15 m
                                0 h  14 m  57 s
12/19/2011 12:09:04 PM
15-02
Blood
12/19/2011 11:54:07 AM
                                       30 m
                                0 h  30 m  33 s
12/19/2011 12:24:40 PM
15-02
Blood
12/19/2011 11:54:07 AM
                                     1 h
                                0 h  59 m  55 s
12/19/2011 12:54:02 PM
15-02
Blood
12/19/2011 11:54:07 AM
                                     2 h
                                1 h  59 m  52 s
12/19/2011 1:53:59 PM
15-02
Blood
12/19/2011 11:54:07 AM
                                     4 h
                                4 h  0 m  59 s
12/19/2011 3:55:06 PM
15-02
Blood
12/19/2011 11:54:07 AM
                                     6 h
                                6 h  0 m  22 s
12/19/2011 5:54:29 PM
15-03
Blood
12/19/2011 11:57:14 AM
                                        5 m
                                0 h  5 m  10 s
12/19/2011 12:02:24 PM
15-03
Blood
12/19/2011 11:57:14 AM
                                       10 m
0 h  10 m  48 s
12/19/2011 12:08:02 PM
15-03
Blood
12/19/2011 11:57:14 AM
                                       15 m
0 h  14 m  50 s
12/19/2011 12:12:04 PM
15-03
Blood
12/19/2011 11:57:14 AM
                                       30 m
0 h  29 m  32 s
12/19/2011 12:26:46 PM
15-03
Blood
12/19/2011 11:57:14 AM
                                     1 h
0 h  59 m  50 s
12/19/2011 12:57:04 PM
15-03
Blood
12/19/2011 11:57:14 AM
                                     2 h
2 h  0 m  40 s
12/19/2011 1:57:54 PM
15-03
Blood
12/19/2011 11:57:14 AM
                                     4 h
4 h  0 m  27 s
12/19/2011 3:57:41 PM
15-03
Blood
12/19/2011 11:57:14 AM
                                     6 h
6 h  0 m  5 s
12/19/2011 5:57:19 PM
15-04
Blood
12/19/2011 12:00:17 PM
                                        5 m
0 h  6 m  4 s
12/19/2011 12:06:21 PM

                                    Subject
                                    Sample
                                   Dose Time
                                   Nominal
                                     Time
                                 Elapsed Time
                                  (hh:mm:ss)
                                 Capture Time

15-04
Blood
12/19/2011 12:00:17 PM
                                     1 h
1 h  0 m  1 s
12/19/2011 1:00:18 PM
15-04
Blood
12/19/2011 12:00:17 PM
                                     2 h
2 h  0 m  15 s
12/19/2011 2:00:32 PM
15-04
Blood
12/19/2011 12:00:17 PM
                                     4 h
3 h  59 m  36 s
12/19/2011 3:59:53 PM
15-04
Blood
12/19/2011 12:00:17 PM
                                     6 h
5 h  59 m  56 s
12/19/2011 6:00:13 PM
16-01
Blood
12/19/2011 12:03:10 PM
                                        5 m
0 h  4 m  58 s
12/19/2011 12:08:08 PM
16-01
Blood
12/19/2011 12:03:10 PM
                                       10 m
0 h  9 m  57 s
12/19/2011 12:13:07 PM
16-01
Blood
12/19/2011 12:03:10 PM
                                       15 m
0 h  18 m  2 s
12/19/2011 12:21:12 PM
16-01
Blood
12/19/2011 12:03:10 PM
                                       30 m
0 h  29 m  49 s
12/19/2011 12:32:59 PM
16-01
Blood
12/19/2011 12:03:10 PM
                                     1 h
1 h  0 m  2 s
12/19/2011 1:03:12 PM
16-01
Blood
12/19/2011 12:03:10 PM
                                     2 h
2 h  0 m  33 s
12/19/2011 2:03:43 PM
16-01
Blood
12/19/2011 12:03:10 PM
                                     4 h
4 h  0 m  22 s
12/19/2011 4:03:32 PM
16-01
Blood
12/19/2011 12:03:10 PM
                                     6 h
6 h  0 m  43 s
12/19/2011 6:03:53 PM
16-02
Blood
12/19/2011 12:06:19 PM
                                        5 m
0 h  5 m  16 s
12/19/2011 12:11:35 PM
16-02
Blood
12/19/2011 12:06:19 PM
                                       10 m
0 h  10 m  9 s
12/19/2011 12:16:28 PM
16-02
Blood
12/19/2011 12:06:19 PM
                                       15 m
0 h  16 m  31 s
12/19/2011 12:22:50 PM
16-02
Blood
12/19/2011 12:06:19 PM
                                       30 m
0 h  29 m  45 s
12/19/2011 12:36:04 PM
16-02
Blood
12/19/2011 12:06:19 PM
                                     1 h
                                0 h  59 m  44 s
12/19/2011 1:06:03 PM
16-02
Blood
12/19/2011 12:06:19 PM
                                     2 h
                                1 h  59 m  52 s
12/19/2011 2:06:11 PM
16-02
Blood
12/19/2011 12:06:19 PM
                                     4 h
                                 4 h  0 m  4 s
12/19/2011 4:06:23 PM
16-02
Blood
12/19/2011 12:06:19 PM
                                     6 h
                                6 h  0 m  47 s
12/19/2011 6:07:06 PM
16-03
Blood
12/19/2011 12:09:02 PM
                                        5 m
                                0 h  11 m  45 s
12/19/2011 12:20:47 PM
16-03
Blood
12/19/2011 12:09:02 PM
                                       10 m
                                0 h  11 m  9 s
12/19/2011 12:20:11 PM
16-03
Blood
12/19/2011 12:09:02 PM
                                       15 m
                                0 h  16 m  9 s
12/19/2011 12:25:11 PM
16-03
Blood
12/19/2011 12:09:02 PM
                                       30 m
                                0 h  29 m  54 s
12/19/2011 12:38:56 PM
16-03
Blood
12/19/2011 12:09:02 PM
                                     1 h
                                 1 h  0 m  2 s
12/19/2011 1:09:04 PM
16-03
Blood
12/19/2011 12:09:02 PM
                                     2 h
                                2 h  0 m  14 s
12/19/2011 2:09:16 PM
16-03
Blood
12/19/2011 12:09:02 PM
                                     4 h
                                 4 h  1 m  6 s
12/19/2011 4:10:08 PM
16-03
Blood
12/19/2011 12:09:02 PM
                                     6 h
                                6 h  0 m  29 s
12/19/2011 6:09:31 PM
16-04
Blood
12/19/2011 12:12:08 PM
                                        5 m
                                0 h  5 m  51 s
12/19/2011 12:17:59 PM
16-04
Blood
12/19/2011 12:12:08 PM
                                       10 m
                                0 h  10 m  9 s
12/19/2011 12:22:17 PM
16-04
Blood
12/19/2011 12:12:08 PM
                                       15 m
                                0 h  15 m  0 s
12/19/2011 12:27:08 PM
16-04
Blood
12/19/2011 12:12:08 PM
                                       30 m
                                0 h  29 m  55 s
12/19/2011 12:42:03 PM
16-04
Blood
12/19/2011 12:12:08 PM
                                     1 h
                                0 h  59 m  54 s
12/19/2011 1:12:02 PM
16-04
Blood
12/19/2011 12:12:08 PM
                                     2 h
1 h  59 m  45 s
12/19/2011 2:11:53 PM
16-04
Blood
12/19/2011 12:12:08 PM
                                     4 h
3 h  59 m  47 s
12/19/2011 4:11:55 PM
16-04
Blood
12/19/2011 12:12:08 PM
                                     6 h
6 h  0 m  27 s
12/19/2011 6:12:35 PM
15-05
Blood
12/19/2011 11:35:33 AM
                                     6.25 h
6 h  14 m  33 s
12/19/2011 5:50:06 PM
15-05
Blood
12/19/2011 11:35:33 AM
                                     6.50 h
6 h  29 m  33 s
12/19/2011 6:05:06 PM
15-05
Blood
12/19/2011 11:35:33 AM
                                     7 h
7 h  0 m  8 s
12/19/2011 6:35:41 PM
15-05
Blood
12/19/2011 11:35:33 AM
                                     7.33 h
7 h  20 m  22 s
12/19/2011 6:55:55 PM
15-05
Blood
12/19/2011 11:35:33 AM
                                     8 h
7 h  59 m  43 s
12/19/2011 7:35:16 PM

                                    Subject
                                    Sample
                                   Dose Time
                                   Nominal
                                     Time
                                 Elapsed Time
                                  (hh:mm:ss)
                                 Capture Time

