APPENDICES 1 APPENDIX I Additional Notes on Water Use 11 04 94 Ed Barnhart, ELBA, Inc.

1. 1993 textile production data from U. S. Dept. of Agriculture, Economic Research Service. 2. Estimates of water use per pound of fiber processed. a. Wool fiber ( scoured): finishing into textile product uses an average of 20 gal./ lb. b. Cotton fiber: conversion into finished textile products uses an average of 13 gal./ lb. c. Synthetic fiber: conversion into finished textile products, uses an average of 11 gal./ lb.

11 09 94 Ed Barnhart, ELBA, Inc.

There are less than 50 woolen mills currently operating in U. S. They are located mostly in MA and lower ME, with a few in NH. Only 5 of these mills still scour wool, compared to 11 mills reportedly scouring in 1980 ( Dev. Doc., Sept. 1982, Tables V 1, V 2, pp 97,98). On average these mills use about 200,000 gal/ day. Virtually all imported wool has been scoured in the country of origin, so wet processing of wool in U. S. is now limited almost entirely to finishing. Water use is variable for wool processing, but ranges from 15 25 gal./ lb. A good average is 20 gal/ lb.

11 10 94 Jeff Silliman, Milliken Corp.

Question: How many days a year does a textile mill operate? Depends on business conditions. Because the days of operation are pegged to sales more than holidays, the days of operation are reduced when sales fall off. The larger textile mills would like to operate 7 days/ week, but do not want to accumulate excess inventories. Can operate fewer days, but prefer to use fewer machines and operate 7 days/ week. Suggested using 355 operating days/ year as a reasonable assumption.

11 25 94 Ed Barnhart, ELBA, Inc.

Question: How many days a year does a textile mill operate? Suggested using 345 operating days/ year as a reasonable assumption. 2 APPENDIX II 1 AMSA POTWs and Their Textile Users Boston, MA  Massachusetts Water Resources Authority Deer Island POTW Emtex, Inc. Synthon Industries, Inc. TYCA Corp. Nut Island POTW Draper Properties, Inc. International Paper, Vertec Div. Tamfelt, Inc.

Cuyahoga Heights, OH  Northeast Ohio Regional Sewer District Phoenix Dye Works Ohio Knitting Mills, Inc.

Chicago, IL  Metropolitan Water Reclamation Districts of Greater Chicago Industrial Coatings Group, Inc. Rubens & Marble, Inc. Western Piece Dyers & Finishers, Inc.

Columbus, GA  Columbus Water Works Bibb Co. Fieldcrest Mills, Inc., Broadway Div. ( Permit 91 026 01) Fieldcrest Mills, Inc., E& P Div. ( Permit 91 025 01) Swift Textiles, Inc., 6th Ave. ( Permit 91 009 01) Swift Textiles, Inc., Flatrock ( Permit 91 008 01) Swift Spinning Mills ( Permit 91 006 01) Meritas Yarns, Inc. Omi Georgia, Inc. Wellington Sears Co., 1st Ave. ( Permit 91 002 02) Wellington Sears Co., Cusseta ( Permit 91 007 02) Columbus Mills, Inc.

Denver, CO  Metro Denver Rocky Mountain Dye & Finishing Elizabeth, NJ  Joint Meeting of Essex & Union Counties Fablok Mills, Inc.

Greenville, SC  Western Carolina Regional Sewer Authority Mauldin Road POTW ( Travelers Rest) Carisbrook Yarns JPS Industrial Fabrics  Dunean Front ( Permit 1154C) JPS Industrial Fabrics  Dunean Back ( Permit 1164C) JPS Automotive Fabrics  Parker ( Permit 0364C)> Low water Judson Plant  Div. of Milliken & Co. KM Fabrics Krieger Textile Corp. M TEX Corp. ( formerly EMB TEX) Palmetto State Finishing 3 AMSA POTWs and Textile Users ( cont.)

Mauldin Road POTW ( cont.) Specialty Shearing & Dyeing, Inc. U. S. Finishing Woven Electronics ( formerly Southern Weaving) Wunda Weve Carpets, Inc. Lakeside POTW Bibb Towels ( JPS White Horse) Pelham POTW Cardinal Garment Dye Corp. Slater Marietta POTW JPS Industrial Fabrics  Slater ( Permit 0424C) Taylors POTW Greenville Finishing JPS Automotive Fabrics  Bleachery ( Permit 0675C) JPS Automotive Fabrics  Kuster ( Permit 0665C) Orion Finishing ( formerly BES)

Knoxville, TN  Knoxville Utilities Board Appalachian Finishing Werks Little Ferry, NJ  Bergen County Utilities Authority Advanced Fiber Technologies Beacon Looms H & W Shoe Supplies Co. Marijon Dyeing & Finishing Co. Spinnerin Yarn Co., Inc.

