puget Sound Air Pollution Control Agency, Engineering
Division. 1983. ``Particulate Source Test Procedures Adopted by
Puget Sound Air Pollution Control Agency Board of Directors.''
Seattle, Washington. August 11, 1983.
    (9) U.S. Environmental Protection Agency, Federal Reference
Methods 1 through 5 and Method 17, 40 CFR 60, appendix A-1 through
A-3 and A-6.
    (10) U.S. Environmental Protection Agency. 2008. ``Evaluation
and Improvement of Condensable PM Measurement,'' EPA Contract No.
EP-D-07-097, Work Assignment 2-03, October 2008.
    (11) U.S. Environmental Protection Agency. 2005. ``Laboratory
Evaluation of Method 202 to Determine Fate of SO2 in
Impinger Water,'' EPA Contract No. 68-D-02-061, Work Assignment 3-
14, September 30, 2005.
    (12) U.S. Environmental Protection Agency. 2010. Field valuation
of an Improved Method for Sampling and Analysis of Filterable and
Condensable Particulate Matter. Office of Air Quality Planning and
Standards, Sector Policy and Program Division Monitoring Policy
Group. Research Triangle Park, NC 27711.
    (13) Wisconsin Department of Natural Resources. 1988. Air
Management Operations Handbook, Revision 3. January 11, 1988.

18.0 Tables, Diagrams, Flowcharts, and Validation Data

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      Figure 4--Field Train Recovery Blank Condensable Particulate
                              Calculations
------------------------------------------------------------------------

------------------------------------------------------------------------
    Field Train Recovery Blank Condensable Particulate Calculations
------------------------------------------------------------------------
Plant                                            .......................
------------------------------------------------------------------------
Date                                             .......................
------------------------------------------------------------------------
Blank No.                                        .......................
------------------------------------------------------------------------
CPM Filter No.                                   .......................
------------------------------------------------------------------------

Water volume added to purge train (Vp).........  ml
------------------------------------------------------------------------
          Field Reagent Blank Mass\a\            .......................
------------------------------------------------------------------------
Water (Section 11.2.7).........................  mg
------------------------------------------------------------------------
Acetone (Section 11.2.6).......................  mg
------------------------------------------------------------------------
Hexane (Section 11.2.8)........................  mg
------------------------------------------------------------------------
        Field Train Recovery Blank Mass          .......................
------------------------------------------------------------------------
Mass of Organic CPM (mob) (Section 11.2.3).....  mg
------------------------------------------------------------------------
Mass of Inorganic CPM (mib) (Equation 3).......  mg
------------------------------------------------------------------------
Mass of the Field Train Recovery Blank (not to   mg
 exceed 2.0 mg) (Equation 2).
------------------------------------------------------------------------
\a\ Field reagent blanks are optional and intended to provide the
  testing contractor with information they can use to implement
  corrective actions, if necessary, to reduce the residual mass
  contribution from reagents used in the field. Field reagent blanks are
  not used to correct the CPM measurement results.

     Figure 5--Other Field Train Sample Condensable Particulate Data
------------------------------------------------------------------------

------------------------------------------------------------------------
         Other Field Train Sample Condensable Particulate Data
------------------------------------------------------------------------
Plant                                            .......................
------------------------------------------------------------------------
Date                                             .......................
------------------------------------------------------------------------
Run No.                                          .......................
------------------------------------------------------------------------
CPM Filter No.                                   .......................
------------------------------------------------------------------------
Water volume added to purge train (max 50 ml)    ml
 (Vp).
------------------------------------------------------------------------
Date                                             .......................
------------------------------------------------------------------------
Run No.                                          .......................
------------------------------------------------------------------------
CPM Filter No.                                   .......................
------------------------------------------------------------------------
Water volume added to purge train (max 50 ml)    ml
 (Vp).
------------------------------------------------------------------------
Date                                             .......................
------------------------------------------------------------------------
Run No.                                          .......................
------------------------------------------------------------------------
CPM Filter No.                                   .......................
------------------------------------------------------------------------
Water volume added to purge train (max 50 ml)    ml
 (Vp).
------------------------------------------------------------------------

                        Figure 6--CPM Work Table
------------------------------------------------------------------------

------------------------------------------------------------------------
Calculations for Recovery of Condensable PM (CPM)
------------------------------------------------------------------------
Plant
------------------------------------------------------------------------
Date
------------------------------------------------------------------------
Run No.
------------------------------------------------------------------------
Sample Preparation--CPM Containers No. 1
 and 2 (Section 11.1):
------------------------------------------------------------------------
    Was significant volume of water lost  ..................
     during transport? Yes or No
                                         --------------------
    If Yes, measure the volume received   ..................
    Estimate the volume lost during       ..................  ml
     transport
Plant
------------------------------------------------------------------------
Date
------------------------------------------------------------------------
Run No.
------------------------------------------------------------------------
    Was significant volume of organic     ..................
     rinse lost during transport? Yes or
     No
------------------------------------------------------------------------
    If Yes, measure the volume received   ..................
    Estimate the volume lost during       ..................  ml
     transport.
For Titration:
    Normality of NH4OH (N) (Section       ..................  N
     10.2)
    Volume of titrant (Vt) (Section       ..................  ml
     <IP_ADDRESS>)
    Mass of NH4 added (mc) (Equation 1)   ..................  mg
For CPM Blank Weights:
    Inorganic Field Train Recovery Blank  ..................  mg
     Mass(mib) (Section 9.9)
    Organic Field Train Recovery Blank    ..................  mg
     Mass (mob) (Section 9.9)
    Mass of Field Train Recovery Blank    ..................  mg
     (Mfb) (max. 2 mg) (Equation 2)
For CPM Train Weights:
    Mass of Organic CPM (mo) (Section     ..................  mg
     11.2.3)
    Mass of Inorganic CPM (mi) (Equation  ..................  mg
     3)
    Total CPM Mass (mcpm) (Equation 4)    ..................  mg
------------------------------------------------------------------------

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[FR Doc. 2010-30847 Filed 12-20-10; 8:45 am]
BILLING CODE 6560-50-C