15-06
Blood
12/19/2011 11:37:06 AM
                                     6.25 h
6 h  15 m  9 s
12/19/2011 5:52:15 PM
15-06
Blood
12/19/2011 11:37:06 AM
                                     6.50 h
6 h  29 m  34 s
12/19/2011 6:06:40 PM
15-06
Blood
12/19/2011 11:37:06 AM
                                     7 h
6 h  59 m  56 s
12/19/2011 6:37:02 PM
15-06
Blood
12/19/2011 11:37:06 AM
                                     7.33 h
7 h  20 m  9 s
12/19/2011 6:57:15 PM
15-06
Blood
12/19/2011 11:37:06 AM
                                     8 h
8 h  0 m  28 s
12/19/2011 7:37:34 PM
15-06
Blood
12/19/2011 11:37:06 AM
                                    10 h
10 h  0 m  7 s
12/19/2011 9:37:13 PM
15-06
Blood
12/19/2011 11:37:06 AM
                                    16 h
16 h  0 m  46 s
12/20/2011 3:37:52 AM
15-07
Blood
12/19/2011 11:38:56 AM
                                     6.25 h
6 h  15 m  27 s
12/19/2011 5:54:23 PM
15-07
Blood
12/19/2011 11:38:56 AM
                                     6.50 h
6 h  29 m  53 s
12/19/2011 6:08:49 PM
15-07
Blood
12/19/2011 11:38:56 AM
                                     7 h
7 h  0 m  9 s
12/19/2011 6:39:05 PM
15-07
Blood
12/19/2011 11:38:56 AM
                                     7.33 h
7 h  20 m  0 s
12/19/2011 6:58:56 PM
15-07
Blood
12/19/2011 11:38:56 AM
                                     8 h
8 h  0 m  10 s
12/19/2011 7:39:06 PM
15-07
Blood
12/19/2011 11:38:56 AM
                                    10 h
10 h  0 m  20 s
12/19/2011 9:39:16 PM
15-07
Blood
12/19/2011 11:38:56 AM
                                    16 h
16 h  0 m  45 s
12/20/2011 3:39:41 AM
15-08
Blood
12/19/2011 11:41:19 AM
                                     6.25 h
6 h  14 m  52 s
12/19/2011 5:56:11 PM
15-08
Blood
12/19/2011 11:41:19 AM
                                     6.50 h
6 h  29 m  24 s
12/19/2011 6:10:43 PM
15-08
Blood
12/19/2011 11:41:19 AM
                                     7 h
                                6 h  59 m  57 s
12/19/2011 6:41:16 PM
15-08
Blood
12/19/2011 11:41:19 AM
                                     7.33 h
                                7 h  19 m  37 s
12/19/2011 7:00:56 PM
15-08
Blood
12/19/2011 11:41:19 AM
                                     8 h
                                 8 h  0 m  2 s
12/19/2011 7:41:21 PM
15-08
Blood
12/19/2011 11:41:19 AM
                                    10 h
                                9 h  59 m  53 s
12/19/2011 9:41:12 PM
15-08
Blood
12/19/2011 11:41:19 AM
                                    16 h
                                16 h  0 m  56 s
12/20/2011 3:42:15 AM
16-05
Blood
12/19/2011 11:43:48 AM
                                     6.25 h
                                6 h  14 m  12 s
12/19/2011 5:58:00 PM
16-05
Blood
12/19/2011 11:43:48 AM
                                     6.50 h
                                6 h  28 m  27 s
12/19/2011 6:12:15 PM
16-05
Blood
12/19/2011 11:43:48 AM
                                     7 h
                                6 h  59 m  46 s
12/19/2011 6:43:34 PM
16-05
Blood
12/19/2011 11:43:48 AM
                                     7.33 h
                                7 h  18 m  59 s
12/19/2011 7:02:47 PM
16-05
Blood
12/19/2011 11:43:48 AM
                                     8 h
                                7 h  59 m  23 s
12/19/2011 7:43:11 PM
16-05
Blood
12/19/2011 11:43:48 AM
                                    10 h
                                9 h  59 m  30 s
12/19/2011 9:43:18 PM
16-05
Blood
12/19/2011 11:43:48 AM
                                    16 h
                                16 h  0 m  23 s
12/20/2011 3:44:11 AM
16-06
Blood
12/19/2011 11:45:16 AM
                                     6.25 h
                                6 h  14 m  57 s
12/19/2011 6:00:13 PM
16-06
Blood
12/19/2011 11:45:16 AM
                                     6.50 h
                                6 h  29 m  28 s
12/19/2011 6:14:44 PM
16-06
Blood
12/19/2011 11:45:16 AM
                                     7 h
                                6 h  59 m  46 s
12/19/2011 6:45:02 PM
16-06
Blood
12/19/2011 11:45:16 AM
                                     7.33 h
                                7 h  20 m  12 s
12/19/2011 7:05:28 PM
16-06
Blood
12/19/2011 11:45:16 AM
                                     8 h
                                7 h  59 m  35 s
12/19/2011 7:44:51 PM
16-06
Blood
12/19/2011 11:45:16 AM
                                    10 h
9 h  59 m  52 s
12/19/2011 9:45:08 PM
16-06
Blood
12/19/2011 11:45:16 AM
                                    16 h
16 h  2 m  14 s
12/20/2011 3:47:30 AM
16-07
Blood
12/19/2011 11:47:32 AM
                                     6.25 h
6 h  14 m  10 s
12/19/2011 6:01:42 PM
16-07
Blood
12/19/2011 11:47:32 AM
                                     6.50 h
6 h  29 m  29 s
12/19/2011 6:17:01 PM
16-07
Blood
12/19/2011 11:47:32 AM
                                     7 h
7 h  0 m  1 s
12/19/2011 6:47:33 PM
16-07
Blood
12/19/2011 11:47:32 AM
                                     7.33 h
7 h  19 m  55 s
12/19/2011 7:07:27 PM
16-07
Blood
12/19/2011 11:47:32 AM
                                     8 h
7 h  59 m  13 s
12/19/2011 7:46:45 PM
16-07
Blood
12/19/2011 11:47:32 AM
                                    10 h
9 h  59 m  24 s
12/19/2011 9:46:56 PM

                                    Subject
                                    Sample
                                   Dose Time
                                   Nominal
                                     Time
                                 Elapsed Time
                                  (hh:mm:ss)
                                 Capture Time

16-07
Blood
12/19/2011 11:47:32 AM
                                    16 h
16 h  1 m  40 s
12/20/2011 3:49:12 AM
16-08
Blood
12/19/2011 11:49:11 AM
                                     6.25 h
6 h  14 m  54 s
12/19/2011 6:04:05 PM
16-08
Blood
12/19/2011 11:49:11 AM
                                     6.50 h
6 h  30 m  10 s
12/19/2011 6:19:21 PM
16-08
Blood
12/19/2011 11:49:11 AM
                                     7 h
7 h  1 m  13 s
12/19/2011 6:50:24 PM
16-08
Blood
12/19/2011 11:49:11 AM
                                     7.33 h
7 h  20 m  12 s
12/19/2011 7:09:23 PM
16-08
Blood
12/19/2011 11:49:11 AM
                                     8 h
7 h  59 m  22 s
12/19/2011 7:48:33 PM
16-08
Blood
12/19/2011 11:49:11 AM
                                    10 h
9 h  59 m  37 s
12/19/2011 9:48:48 PM
16-08
Blood
12/19/2011 11:49:11 AM
                                    16 h
16 h  1 m  56 s
12/20/2011 3:51:07 AM
15-05
Blood
12/19/2011 11:35:33 AM
                                    24 h
23 h  59 m  29 s
12/20/2011 11:35:02 AM
15-06
Blood
12/19/2011 11:37:06 AM
                                    24 h
23 h  59 m  51 s
12/20/2011 11:36:57 AM
15-07
Blood
12/19/2011 11:38:56 AM
                                    24 h
24 h  0 m  5 s
12/20/2011 11:39:01 AM
15-08
Blood
12/19/2011 11:41:19 AM
                                    24 h
23 h  59 m  47 s
12/20/2011 11:41:06 AM
16-05
Blood
12/19/2011 11:43:48 AM
                                    24 h
23 h  59 m  46 s
12/20/2011 11:43:34 AM
16-06
Blood
12/19/2011 11:45:16 AM
                                    24 h
24 h  0 m  5 s
12/20/2011 11:45:21 AM
16-07
Blood
12/19/2011 11:47:32 AM
                                    24 h
23 h  59 m  38 s
12/20/2011 11:47:10 AM
16-08
Blood
12/19/2011 11:49:11 AM
                                    24 h
23 h  59 m  53 s
12/20/2011 11:49:04 AM