Los Angeles, CA  L. A. Sanitation District American International Textiles Artesia Dyeing & Printing, Inc. ( Permit 13066) Artesia Dyeing & Printing, Inc. ( Permit 12330) Artistic Dyers, Inc. Atlas Carpet Mills Bentley Mills Cal Pacific Dyeing & Finishing Corp. California Webbing Industries Care Tex Industries, Inc. Chemtex Print USA, Inc. Coloramerica Textile Processing, Inc. Colortex Dyeing & Finishing, Inc. Cotton Club Delta Dyeing & Finishing, Inc. Downtown Dyers Dynamic Dye & Laundry E & J Dye House EKPG E. T. C. Carpet Mills, Ltd. F & J Metro Dyeing, Inc. Factory, Inc. Flamingo Textile Mills, Inc. Formosa Dyeing & Finishing, Inc. Giant Merchandising 4 AMSA POTWs and Textile Users ( cont.)

L. A. Sanitation District ( cont.) Grace Kimmy Designs L. A. Airline, Inc. L. A. Dye & Print Works, Inc. ( Permit 12817) L. A. Dye & Print Works, Inc. ( Permit 12818) L. A. Dye & Print Works, Inc. ( Permit for by pass only) L. A. Dye & Print Works, Inc. ( Permit 11216) L. A. Dye & Wash Co., Inc. ( Permit 12943) L. A. Dye & Wash Co., Inc. ( Permit 13074) Long Beach Dyeing & Finishing Lorber Industries Louie Bernard, Inc. Pacific Combing Pacific Continental Textile, Inc. Pacific Fabric Printers Pan Pacific Yarn Polytex Thread Mills Pomona Textile Co., Inc. Rainbow Textile Co. S. S. Dyeing & Finishing Santa Fe Dye & Finish Co. ( not SIC 22 > SIC 23) Shing Jye Supplies, Inc. Somitex Prints of California Southern California Dyeing & Finishing ( not SIC 22 > SIC 23) Spectrum Dyeing & Finishing Sun Dyeing & Finishing Corp. Sung Do International, Inc. Texlon Corp. Texollini, Inc. Tissurama Industries, Inc. Toyoshima America, Inc. ( not SIC 22 > SIC 23) Triple A Garment Care ( not SIC 22 > SIC 23) Tuftex Carpet Mills, Inc. U. S. Boys, Inc. U. S. Garment Processing ( not SIC 22 > SIC 23) U. S. Namesung Textile, Inc. ( not SIC 22 > SIC 23) Uni Hosiery Co., Inc. United Thread Manufacturing Corp. Western Dyeing & Finishing Co. Western Tex Industries, Inc.

Los Angeles, CA  City of Los Angeles Hyperion POTW ABC Dye House, Inc. Bruck Braid Co. California Dye House City Dyeing & Finishing Co. ( Permit 488879) City Dyeing & Finishing Co. ( Permit 488887) Coast Arrow, Inc. Colormax Industries, Inc. Coloring Button Dyers Color Master Garmet Dyeing & Finishing 5 AMSA POTWs and Textile Users ( cont.)

Hyperion POTW ( cont.) Dara, Inc. David S. Gibson, Inc. Dixie Trimming Co. Double " A" Wash & Dye Dyetech Corp. Dye to Match Fashion Art International Foid Garment Dyeing  Div. of Fashion Out In California, Inc. J & J Tee Shirts & Fashions, Inc. Kesbaf Knittng, Inc. ( Permit 449694) Kesbaf Knitting, Inc. ( Permit 449702) Koo's Manufacturing Co. L. A. Dye Works, Inc. ( Permit 473088) L. A. Dye Works, Inc.  Rainbow Div. ( Permit 484357) L. A. Dye & Print Works, Inc. M & D Buttons & Lace Dyers Maria Kipp, Inc. Matchmaster, Inc. ( Permit 478475) Matchmaster Dyeing & Finishing, Inc. ( Permit 465176) Matchmaster Dyeing & Finishing, Inc. ( Permit 404107) Matchmaster Dyeing & Finishing, Inc. ( Permit 404115) MW Graphics/ Melvin Wyner Modern Button Co. of California, Inc. Only in USA Pico Dyeing & Finishing Co. Pour le Bebe, Inc. ( Baby Guess) Rainbow Button Dyers S & A Button Dyers Sealmaster W. T. Co., Inc. ( dba Elite Dyers) Sharon & Joyces Clothing, Inc. SNS Brothers, Inc. S & S Dye House Super Yarn Mart Uni Hosiery Co., Inc. Washington Garment Dyeing & Finishing, Inc. Western Dye House ( Permit 12417) Account serviced by LA Co. Western Dye House ( Permit 12418) Western Synthetic Felt Co. Glendale POTW A & H California, Inc. Almore Dye House Avi Levy Caravan Fashion Enterprises Color Fabric Processing, Inc. New Hero 6 AMSA POTWs and Textile Users ( cont.)

Orange County, CA  O. C. Sanitation Districts American Continental Cherokee ( Error: not SIC 22 > 2335 or 2339) Anaheim Mills Corp. Chroma Systems Partners Crazy Shirts, Inc. ( Error: not SIC 22 > 2396) Dye Technique Margaretis Textile Service Pharr Palomar, Inc. Primatex Industries ( Error: not SIC 22 > 2396) Royal Carpet Mills Saba Textiles Saliba Center USA ( Error: not SIC 22 > 2396) Sees Color Textile U. S. Dyeing & Finishing Vans, Inc.

Nashville, TN  Nashville & Davidson Co. Dept. of Water & Sewerage Services Springs Industries, Inc.

Newark, NJ  Passaic Valley Sewerage Commissioners A & S Dyers Apollo Dyeing & Finishing Co. Baltic Dyeing & Finishing Co. Champion Dyeing & Finishing Co. Columbia Textile Services, Inc. Como Textile Prints, Inc. Coral Dyeing & Finishing Corp. Craft Textile Printing Co. Crestany Textile Processors Dye Tex Corp. E & W Textile Processors, Inc. Fairfield Textiles International Veeling Corp. Interstate Dyeing & Finishing Leader Dyeing & Finishing Manner Textile Processing Messbrenner Prints, Inc. North Jersey Skein Dye Co. Paragon Dyeing & Finishing Paterson Bleachery & Chemicals Pauls Dyeing Perennial Print Corp. Poughkeepsie Finishing Rainbow Dye & Finishing Renco Finishing Corp. Safer Textile Processing Corp. Signature Cloth Co. Sunbrite Dye Co. Superior Dyeing Corp. Thomas Henshall Silk Finishing Thorn, Inc. Trio Dyeing & Finishing 7 AMSA POTWs and Textile Users ( cont.)

Newark, NJ ( cont.) Uni Trade Co. United Veil Dyeing & Finishing Zenith Dyeing & Finishing Philadelphia, PA  Philadelphia Water Dept. Anchor Dyeing & Finishing Co. Delaware Valley Wool Scouring Co. General Felt Industries Globe Dye Works Phoenix, AZ  City of Phoenix Arizona Garment Finishers Portland, OR  City of Portland Columbia Wool Scouring Mills East Providence, RI ( Bucklin Point)  The Narragansett Bay Commission Conrad Jarvis Corp. Crown Yarn Dye Co., Inc. Elizabeth Webbing Mills  Dyehouse Elizabeth Webbing Mills  Healthtex Facility Glencairn Manufacturing Co. Greenhalgh Mills, Inc. Hope Webbing Microfibres, Inc. Murdock Webbing Providence Braid Co. R. I. Textile Co. Rochambeau Worsted Slater Finishing Co. Slater Dye Works, Inc. Slater Screen Print Corp. Tastex Corp. Union Wadding Co.

Providence, RI ( Field's Point) Worcester Co.

Rockford, IL  Rock River Water Reclamation District Cellusuede Products, Inc.

Sayreville, NJ  Middlesex County Utilities Authority J & J Worldwide Absorbant Products & Materials Research San Diego, CA  S. D. Metropolitan Wastewater Dept. Webb Designs California Dept. of Corrections 8 AMSA POTWs and Textile Users ( cont.)