Table 61.  Blood Sample Weights for Groups 11 and 12.
                                    Subject
                                    Sample
                                     Time
                                    Pot wt.
                                  Sample  wt.
                                   Corrected
                                 Sample Weight
11-01
Blood
                                    Predose
                                   11.0163 g
                                   11.1947 g
                                   0.1784 g
11-01
Blood
                                      5 m
                                   10.9842 g
                                   11.1527 g
                                   0.1685 g
11-01
Blood
                                     10 m
                                   11.0020 g
                                   11.1755 g
                                   0.1735 g
11-01
Blood
                                     15 m
                                   10.9977 g
                                   11.1549 g
                                   0.1572 g
11-01
Blood
                                     30 m
                                   11.0298 g
                                   11.2181 g
                                   0.1883 g
11-01
Blood
                                      1 h
                                   11.0138 g
                                   11.1791 g
                                   0.1653 g
11-01
Blood
                                      2 h
                                   10.9949 g
                                   11.1732 g
                                   0.1783 g
11-01
Blood
                                      4 h
                                   11.0351 g
                                   11.2162 g
                                   0.1811 g
11-01
Blood
                                      6 h
                                   11.0308 g
                                   11.2164 g
                                   0.1856 g
11-02
Blood
                                    Predose
                                   10.9996 g
                                   11.1292 g
                                   0.1296 g
11-02
Blood
                                      5 m
                                   11.0514 g
                                   11.2366 g
                                   0.1852 g
11-02
Blood
                                     10 m
                                   11.0354 g
                                   11.1586 g
                                   0.1232 g
11-02
Blood
                                     15 m
                                   11.0317 g
                                   11.2385 g
                                   0.2068 g
11-02
Blood
                                     30 m
                                   11.0001 g
                                   11.1270 g
                                   0.1269 g
11-02
Blood
                                      1 h
                                   11.0584 g
                                   11.2824 g
                                   0.2240 g
11-02
Blood
                                      2 h
                                   11.0305 g
                                   11.2015 g
                                   0.1710 g
11-02
Blood
                                      4 h
                                   11.0287 g
                                   11.2007 g
                                   0.1720 g
11-02
Blood
                                      6 h
                                   10.9426 g
                                   11.1051 g
                                   0.1625 g
11-03
Blood
                                    Predose
                                   11.0501 g
                                   11.2457 g
                                   0.1956 g
11-03
Blood
                                      5 m
                                   11.0083 g
                                   11.1616 g
                                   0.1533 g
11-03
Blood
                                     10 m
                                   11.0539 g
                                   11.2226 g
                                   0.1687 g
11-03
Blood
                                     15 m
                                   11.0466 g
                                   11.2499 g
                                   0.2033 g
11-03
Blood
                                     30 m
                                   11.0364 g
                                   11.2659 g
                                   0.2295 g
11-03
Blood
                                      1 h
                                   11.0472 g
                                   11.2773 g
                                   0.2301 g
11-03
Blood
                                      2 h
                                   11.0563 g
                                   11.2134 g
                                   0.1571 g
11-03
Blood
                                      4 h
                                   11.0220 g
                                   11.1912 g
                                   0.1692 g
11-03
Blood
                                      6 h
                                   11.1244 g
                                   11.2936 g
                                   0.1692 g
11-04
Blood
                                    Predose
                                   11.0297 g
                                   11.1966 g
                                   0.1669 g
11-04
Blood
                                      5 m
                                   11.0472 g
                                   11.1957 g
                                   0.1485 g
11-04
Blood
                                     10 m
                                   11.0457 g
                                   11.2194 g
                                   0.1737 g
11-04
Blood
                                     15 m
                                   11.0511 g
                                   11.2479 g
                                   0.1968 g
11-04
Blood
                                     30 m
                                   11.0834 g
                                   11.2562 g
                                   0.1728 g
11-04
Blood
                                      1 h
                                   11.0229 g
                                   11.2145 g
                                   0.1916 g
11-04
Blood
                                      2 h
                                   11.0174 g
                                   11.1677 g
                                   0.1503 g
11-04
Blood
                                      4 h
                                   11.1094 g
                                   11.3113 g
                                   0.2019 g
11-04
Blood
                                      6 h
                                   11.0730 g
                                   11.2618 g
                                   0.1888 g
11-05
Blood
                                    Predose
                                   11.0416 g
                                   11.1959 g
                                   0.1543 g
11-05
Blood
                                    6.25 h
                                   11.0558 g
                                   11.2186 g
                                   0.1628 g
11-05
Blood
                                    6.50 h
                                   11.0421 g
                                   11.1625 g
                                   0.1204 g
11-05
Blood
                                      7 h
                                   11.0031 g
                                   11.1821 g
                                   0.1790 g

                                    Subject
                                    Sample
                                     Time
                                    Pot wt.
                                  Sample  wt.
                                   Corrected
                                 Sample Weight
11-05
Blood
                                    7.33 h
                                   11.0852 g
                                   11.2209 g
                                   0.1357 g
11-05
Blood
                                      8 h
                                   11.0411 g
                                   11.1631 g
                                   0.1220 g
11-05
Blood
                                     10 h
                                   11.0464 g
                                   11.1947 g
                                   0.1483 g
11-05
Blood
                                     16 h
                                   11.0472 g
                                   11.2187 g
                                   0.1715 g
11-05
Blood
                                     24 h
                                   11.0343 g
                                   11.2055 g
                                   0.1712 g
11-06
Blood
                                    Predose
                                   10.9889 g
                                   11.1618 g
                                   0.1729 g
11-06
Blood
                                    6.25 h
                                   11.0038 g
                                   11.1456 g
                                   0.1418 g
11-06
Blood
                                    6.50 h
                                   11.0446 g
                                   11.2597 g
                                   0.2151 g
11-06
Blood
                                      7 h
                                   11.0780 g
                                   11.2587 g
                                   0.1807 g
11-06
Blood
                                    7.33 h
                                   10.9929 g
                                   11.1610 g
                                   0.1681 g
11-06
Blood
                                      8 h
                                   11.0504 g
                                   11.2406 g
                                   0.1902 g
11-06
Blood
                                     10 h
                                   11.1003 g
                                   11.2086 g
                                   0.1083 g
11-06
Blood
                                     16 h
                                   11.0461 g
                                   11.2661 g
                                   0.2200 g
11-06
Blood
                                     24 h
                                   11.0226 g
                                   11.2655 g
                                   0.2429 g
11-07
Blood
                                    Predose
                                   11.0546 g
                                   11.2385 g
                                   0.1839 g
11-07
Blood
                                    6.25 h
                                   11.0311 g
                                   11.1968 g
                                   0.1657 g
11-07
Blood
                                    6.50 h
                                   11.0619 g
                                   11.2500 g
                                   0.1881 g
11-07
Blood
                                      7 h
                                   11.0699 g
                                   11.3246 g
                                   0.2547 g
11-07
Blood
                                    7.33 h
                                   11.0419 g
                                   11.2184 g
                                   0.1765 g
11-07
Blood
                                      8 h
                                   11.0322 g
                                   11.2056 g
                                   0.1734 g
11-07
Blood
                                     10 h
                                   10.9813 g
                                   11.1347 g
                                   0.1534 g
11-07
Blood
                                     16 h
                                   10.9864 g
                                   11.1561 g
                                   0.1697 g
11-07
Blood
                                     24 h
                                   11.0741 g
                                   11.3393 g
                                   0.2652 g
11-08
Blood
                                    Predose
                                   10.9963 g
                                   11.1325 g
                                   0.1362 g
11-08
Blood
                                    6.25 h
                                   11.1056 g
                                   11.1813 g
                                   0.0757 g
11-08
Blood
                                    6.50 h
                                   11.0801 g
                                   11.2471 g
                                   0.1670 g
11-08
Blood
                                      7 h
                                   11.0323 g
                                   11.1790 g
                                   0.1467 g
11-08
Blood
                                    7.33 h
                                   11.1216 g
                                   11.3112 g
                                   0.1896 g
11-08
Blood
                                      8 h
                                   11.0577 g
                                   11.2457 g
                                   0.1880 g
11-08
Blood
                                     10 h
                                   11.0342 g
                                   11.1139 g
                                   0.0797 g
11-08
Blood
                                     16 h
                                   11.0850 g
                                   11.2477 g
                                   0.1627 g
11-08
Blood
                                     24 h
                                   11.0217 g
                                   11.1971 g
                                   0.1754 g
12-01
Blood
                                    Predose
                                   11.0188 g
                                   11.2015 g
                                   0.1827 g
12-01
Blood
                                      5 m
                                   11.0317 g
                                   11.2005 g
                                   0.1688 g
12-01
Blood
                                     10 m
                                   11.0131 g
                                   11.1639 g
                                   0.1508 g
12-01
Blood
                                     15 m
                                   11.0394 g
                                   11.2040 g
                                   0.1646 g
12-01
Blood
                                     30 m
                                   11.0505 g
                                   11.2195 g
                                   0.1690 g
12-01
Blood
                                      1 h
                                   11.0410 g
                                   11.2321 g
                                   0.1911 g
12-01
Blood
                                      2 h
                                   11.0658 g
                                   11.2607 g
                                   0.1949 g
12-01
Blood
                                      4 h
                                   11.0040 g
                                   11.1368 g
                                   0.1328 g

                                    Subject
                                    Sample
                                     Time
                                    Pot wt.
                                  Sample  wt.
                                   Corrected
                                 Sample Weight
12-01
Blood
                                      6 h
                                   11.0444 g
                                   11.2132 g
                                   0.1688 g
12-02
Blood
                                    Predose
                                   11.1106 g
                                   11.3040 g
                                   0.1934 g
12-02
Blood
                                      5 m
                                   11.0298 g
                                   11.2093 g
                                   0.1795 g
12-02
Blood
                                     10 m
                                   11.0011 g
                                   11.1589 g
                                   0.1578 g
12-02
Blood
                                     15 m
                                   11.0383 g
                                   11.2053 g
                                   0.1670 g
12-02
Blood
                                     30 m
                                   10.9946 g
                                   11.1571 g
                                   0.1625 g
12-02
Blood
                                      1 h
                                   11.0513 g
                                   11.2188 g
                                   0.1675 g
12-02
Blood
                                      2 h
                                   11.0638 g
                                   11.2114 g
                                   0.1476 g
12-02
Blood
                                      4 h
                                   10.9824 g
                                   11.1495 g
                                   0.1671 g
12-02
Blood
                                      6 h
                                   11.0447 g
                                   11.1866 g
                                   0.1419 g
12-03
Blood
                                    Predose
                                   11.0738 g
                                   11.2589 g
                                   0.1851 g
12-03
Blood
                                      5 m
                                   11.0440 g
                                   11.2123 g
                                   0.1683 g
12-03
Blood
                                     10 m
                                   11.0659 g
                                   11.2336 g
                                   0.1677 g
12-03
Blood
                                     15 m
                                   11.0882 g
                                   11.2849 g
                                   0.1967 g
12-03
Blood
                                     30 m
                                   11.0154 g
                                   11.2039 g
                                   0.1885 g
12-03
Blood
                                      1 h
                                   11.0646 g
                                   11.2558 g
                                   0.1912 g
12-03
Blood
                                      2 h
                                   11.0914 g
                                   11.2789 g
                                   0.1875 g
12-03
Blood
                                      4 h
                                   11.0735 g
                                   11.2559 g
                                   0.1824 g
12-03
Blood
                                      6 h
                                   10.9909 g
                                   11.2014 g
                                   0.2105 g
12-04
Blood
                                    Predose
                                   11.0160 g
                                   11.2150 g
                                   0.1990 g
12-04
Blood
                                      5 m
                                   11.0541 g
                                   11.1959 g
                                   0.1418 g
12-04
Blood
                                     10 m
                                   11.0828 g
                                   11.2604 g
                                   0.1776 g
12-04
Blood
                                     15 m
                                   11.0198 g
                                   11.2189 g
                                   0.1991 g

                                    Subject
                                    Sample
                                     Time
                                    Pot wt.
                                  Sample  wt.
                                   Corrected
                                 Sample Weight
12-04
Blood
                                     30 m
                                   11.0920 g
                                   11.2422 g
                                   0.1502 g
12-04
Blood
                                      1 h
                                   11.0763 g
                                   11.2754 g
                                   0.1991 g
12-04
Blood
                                      2 h
                                   11.0500 g
                                   11.2274 g
                                   0.1774 g
12-04
Blood
                                      4 h
                                   11.0226 g
                                   11.1794 g
                                   0.1568 g
12-04
Blood
                                      6 h
                                   11.0055 g
                                   11.1713 g
                                   0.1658 g
12-05
Blood
                                    Predose
                                   11.0193 g
                                   11.1617 g
                                   0.1424 g
12-05
Blood
                                    6.25 h
                                   11.0441 g
                                   11.1882 g
                                   0.1441 g
12-05
Blood
                                    6.50 h
                                   11.0759 g
                                   11.2410 g
                                   0.1651 g
12-05
Blood
                                      7 h
                                   11.0387 g
                                   11.2146 g
                                   0.1759 g
12-05
Blood
                                    7.33 h
                                   11.0421 g
                                   11.2228 g
                                   0.1807 g
12-05
Blood
                                      8 h
                                   11.0128 g
                                   11.1538 g
                                   0.1410 g
12-05
Blood
                                     10 h
                                   11.0963 g
                                   11.2988 g
                                   0.2025 g
12-05
Blood
                                     16 h
                                   11.0624 g
                                   11.2340 g
                                   0.1716 g
12-05
Blood
                                     24 h
                                   11.0486 g
                                   11.2049 g
                                   0.1563 g
12-06
Blood
                                    Predose
                                   10.9995 g
                                   11.1536 g
                                   0.1541 g
12-06
Blood
                                    6.25 h
                                   11.0543 g
                                   11.2209 g
                                   0.1666 g
12-06
Blood
                                    6.50 h
                                   11.1035 g
                                   11.2591 g
                                   0.1556 g
12-06
Blood
                                      7 h
                                   11.1145 g
                                   11.2582 g
                                   0.1437 g
12-06
Blood
                                    7.33 h
                                   11.0131 g
                                   11.1992 g
                                   0.1861 g
12-06
Blood
                                      8 h
                                   11.0116 g
                                   11.1574 g
                                   0.1458 g
12-06
Blood
                                     10 h
                                   11.0403 g
                                   11.2244 g
                                   0.1841 g
12-06
Blood
                                     16 h
                                   11.0150 g
                                   11.1740 g
                                   0.1590 g
12-06
Blood
                                     24 h
                                   11.0147 g
                                   11.1890 g
                                   0.1743 g
12-07
Blood
                                    Predose
                                   11.0266 g
                                   11.2259 g
                                   0.1993 g
12-07
Blood
                                    6.25 h
                                   11.0001 g
                                   11.1527 g
                                   0.1526 g
12-07
Blood
                                    6.50 h
                                   11.1242 g
                                   11.2849 g
                                   0.1607 g
12-07
Blood
                                      7 h
                                   11.0771 g
                                   11.2281 g
                                   0.1510 g
12-07
Blood
                                    7.33 h
                                   11.0080 g
                                   11.2669 g
                                   0.2589 g
12-07
Blood
                                      8 h
                                   11.0045 g
                                   11.2407 g
                                   0.2362 g
12-07
Blood
                                     10 h
                                   11.0811 g
                                   11.2577 g
                                   0.1766 g
12-07
Blood
                                     16 h
                                   11.0623 g
                                   11.2120 g
                                   0.1497 g
12-07
Blood
                                     24 h
                                   11.0126 g
                                   11.1910 g
                                   0.1784 g
12-08
Blood
                                    Predose
                                   11.0413 g
                                   11.2350 g
                                   0.1937 g
12-08
Blood
                                    6.25 h
                                   11.0494 g
                                   11.2164 g
                                   0.1670 g
12-08
Blood
                                    6.50 h
                                   11.0447 g
                                   11.1948 g
                                   0.1501 g
12-08
Blood
                                      7 h
                                   11.0010 g
                                   11.1527 g
                                   0.1517 g
12-08
Blood
                                    7.33 h
                                   10.9796 g
                                   11.1139 g
                                   0.1343 g
12-08
Blood
                                      8 h
                                   11.0366 g
                                   11.1857 g
                                   0.1491 g
12-08
Blood
                                     10 h
                                   11.0400 g
                                   11.2110 g
                                   0.1710 g
12-08
Blood
                                     16 h
                                   11.0461 g
                                   11.2073 g
                                   0.1612 g