San Francisco, CA  City & County Dept. of Public Works Southeast Water Pollution Control Plant Color Me, Inc. ( Simply Cotton) Hueline, Inc.

St. Louis, MO  Metropolitan St. Louis Sewer District Marchem Coated Fabrics St. Louis Dyeing & Processing Co.

St. Paul, MN  Metropolitan Waste Control Commission Minnesota Knitting Mills Bro Tex Corp.

Tacoma, WA  City of Tacoma Public Works & Sewer Utility Post Industrial Press Otto Screen Printing Sportswear Services, Inc.

Total POTWs = 31 Total Textile Users: 255  4 = 251 9 APPENDIX II 2 Parameters With POTW Local Limits and Monitored in 1993 at Textile Users Parameter 1 a 2 a 3 a b 4 a 5 a b BOD    s         TSS  s  s  s s    s s COD  s  s       s s Conductivity     s x       O& G total p x p  n  x   n x  pH n x n x n x x n x n x x Temp. p  p  p x x p  p   Chlorine ( resid.)   n          Sulfide     n        Perchloroethylene        n1     Cyanide n x n  n   n x n   Arsenic n x      n x    Boron   n          Cadmium n x n     n x n  x Chromium n x n  n   n x n  x Copper n x n  n   n x n  x Lead n x n  n   n x n  x Mercury n x n     n x n   Molybdenum        n x    Nickel n x n     n x n  x Selenium   n     n x    Silver n x n  n  x n x    Zinc n x n  n   n x n  x p = prohibition adopted from Section 403.5( b). n = numeric limit s = monitored as a basis for calculating POTW IU surcharge. x = monitored at textile user.  = local limit unspecified/ not monitored at textile user.

POTW at: 1. San Francisco, CA Monitors parameters at: a. 3 textile SIUs. 2. Phoenix, AZ Monitors parameters at: a. 1 textile IU2 3. San Diego, CA3 Monitors parameters at: a. Webb Designs b. California Dept. of Corrections 4. Denver, CO Monitors parameters at: a. Rocky Mountain Dye & Finishing 5. St. Paul, MN Monitors parameters at: a. Minnesota Knitting Mills, Inc. b. Bro Tex Corp.

1. Beyond the numeric limitation, the discharge of dry cleaning waste, including new and used perchloroethylene, is prohibited entirely by local limits of the Denver POTW. 2. Now reclassified as an IU, which cancels former SIU monitoring requirements ( 2X/ yr). 3. Textile users have been monitored for metals in the past, but such low levels were found that monitoring at textile users was discontinued. Silver is monitored at the prison only because of the photo lab. 10 Parameters With POTW Local Limits and Monitored in 1993 at Textile Users ( cont.)

Parameter 1 a b c d e f 2 a b BOD         s s TSS    x     s s COD           O& G total p x x   x  n x x TPH p x  x    n x x pH n x x x x x x n x x Temp. p          Phenols        p x  Ammonia N           TKN        n x x TTO          x VOCs p x x x       VOCs ( 601)           PCBs n x x x       Acids ( 625) n          Pesticides n1 x         Cyanide n       n x x Antimony n          Arsenic n       p x x Cadmium n   x   x p x x Chromium + 6 n   x   x p x x Chromium n   x   x p x x Copper n x x    x n x x Lead n  x x   x p x x Mercury p       p x x Molybdenum p      x    Nickel n      x p x x Silver n       p x x Zinc n x x x   x p x x p = prohibition adopted from Section 403.5( b). n = numeric limit s = monitored as a basis for calculating POTW IU surcharge. x = monitored at textile user.  = local limit unspecified/ not monitored at textile user.

POTW at: 1. Boston, MA ( Metropolitan) Monitors parameters at: a. International Paper ( Vertac Div) b. Draper Properties c. Synthon Industries d. TYCA Corp. e. TamFelt, Inc. f. EmTex, Inc. 2. Little Ferry, NJ Monitors parameters at: a. 3 textile SIUs b. 2 textile SIUs 1. Pesticides, as well as acrolein, Demeton, Lindane, Methoxychlor, etc., analyzed by EPA Method 608. 11 Parameters With POTW Local Limits and Monitored in 1993 at Textile Users ( cont.)