Table 62.  Blood Sample Weights for Groups 11 and 12.
Subject
Sample
                                     Time
                                    Pot wt.
                                  Sample  wt.
                                   Corrected
                                 Sample Weight
15-01
Blood
                                    Predose
                                   11.4289 g
                                   11.5688 g
                                   0.1399 g
15-01
Blood
                                      5 m
                                   11.3565 g
                                   11.5599 g
                                   0.2034 g
15-01
Blood
                                     10 m
                                   11.4640 g
                                   11.7099 g
                                   0.2459 g
15-01
Blood
                                     15 m
                                   11.2454 g
                                   11.4734 g
                                   0.2280 g
15-01
Blood
                                     30 m
                                   11.2697 g
                                   11.5015 g
                                   0.2318 g
15-01
Blood
                                     30 m
                                   11.2697 g
                                   11.5015 g
                                   0.2318 g
15-01
Blood
                                      1 h
                                   11.3346 g
                                   11.5243 g
                                   0.1897 g
15-01
Blood
                                      2 h
                                   11.3277 g
                                   11.5112 g
                                   0.1835 g
15-01
Blood
                                      4 h
                                   11.1890 g
                                   11.4363 g
                                   0.2473 g
15-01
Blood
                                      4 h
                                   11.1890 g
                                   11.4363 g
                                   0.2473 g
15-01
Blood
                                      6 h
                                   11.2910 g
                                   11.4466 g
                                   0.1556 g
15-02
Blood
                                    Predose
                                   11.3038 g
                                   11.4575 g
                                   0.1537 g
15-02
Blood
                                      5 m
                                   11.3380 g
                                   11.5198 g
                                   0.1818 g
15-02
Blood
                                     10 m
                                   11.2734 g
                                   11.4662 g
                                   0.1928 g
15-02
Blood
                                     15 m
                                   11.3547 g
                                   11.5426 g
                                   0.1879 g
15-02
Blood
                                     30 m
                                   11.2503 g
                                   11.4528 g
                                   0.2025 g
15-02
Blood
                                      1 h
                                   11.3543 g
                                   11.5061 g
                                   0.1518 g
15-02
Blood
                                      2 h
                                   11.3648 g
                                   11.5519 g
                                   0.1871 g
15-02
Blood
                                      4 h
                                   11.3002 g
                                   11.5057 g
                                   0.2055 g
15-02
Blood
                                      6 h
                                   11.2156 g
                                   11.4257 g
                                   0.2101 g
15-03
Blood
                                    Predose
                                   11.4206 g
                                   11.6092 g
                                   0.1886 g
15-03
Blood
                                      5 m
                                   11.3111 g
                                   11.5032 g
                                   0.1921 g
15-03
Blood
                                     10 m
                                   11.1756 g
                                   11.3981 g
                                   0.2225 g
15-03
Blood
                                     15 m
                                   11.2084 g
                                   11.4239 g
                                   0.2155 g
15-03
Blood
                                     30 m
                                   11.3247 g
                                   11.5155 g
                                   0.1908 g
15-03
Blood
                                      1 h
                                   11.3608 g
                                   11.5427 g
                                   0.1819 g
15-03
Blood
                                      2 h
                                   11.2868 g
                                   11.4387 g
                                   0.1519 g
15-03
Blood
                                      4 h
                                   11.1947 g
                                   11.3650 g
                                   0.1703 g
15-03
Blood
                                      6 h
                                   11.3682 g
                                   11.5354 g
                                   0.1672 g
15-04
Blood
                                    Predose
                                   11.2953 g
                                   11.4669 g
                                   0.1716 g
15-04
Blood
                                      5 m
                                   11.2692 g
                                   11.5071 g
                                   0.2379 g
15-04
Blood
                                     10 m
                                   11.2570 g
                                   11.4730 g
                                   0.2160 g
15-04
Blood
                                     15 m
                                   11.2430 g
                                   11.4179 g
                                   0.1749 g
15-04
Blood
                                     30 m
                                   11.2969 g
                                   11.4855 g
                                   0.1886 g
15-04
Blood
                                      1 h
                                   11.3568 g
                                   11.5333 g
                                   0.1765 g
15-04
Blood
                                      2 h
                                   11.3800 g
                                   11.5789 g
                                   0.1989 g

                                    Subject
                                    Sample
                                     Time
                                    Pot wt.
                                  Sample  wt.
                                   Corrected
                                 Sample Weight
15-04
Blood
                                      4 h
                                   11.4319 g
                                   11.5906 g
                                   0.1587 g
15-04
Blood
                                      6 h
                                   11.2608 g
                                   11.4758 g
                                   0.2150 g
15-05
Blood
                                    Predose
                                   11.2638 g
                                   11.4187 g
                                   0.1549 g
15-05
Blood
                                    6.25 h
                                   11.2540 g
                                   11.4457 g
                                   0.1917 g
15-05
Blood
                                    6.50 h
                                   11.3115 g
                                   11.4876 g
                                   0.1761 g
15-05
Blood
                                      7 h
                                   11.2602 g
                                   11.4332 g
                                   0.1730 g
15-05
Blood
                                    7.33 h
                                   11.2717 g
                                   11.4547 g
                                   0.1830 g
15-05
Blood
                                      8 h
                                   11.3463 g
                                   11.6027 g
                                   0.2564 g
15-05
Blood
                                     10 h
                                   11.2959 g
                                   11.5480 g
                                   0.2521 g
15-05
Blood
                                     16 h
                                   11.3294 g
                                   11.5086 g
                                   0.1792 g
15-05
Blood
                                     24 h
                                   11.2868 g
                                   11.4880 g
                                   0.2012 g
15-06
Blood
                                    Predose
                                   11.1042 g
                                   11.2916 g
                                   0.1874 g
15-06
Blood
                                    6.25 h
                                   11.3702 g
                                   11.5550 g
                                   0.1848 g
15-06
Blood
                                    6.50 h
                                   11.3263 g
                                   11.4225 g
                                   0.0962 g
15-06
Blood
                                      7 h
                                   11.3307 g
                                   11.5280 g
                                   0.1973 g
15-06
Blood
                                    7.33 h
                                   11.2949 g
                                   11.4906 g
                                   0.1957 g
15-06
Blood
                                      8 h
                                   11.3665 g
                                   11.6149 g
                                   0.2484 g
15-06
Blood
                                     10 h
                                   11.3817 g
                                   11.5708 g
                                   0.1891 g
15-06
Blood
                                     16 h
                                   11.3327 g
                                   11.4916 g
                                   0.1589 g
15-06
Blood
                                     24 h
                                   11.3622 g
                                   11.5681 g
                                   0.2059 g
15-07
Blood
                                    Predose
                                   11.1540 g
                                   11.3137 g
                                   0.1597 g
15-07
Blood
                                    6.25 h
                                   11.2743 g
                                   11.4540 g
                                   0.1797 g
15-07
Blood
                                    6.50 h
                                   11.3406 g
                                   11.5133 g
                                   0.1727 g
15-07
Blood
                                      7 h
                                   11.2813 g
                                   11.4751 g
                                   0.1938 g
15-07
Blood
                                    7.33 h
                                   11.2024 g
                                   11.3752 g
                                   0.1728 g
15-07
Blood
                                      8 h
                                   11.2339 g
                                   11.4447 g
                                   0.2108 g
15-07
Blood
                                     10 h
                                   11.3097 g
                                   11.5269 g
                                   0.2172 g
15-07
Blood
                                     16 h
                                   11.1488 g
                                   11.3047 g
                                   0.1559 g
15-07
Blood
                                     24 h
                                   11.0858 g
                                   11.2863 g
                                   0.2005 g
15-08
Blood
                                    Predose
                                   11.0194 g
                                   11.1912 g
                                   0.1718 g
15-08
Blood
                                    6.25 h
                                   11.0443 g
                                   11.2497 g
                                   0.2054 g
15-08
Blood
                                    6.50 h
                                   11.2673 g
                                   11.4629 g
                                   0.1956 g
15-08
Blood
                                      7 h
                                   11.3609 g
                                   11.5353 g
                                   0.1744 g
15-08
Blood
                                    7.33 h
                                   11.1097 g
                                   11.2843 g
                                   0.1746 g
15-08
Blood
                                      8 h
                                   11.1675 g
                                   11.3633 g
                                   0.1958 g
15-08
Blood
                                     10 h
                                   11.0593 g
                                   11.2535 g
                                   0.1942 g
15-08
Blood
                                     16 h
                                   10.9917 g
                                   11.1472 g
                                   0.1555 g
15-08
Blood
                                     24 h
                                   11.2366 g
                                   11.4204 g
                                   0.1838 g
16-01
Blood
                                    Predose
                                   11.3519 g
                                   11.5107 g
                                   0.1588 g
16-01
Blood
                                      5 m
                                   11.3353 g
                                   11.5418 g
                                   0.2065 g
16-01
Blood
                                     10 m
                                   11.3337 g
                                   11.5195 g
                                   0.1858 g
16-01
Blood
                                     15 m
                                   11.2459 g
                                   11.5084 g
                                   0.2625 g
16-01
Blood
                                     30 m
                                   11.2977 g
                                   11.4918 g
                                   0.1941 g
16-01
Blood
                                      1 h
                                   11.2420 g
                                   11.3866 g
                                   0.1446 g
16-01
Blood
                                      2 h
                                   11.2863 g
                                   11.4779 g
                                   0.1916 g
16-01
Blood
                                      4 h
                                   11.2553 g
                                   11.4295 g
                                   0.1742 g
16-01
Blood
                                      6 h
                                   11.2830 g
                                   11.4743 g
                                   0.1913 g
16-02
Blood
                                    Predose
                                   11.3411 g
                                   11.5336 g
                                   0.1925 g
16-02
Blood
                                      5 m
                                   11.3325 g
                                   11.5890 g
                                   0.2565 g
16-02
Blood
                                     10 m
                                   11.3150 g
                                   11.5298 g
                                   0.2148 g
16-02
Blood
                                     15 m
                                   11.3551 g
                                   11.5470 g
                                   0.1919 g
16-02
Blood
                                     30 m
                                   11.2601 g
                                   11.4291 g
                                   0.1690 g
16-02
Blood
                                      1 h
                                   11.2718 g
                                   11.4781 g
                                   0.2063 g
16-02
Blood
                                      2 h
                                   11.3306 g
                                   11.5220 g
                                   0.1914 g
16-02
Blood
                                      4 h
                                   11.2877 g
                                   11.4785 g
                                   0.1908 g
16-02
Blood
                                      6 h
                                   11.2497 g
                                   11.4352 g
                                   0.1855 g
16-03
Blood
                                    Predose
                                   11.2212 g
                                   11.3774 g
                                   0.1562 g
16-03
Blood
                                      5 m
                                   11.2893 g
                                   11.4592 g
                                   0.1699 g
16-03
Blood
                                     10 m
                                   11.3173 g
                                   11.4920 g
                                   0.1747 g
16-03
Blood
                                     15 m
                                   11.3409 g
                                   11.5158 g
                                   0.1749 g
16-03
Blood
                                     30 m
                                   11.3211 g
                                   11.4971 g
                                   0.1760 g
16-03
Blood
                                      1 h
                                   11.3686 g
                                   11.4988 g
                                   0.1302 g
16-03
Blood
                                      2 h
                                   11.2046 g
                                   11.3769 g
                                   0.1723 g
16-03
Blood
                                      4 h
                                   11.2882 g
                                   11.4771 g
                                   0.1889 g
16-03
Blood
                                      6 h
                                   11.3178 g
                                   11.4647 g
                                   0.1469 g
16-04
Blood
                                    Predose
                                   11.3686 g
                                   11.5664 g
                                   0.1978 g
16-04
Blood
                                      5 m
                                   11.3695 g
                                   11.5584 g
                                   0.1889 g
16-04
Blood
                                     10 m
                                   11.3489 g
                                   11.5507 g
                                   0.2018 g
16-04
Blood
                                     15 m
                                   11.3519 g
                                   11.5203 g
                                   0.1684 g
16-04
Blood
                                     30 m
                                   11.3173 g
                                   11.5101 g
                                   0.1928 g
16-04
Blood
                                      1 h
                                   11.2609 g
                                   11.4527 g
                                   0.1918 g
16-04
Blood
                                      2 h
                                   11.2697 g
                                   11.4611 g
                                   0.1914 g
16-04
Blood
                                      4 h
                                   11.3144 g
                                   11.5208 g
                                   0.2064 g
16-04
Blood
                                      6 h
                                   11.2897 g
                                   11.5018 g
                                   0.2121 g
16-05
Blood
                                    Predose
                                   11.3208 g
                                   11.4523 g
                                   0.1315 g
16-05
Blood
                                    6.25 h
                                   11.0979 g
                                   11.2576 g
                                   0.1597 g
16-05
Blood
                                    6.50 h
                                   11.0990 g
                                   11.2590 g
                                   0.1600 g
16-05
Blood
                                      7 h
                                   11.1481 g
                                   11.4196 g
                                   0.2715 g
16-05
Blood
                                    7.33 h
                                   11.0463 g
                                   11.2206 g
                                   0.1743 g
16-05
Blood
                                      8 h
                                   11.0451 g
                                   11.2300 g
                                   0.1849 g
16-05
Blood
                                     10 h
                                   11.0209 g
                                   11.2069 g
                                   0.1860 g
16-05
Blood
                                     16 h
                                   11.0925 g
                                   11.3021 g
                                   0.2096 g
16-05
Blood
                                     24 h
                                   11.0172 g
                                   11.2057 g
                                   0.1885 g
16-06
Blood
                                    Predose
                                   10.9800 g
                                   11.1305 g
                                   0.1505 g
16-06
Blood
                                    6.25 h
                                   11.0911 g
                                   11.2586 g
                                   0.1675 g
16-06
Blood
                                      7 h
                                   11.1414 g
                                   11.3377 g
                                   0.1963 g
16-06
Blood
                                    7.33 h
                                   11.0614 g
                                   11.2569 g
                                   0.1955 g
16-06
Blood
                                      8 h
                                   11.2690 g
                                   11.4389 g
                                   0.1699 g
16-06
Blood
                                     10 h
                                   11.0302 g
                                   11.2275 g
                                   0.1973 g
16-06
Blood
                                     16 h
                                   11.1344 g
                                   11.3019 g
                                   0.1675 g
16-06
Blood
                                     24 h
                                   11.0666 g
                                   11.2534 g
                                   0.1868 g
16-07
Blood
                                    Predose
                                   11.0411 g
                                   11.2227 g
                                   0.1816 g
16-07
Blood
                                    6.25 h
                                   11.1220 g
                                   11.2949 g
                                   0.1729 g
16-07
Blood
                                    6.50 h
                                   11.2058 g
                                   11.3956 g
                                   0.1898 g
16-07
Blood
                                      7 h
                                   11.0734 g
                                   11.2271 g
                                   0.1537 g
16-07
Blood
                                    7.33 h
                                   11.2107 g
                                   11.3887 g
                                   0.1780 g
16-07
Blood
                                      8 h
                                   11.1425 g
                                   11.3289 g
                                   0.1864 g
16-07
Blood
                                     10 h
                                   11.0091 g
                                   11.1917 g
                                   0.1826 g
16-07
Blood
                                     16 h
                                   11.1184 g
                                   11.2938 g
                                   0.1754 g
16-07
Blood
                                     24 h
                                   11.0527 g
                                   11.2307 g
                                   0.1780 g
16-08
Blood
                                    Predose
                                   11.0403 g
                                   11.1987 g
                                   0.1584 g
16-08
Blood
                                    6.25 h
                                   11.0832 g
                                   11.2328 g
                                   0.1496 g
16-08
Blood
                                    6.50 h
                                   11.2325 g
                                   11.4501 g
                                   0.2176 g
16-08
Blood
                                      7 h
                                   10.9866 g
                                   11.1581 g
                                   0.1715 g
16-08
Blood
                                    7.33 h
                                   11.2202 g
                                   11.3895 g
                                   0.1693 g
16-08
Blood
                                      8 h
                                   11.1086 g
                                   11.2989 g
                                   0.1903 g
16-08
Blood
                                     10 h
                                   11.0481 g
                                   11.2604 g
                                   0.2123 g
16-08
Blood
                                     16 h
                                   11.0726 g
                                   11.2500 g
                                   0.1774 g
16-08
Blood
                                     24 h
                                   11.0497 g
                                   11.2772 g
                                   0.2275 g

Table 63.  Low Calibration curve for DIPE in blood for 600 ppm exposures.

                                   Peak Area

Sample I.D.
                               Standard/QC I.D
                                 Conc. (ug/ml)
                                     DIPE
                                     MTBE
                                Peak Area Ratio
                              Cal. Conc. (ug/ml)
                                     Mean
                                      SD
                               RSD% (Precision)
                                 Accuracy (%)
13425-23A
                                  Blood blank
                                       0
                                       0
                                       0
                                      n/a
                                      n/a
                                      n/a
                                      n/a
                                      n/a
                                      n/a
13425-24A
                                  Blood blank
                                       0
                                       0
                                       0
                                      n/a
                                      n/a
                                       -
                                       -
                                       -
                                      n/a
13425-25A
                                  Blood blank
                                       0
                                       0
                                       0
                                      n/a
                                      n/a
                                       -
                                       -
                                       -
                                      n/a
13425-23B
                               Blood ISTD blank
                                       0
                                       0
                                    3762103
                                       0
                                      n/a
                                      n/a
                                      n/a
                                      n/a
                                      n/a
13425-24B
                               Blood ISTD blank
                                       0
                                       0
                                    3725364
                                       0
                                      n/a
                                       -
                                       -
                                       -
                                      n/a
13425-25B
                               Blood ISTD blank
                                       0
                                       0
                                    3415475
                                       0
                                      n/a
                                       -
                                       -
                                       -
                                      n/a
13425-23C
                                    Std A1
                                    0.0932
                                     28163
                                    3738967
                                    0.00753
                                    0.0868
                                    0.1017
                                    0.01467
                                    14.43%
                                     93.1%
13425-24C
                                    Std A1
                                    0.0932
                                     31567
                                    3666201
                                    0.00861
                                     0.102
                                       -
                                       -
                                       -
                                     110%
13425-25C
                                    Std A1
                                    0.0932
                                     33176
                                    3459081
                                    0.00959
                                    0.1161
                                       -
                                       -
                                       -
                                     125%
13425-23D
                                    Std B1
                                     0.236
                                     63060
                                    3314779
                                    0.0190
                                     0.251
                                     0.248
                                    0.01330
                                     5.36%
                                     106%
13425-24D
                                    Std B1
                                     0.236
                                     65344
                                    3662856
                                    0.0178
                                     0.234

                                     99.0%
13425-25D
                                    Std B1
                                     0.236
                                     69290
                                    3520621
                                    0.0197
                                     0.260

                                     110%
13425-23E
                                    Std A2
                                     0.472
                                    111256
                                    3600170
                                    0.0309
                                     0.420
                                     0.450
                                    0.03592
                                     7.98%
                                     88.9%
13425-24E
                                    Std A2
                                     0.472
                                    116893
                                    3613255
                                    0.0324
                                     0.440
                                       -
                                       -
                                       -
                                     93.3%
13425-25E
                                    Std A2
                                     0.472
                                    123649
                                    3453034
                                    0.0358
                                     0.490
                                       -
                                       -
                                       -
                                    103.7%
13425-23F
                                    Std B2
                                     0.960
                                    245237
                                    3758730
                                    0.0652
                                     0.909
                                     0.902
                                    0.18149
                                    20.12%
                                     94.7%
13425-24F
                                    Std B2
                                     0.960
                                    192756
                                    3722665
                                    0.0518
                                     0.717