Parameter 1a 2a 3a 4a 5a BOD  s  s    s  s TSS  s  s    s  s COD  s  s      s O& G total n         O& G/ TPH n  n    n x n x pH n x n x   n x n x Temperature         nx Phenols       n   Ammonia N n     px   Sulfide nx         Sulfate nx         TTO       n1 x   VOCs         px Acids/ BN         p x Acids ( Method 625) n x         Solvents     n2     Cyanide n p n   nx Arsenic n p     nx Cadmium nx p n nx nx Chromium VI     n    n x Chromium nx p n nx nx Copper nx px n nx nx Lead n x p  n  n x n x Mercury n p   n nx Nickel n x p  n  n x n x Silver n  p    n x n x Zinc n x p x n  n x n x p = prohibition adopted from Section 403.5( b). n = numeric limit s = monitored as a basis for calculating POTW IU surcharge. x = monitored at textile user.  = local limit unspecified/ not monitored at textile user. POTW at: 1. Portland, OR Monitors parameters at: a. Columbia Wool Scouring Mills 2. Sayreville, NJ3 Monitors parameters at: a. Johnson & Johnson 3. Cuyahoga Heights, OH Monitors paramaters at: a. 2 textile SIUs. 4. Knoxville, TN Monitors parameters at: a. 2 textile SIUs. 5. Tacoma, WA Monitors parameters at: a. Sportswear Services, Inc. 1 other textile IU not monitored 1. TTO = Volatiles as defined by the Electroplating Categorical Pretreatment Standards. 2. Solvents = carbon tetrachloride, tetrachloroethylene, chlorobenzene, o chlorobenzene, cresols, cresylic acid, nitrobenzene, toluene, carbon disulfide, isobutanol, spent CFCs, MEK. 3. The surrounding towns monitor BOD, TSS, and COD at the confluence of their sewers with the POTW's trunk line. These measurements are used by the POTW to assess the towns' respective user charges. 12 Parameters With POTW Local Limits and Monitored in 1993 at Textile Users ( cont.)

Parameter 1 a 2 a b c 3 a b 4 a BOD  s  s s s  s s  s TSS  s  s s s  s s  s COD        s s   pH n x n x x x n x x n x Temp.       p x x   O& G total n x     n x x   Sulfide n x          Phenols       p 1 x x   TTO   n2 x        TICH p3           Cyanide n x n    n     Antimony       n  x   Arsenic n x n    n   n  Cadmium n x n x x x n   n  Chromium n x n x x x n   n  Copper n x n x x x n   n  Lead n x n x x x n     Molybdenum          n  Mercury p  n    n   n  Nickel n x n x x x n   n  Silver n x n x x x n     Zinc n x n x x x n   n

p = prohibition adopted from Section 403.5( b). n = numeric limit s = monitored as a basis for calculating POTW IU surcharge. x = monitored at textile user  = local limit unspecified/ not monitored at textile user.

POTW at: 1. City of Los Angeles, CA Monitors parameters at: a. 15 textile SIUs. 38 textile IUs not monitored. 2 textile users not monitored at present. ( not expected to violate local limits) 2. Orange County, CA Monitors parameters at: a. 3 textile SIUs. b. 6 textile SIUs. c. 2 textile SIUs. 1 textile IU not monitored. 3. St. Louis, MO Monitors parameters at: a. St. Louis Dyeing & Processing Co. b. Marchem Coated Fabrics Div. 4. Newark, NJ4 Monitors parameters at: a. 35 textile users.

1. Phenols ( total) monitored for screening. If response is significant, then analyze for phenol by 625. 2. TTO = Purgeable halocarbons ( EPA Method 601) and Purgeable aromatics ( EPA Method 602). 3. TICH = Total Identifiable Chlorinated Hydrocarbons. 4. Numeric limits for metals ( indicated by ' n') await approval by NJDEP. When approved, numeric limits for these metals will be added to the local limits and, at least initially, monitored at textile users. 13 Parameters With POTW Local Limits and Monitored in 1993 at Textile Users ( cont.)