                                     74.7%
13425-25F
                                    Std B2
                                     0.960
                                    270408
                                    3500966
                                    0.0772
                                     1.08

                                     113%
13425-23G
                                    Std A3
                                     2.40
                                    579989
                                    3706629
                                     0.156
                                     2.21
                                     2.18
                                    0.1116
                                     5.11%
                                     92.0%
13425-24G
                                    Std A3
                                     2.40
                                    530120
                                    3624960
                                     0.146
                                     2.06

                                     86.0%
13425-25G
                                    Std A3
                                     2.40
                                    548087
                                    3390861
                                     0.162
                                     2.28

                                     95.1%
13425-23H
                                    Std B3
                                     4.87
                                    1229642
                                    3695637
                                     0.333
                                     4.72
                                     5.14
                                     0.443
                                     8.62%
                                     96.9%
13425-24H
                                    Std B3
                                     4.87
                                    1316003
                                    3658777
                                     0.360
                                     5.10
                                       -
                                       -
                                       -
                                     105%
13425-25H
                                    Std B3
                                     4.87
                                    1387013
                                    3513575
                                     0.395
                                     5.60
                                       -
                                       -
                                       -
                                     115%
13425-26-7
                                      LQC
                                     0.472
                                    132566
                                    4199237
                                    0.0316
                                     0.429
                                       -
                                       -
                                       -
                                     90.9%
13425-28-25
                                      LQC
                                     0.472
                                    100859
                                    3639015
                                    0.0277
                                     0.374
                                       -
                                       -
                                       -
                                     79.3%
13425-26-33
                                      MQC
                                     4.87
                                    1335973
                                    4289744
                                     0.311
                                     4.42
                                       -
                                       -
                                       -
                                     90.7%
13425-27-38
                                      MQC
                                     4.87
                                    1154003
                                    3783218
                                     0.305
                                     4.33
                                       -
                                       -
                                       -
                                     88.8%

                                   INTERCEPT
                                   0.001443

                                     SLOPE
                                    0.07018

                                       r
                                     0.993

Table 64.  High Calibration curve for DIPE in blood for 600 ppm exposures.

                                   Peak Area

Sample I.D.
                               Standard/QC I.D
                                 Conc. (ug/ml)
                                     DIPE
                                     MTBE
                                Peak Area Ratio
                              Cal. Conc. (ug/ml)
                                     Mean
                                      SD
                               RSD% (Precision)
                                 Accuracy (%)
13425-23H
                                    Std B3
                                     4.87
                                    1229642
                                    3695637
                                     0.333
                                     4.91
                                     5.25
                                     0.356
                                     6.78%
                                     101%
13425-24H
                                    Std B3
                                     4.87
                                    1316003
                                    3658777
                                     0.360
                                     5.22
                                       -
                                       -
                                       -
                                     107%
13425-25H
                                    Std B3
                                     4.87
                                    1387013
                                    3513575
                                     0.395
                                     5.62
                                       -
                                       -
                                       -
                                     115%
13425-23I
                                    Std A4
                                     9.68
                                    2358415
                                    3629250
                                     0.650
                                     8.53
                                     9.38
                                     0.769
                                     8.20%
                                     88.1%
13425-24I
                                    Std A4
                                     9.68
                                    2862759
                                    3855341
                                     0.743
                                     9.59
                                       -
                                       -
                                       -
                                     99.1%
13425-25I
                                    Std A4
                                     9.68
                                    2767098
                                    3544536
                                     0.781
                                     10.0
                                       -
                                       -
                                       -
                                     104%
13425-23J
                                    Std B4
                                     24.7
                                    5572018
                                    3183436
                                     1.75
                                     21.1
                                     23.8
                                     2.54
                                    10.68%
                                     85.5%
13425-24J
                                    Std B4
                                     24.7
                                    7574370
                                    3773740
                                     2.01
                                     24.0
                                       -
                                       -
                                       -
                                     97.3%
13425-25J
                                    Std B4
                                     24.7
                                    7874922
                                    3591233
                                     2.19
                                     26.2
                                       -
                                       -
                                       -
                                    105.9%
13425-23K
                                    Std A5
                                     48.9
                                   13815022
                                    3780190
                                     3.65
                                     42.9
                                     47.3
                                     4.51
                                     9.55%
                                     87.7%
13425-24K
                                    Std A5
                                     48.9
                                   15299434
                                    3810538
                                     4.02
                                     47.0
                                       -
                                       -
                                       -
                                     96.1%
13425-25K
                                    Std A5
                                     48.9
                                   16054132
                                    3613168
                                     4.44
                                     51.9
                                       -
                                       -
                                       -
                                     106%
13425-23L
                                    Std B5
                                     99.7
                                   29517096
                                    3727530
                                     7.92
                                     91.6
                                     102.0
                                     9.95
                                     9.76%
                                     91.9%
13425-24L
                                    Std B5
                                     99.7
                                   34202536
                                    3845198
                                     8.89
                                      103
                                       -
                                       -
                                       -
                                    103.1%
13425-25L
                                    Std B5
                                     99.7
                                   35405538
                                    3666790
                                     9.66
                                      111
                                       -
                                       -
                                       -
                                    111.8%
13425-23M
                                    Std A6
                                      247
                                   66287942
                                    3661535
                                     18.1
                                      208
                                      247
                                     35.42
                                    14.32%
                                     84.4%
13425-24M
                                    Std A6
                                      247
                                   83281573
                                    3715376
                                     22.4
                                      257
                                       -
                                       -
                                       -
                                     104%
13425-25M
                                    Std A6
                                      247
                                   82353762
                                    3415122
                                     24.1
                                      277
                                       -
                                       -
                                       -
                                     112%
13425-27-19
                                      HQC
                                     99.7
                                   33512784
                                    4288510
                                     7.81
                                     90.4
                                       -
                                       -
                                       -
                                     90.7%
13425-28-32
                                      HQC
                                     99.7
                                   36275868
                                    4007133
                                     9.05
                                      105
                                       -
                                       -
                                       -
                                     105%

                                    INTERCEPT
                                   -0.09661

                                     SLOPE
                                    0.08749

                                       r
                                     0.993

Table 65.  Low Calibration curve for Isopropanol in blood for 600 ppm exposures.

                                   Peak Area

Sample I.D.
                               Standard/QC I.D
                                 Conc. (ug/ml)
                                  Isopropanol
                                  1-Propanol
                                Peak Area Ratio
                              Cal. Conc. (ug/ml)
                                     Mean
                                      SD
                               RSD% (Precision)
                                 Accuracy (%)
13425-23A
                                  Blood blank
                                      n/a
                                     4213
                                     5931
                                      n/a
                                      n/a
                                      n/a
                                      n/a
                                      n/a
                                      n/a
13425-24A
                                  Blood blank
                                      n/a
                                     16350
                                     11335
                                      n/a
                                      n/a
                                       -
                                       -
                                       -
                                      n/a
13425-25A
                                  Blood blank
                                      n/a
                                     3601
                                     5415
                                      n/a
                                      n/a
                                       -
                                       -
                                       -
                                      n/a
13425-23B
                               Blood ISTD blank
                                      n/a
                                     3850
                                    3948653
                                    0.00098
                                   below LOQ
                                      n/a
                                      n/a
                                      n/a
                                      n/a
13425-24B
                               Blood ISTD blank
                                      n/a
                                     5316
                                    4331379
                                    0.00123
                                   below LOQ
                                       -
                                       -
                                       -
                                      n/a
13425-25B
                               Blood ISTD blank
                                      n/a
                                     4236
                                    4164903
                                    0.00102
                                   below LOQ
                                       -
                                       -
                                       -
                                      n/a
13425-23C
                                    Std A1
                                    0.0906
                                     17305
                                    4031382
                                    0.00429
                                    0.0994
                                    0.0947
                                    0.00404
                                     4.27%
                                     110%
13425-24C
                                    Std A1
                                    0.0906
                                     18872
                                    4680409
                                    0.00403
                                    0.0923
                                       -
                                       -
                                       -
                                     102%
13425-25C
                                    Std A1
                                    0.0906
                                     19005
                                    4704762
                                    0.00404
                                    0.0925
                                       -
                                       -
                                       -
                                     102%
13425-23D
                                    Std B1
                                     0.227
                                     36978
                                    3971808
                                    0.00931
                                     0.236
                                     0.225
                                    0.0115
                                     5.10%
                                     104%
13425-24D
                                    Std B1
                                     0.227
                                     39062
                                    4611733
                                    0.00847
                                     0.213
                                       -
                                       -
                                       -
                                     94.0%
13425-25D
                                    Std B1
                                     0.224
                                     39516
                                    4455056
                                    0.00887
                                     0.224
                                       -
                                       -
                                       -
                                     100%
13425-23E
                                    Std A2
                                     0.459
                                     71436
                                    3954100
                                    0.0181
                                     0.475
                                     0.452
                                    0.0259
                                     5.73%
                                     103%
13425-24E
                                    Std A2
                                     0.459
                                     73511
                                    4538323
                                    0.0162
                                     0.424
                                       -
                                       -
                                       -
                                     92.4%
13425-25E
                                    Std A2
                                     0.459
                                     77487
                                    4443095
                                    0.0174
                                     0.458
                                       -
                                       -
                                       -
                                     100%
13425-23F
                                    Std B2
                                     0.924
                                    143041
                                    4001474
                                    0.0357
                                     0.957
                                     0.906
                                    0.0497
                                     5.49%
                                     104%
13425-24F
                                    Std B2
                                     0.924
                                    150268
                                    4680603
                                    0.0321
                                     0.857
                                       -
                                       -
                                       -
                                     92.8%
13425-25F
                                    Std B2
                                     0.924
                                    149780
                                    4437194
                                    0.0338
                                     0.902
                                       -
                                       -
                                       -
                                     97.7%
13425-23G
                                    Std A3
                                     2.33
                                    364466
                                    4083466
                                    0.0893
                                     2.42
                                     2.31
                                     0.114
                                     4.92%
                                     104%
13425-24G
                                    Std A3
                                     2.33
                                    378970
                                    4680793
                                    0.0810
                                     2.19
                                       -
                                       -
                                       -
                                     94.0%
13425-25G
                                    Std A3
                                     2.33
                                    374705
                                    4363665
                                    0.0859
                                     2.32
                                       -
                                       -
                                       -
                                     100%
13425-13H
                                    Std B3
                                     4.69
                                    749765
                                    4011319
                                     0.187
                                     5.08
                                     4.73
                                     0.331
                                     6.99%
                                     108%
13425-14H
                                    Std B3
                                     4.69
                                    762622
                                    4686024
                                     0.163
                                     4.42
                                       -
                                       -
                                       -
                                     94.2%
13425-15H
                                    Std B3
                                     4.69
                                    780747
                                    4515136
                                     0.173
                                     4.70
                                       -
                                       -
                                       -
                                     100%
13425-26-7
                                      LQC
                                     0.459
                                     80465
                                    4532568
                                    0.0178
                                     0.466
                                       -
                                       -
                                       -
                                     102%
13425-28-25
                                      LQC
                                     0.459
                                     67770
                                    3586288
                                    0.0189
                                     0.497
                                       -
                                       -
                                       -
                                     108%
13425-26-33
                                      MQC
                                     4.69
                                    824159
                                    4387629
                                     0.188
                                     5.10
                                       -
                                       -
                                       -
                                     109%
13425-27-38
                                      MQC
                                     4.69
                                    724367
                                    3823243
                                     0.189
                                     5.15
                                       -
                                       -
                                       -
                                     110%

                                   INTERCEPT
                                   0.0006453

                                     SLOPE
                                    0.03669

                                       r
                                     0.998

Table 66.  High Calibration curve for Isopropanol in blood for 600 ppm exposures.

                                   Peak Area

Sample I.D.
                               Standard/QC I.D
                                 Conc. (ug/ml)
                                  Isopropanol
                                  1-Propanol
                                Peak Area Ratio
                              Cal. Conc. (ug/ml)
                                     Mean
                                      SD
                               RSD% (Precision)
                                 Accuracy (%)
13425-13H
                                    Std B3
                                     4.69
                                    749765
                                    4011319
                                     0.187
                                     5.49
                                     5.22
                                     0.261
                                     5.00%
                                     117%
13425-14H
                                    Std B3
                                     4.69
                                    762622
                                    4686024
                                     0.163
                                     4.97
                                       -
                                       -
                                       -
                                     106%
13425-15H
                                    Std B3
                                     4.69
                                    780747
                                    4515136
                                     0.173
                                     5.19
                                       -
                                       -
                                       -
                                     111%
13425-13I
                                    Std A4
                                     9.42
                                    1779703
                                    4792988
                                     0.371
                                     9.45
                                     9.26
                                     0.207
                                     2.23%
                                     100%
13425-14I
                                    Std A4
                                     9.42
                                    1683595
                                    4779363
                                     0.352
                                     9.04
                                       -
                                       -
                                       -
                                     95.9%
13425-15I
                                    Std A4
                                     9.42
                                    1690040
                                    4638233
                                     0.364
                                     9.30
                                       -
                                       -
                                       -
                                     98.7%
13425-13J
                                    Std B4
                                     23.7
                                    4642480
                                    4625810
                                     1.004
                                     23.0
                                     22.2
                                     0.850
                                     3.83%
                                     97.1%
13425-14J
                                    Std B4
                                     23.7
                                    4563472
                                    4936501
                                     0.924
                                     21.3
                                       -
                                       -
                                       -
                                     90.0%
13425-15J
                                    Std B4
                                     23.7
                                    4506855
                                    4662018
                                     0.967
                                     22.2
                                       -
                                       -
                                       -
                                     93.8%
13425-13K
                                    Std A5
                                     47.6
                                    9592923
                                    4510726
                                     2.13
                                     47.1
                                     45.2
                                     2.13
                                     4.72%
                                     99.0%
13425-14K
                                    Std A5
                                     47.6
                                    9981952
                                    5170005
                                     1.93
                                     42.9
                                       -
                                       -
                                       -
                                     90.2%
13425-15K
                                    Std A5
                                     47.6
                                    9661658
                                    4695041
                                     2.06
                                     45.7
                                       -
                                       -
                                       -
                                     95.9%
13425-13L
                                    Std B5
                                     95.9
                                   19694469
                                    4448358
                                     4.43
                                     96.5
                                     94.6
                                     3.35
                                     3.55%
                                     101%
13425-14L
                                    Std B5
                                     95.9
                                   20210941
                                    4863419
                                     4.16
                                     90.7
                                       -
                                       -
                                       -
                                     94.6%
13425-15L
                                    Std B5
                                     95.9
                                   20689392
                                    4675246
                                     4.43
                                     96.5
                                       -
                                       -
                                       -
                                     101%
12322-126M
                                    Std A6
                                      240
                                   49015129
                                    4201901
                                     11.7
                                      252
                                      244
                                     9.21
                                     3.77%
                                     105%
13425-13M
                                    Std A6
                                      240
                                   52592878
                                    4855710
                                     10.8
                                      234
                                       -
                                       -
                                       -
                                     97.6%
13425-14M
                                    Std A6
                                      240
                                   49975123
                                    4375106
                                     11.4
                                      247
                                       -
                                       -
                                       -
                                     103%
13425-27-19
                                      HQC
                                     95.9
                                   19666864
                                    4415364
                                     4.45
                                     97.1
                                       -
                                       -
                                       -
                                     101%
13425-28-32
                                      HQC
                                     95.9
                                   19361213
                                    4792120
                                     4.04
                                     88.2
                                       -
                                       -
                                       -
                                     92.0%

                                    INTERCEPT
                                   -0.06873

                                     SLOPE
                                    0.04658

                                       r
                                     0.999

Table 67.  Low Calibration curve for Acetone in blood for 600 ppm exposures.

                                   Peak Area

Sample I.D.
                               Standard/QC I.D
                                 Conc. (ug/ml)
                                    Acetone
                                  1-Propanol
                                Peak Area Ratio
                              Cal. Conc. (ug/ml)
                                     Mean
                                      SD
                               RSD% (Precision)
                                 Accuracy (%)
13425-23A
                                  Blood blank
                                      n/a
                                     63964
                                     5931
                                      n/a
                                      n/a
                                      n/a
                                      n/a
                                      n/a
                                      n/a
13425-24A
                                  Blood blank
                                      n/a
                                     80842
                                     11335
                                      n/a
                                      n/a
                                       -
                                       -
                                       -
                                      n/a
13425-25A
                                  Blood blank
                                      n/a
                                     76537
                                     5415
                                      n/a
                                      n/a
                                       -
                                       -
                                       -
                                      n/a
13425-23B
                               Blood ISTD blank
                                      n/a
                                     62491
                                    3948653
                                    0.0158
                                   below LOQ
                                      n/a
                                      n/a
                                      n/a
                                      n/a
13425-24B
                               Blood ISTD blank
                                      n/a
                                     79553
                                    4331379
                                    0.0184
                                   below LOQ
                                       -
                                       -
                                       -
                                      n/a
13425-25B
                               Blood ISTD blank
                                      n/a
                                     74378
                                    4164903
                                    0.0179
                                   below LOQ
                                       -
                                       -
                                       -
                                      n/a
13425-23C
                                    Std A1
                                    0.0910
                                     73727
                                    4031382
                                    0.0183
                                     0.100
                                    0.0818
                                    0.0180
                                     22.1%
                                     110%
13425-24C
                                    Std A1
                                    0.0910