Parameter 1 a b c d e f g h i j k l m n o p 2 a b c BOD                  n s s  TSS  s s s s s s s s s s s s s s s s n s s s TS                   x x x COD  s s s s s s s s s s s s s s s s n    pH n x x x x x x x x x x x x x x x x n x x x Temperature                  p x x x O& G petrol. p x x x x x x x     x x    n    Conductivity                  p x x x Phenols ( total)                  n    Sulfide p x x x x x x x x x x x      p  x  Phosphorus                  p x x x TCE p1           x          Cyanide n x        x        n    Arsenic n x x   x   x x  x      n    Cadmium n x x x   x  x x x x x x x x x n    Chromium n x x x x x  x x x x x x x x x x n    Copper n x x x x x x x x x x x x x x x x n    Lead n x x x x    x x x x x x x x x n    Mercury n x x   x  x x x  x  x    n    Nickel n x x x x  x x x x x x x x  x x n    Silver n x x x    x x x x x x x   x n    Zinc n x x x x  x  x x x x x x  x x n

p = prohibition adopted from Section 403.5( b). n = numeric limit ( maximum concentration). s = monitored as a basis for calculating POTW IU surcharge. x = monitored at textile user.  = local limit unspecified/ not monitored at textile user.

POTW at: 1. County of Los Angeles, CA Monitors parameters at 54 textile users. a. 5 textile SIUs e. 1 textile SIU i. 7 textile SIUs m. 1 textile SIU b. 6 textile SIUs f. 1 textile SIU j. 5 textile SIUs n. 1 textile SIU c. 10 textile SIUs g. 1 textile SIU k. 1 textile SIU o. 2 textile SIUs d. 1 textile SIU h. 7 textile SIUs l. 1 textile SIU p. 4 textile SIUs 11 textile users not monitored. 2. Columbus, GA Monitors parameters at 10 textile users: a. 7 textile SIUs b. 2 textile SIUs c. 1 textile SIU 1 textile user not monitored 1. TCE = tetrachloroethylene. This POTW does not routinely monitor organic priority pollutants at textile users. The TCE was detected in only one sample from several textile users selected to be checked for VOCs. 14 Parameters With POTW Local Limits and Monitored in 1993 at Textile Users ( cont.)

Parameter 1 a b c d e f g h i j k m n 2 a b c 3 a b BOD n s s s s s s s s s s s s s  s s s  s s TSS n x x x x x x x x x x x x x  s s s  s s COD n  x x   x x  x x x x         pH n x x x x x x x x x x x x x n x x x n x x O& G total p      x        n x  x n x x TPH p      x               Ammonia N p   x      x x  x         Phosphorus p          x x   n       Sulfide                   n   CTAS1 p   x         x         MBAS2 p            x         TCE3 p            x         PCE4 p             x        VOCs p          x           Cyanide n              n x   n   Arsenic n                  n   Cadmium n              n x x x n   Chromium n x x  x          n x x x n x  Copper n x x x  x         n x x x n   Lead n              n x x x n   Mercury n              n x x x n   Nickel n              n x x x n   Silver n                  n   Zinc n              n x x x n

p = prohibition adopted from Section 403.5( b) n = numeric limit s = monitored as a basis for calculating POTW IU surcharge x = monitored at textile user  = local limit unspecified/ not monitored at textile user POTW at: 1. Greenville, SC Monitors parameters at 20 textile users. a. 2 textile SIUs d. 1 textile SIU g. 3 textile SIUs j. 1 textile SIU n. 1 textile SIU b. 1 textile SIU e. 2 textile SIUs h. 4 textile SIUs k. 1 textile SIU c. 1 textile SIU f. 1 textile SIU i. 1 textile SIU m. 1 textile SIU 2. Chicago, IL Monitors parameters at: a. 1 textile SIU ( Western Piece Dyeing & Finishing) b. 1 textile SIU ( Industrial Coatings) c. 1 textile SIU ( Rubens & Marble) 3. Philadelphia, PA Monitors parameters at: a. 2 textile SIUs ( Anchor, Globe) b. 2 textile SIUs ( DV Wool Scour, General Felt)

1. CTAS = Cobalt Thiocyanate Active Substances ( nonionic surfactants). 2. MBAS = Methylene Blue Active Substances ( anionic surfactants). 3. TCE = 1,1,1 Trichloroethane ( methylchloroform). 4. PCE = Perchloroethylene ( Tetrachloroethylene). 15 Parameters With POTW Local Limits and Monitored in 1993 at Textile Users ( cont.)

Parameter 1 a b c d e f g h i j 2 a 3 a 4 a BOD n s s s s s s s s s s  s  s n s TSS n s s s s s s s s s s  s  s n s COD               s n  pH n x x x x x x x x x x n x n x n x Temperature                p  O& G total n  x  x x  x x  x n x n  n x TPH p  x  x    x   P  n    Phenols ( total)                n  Sulfate      x            Ammonia N              n x   VOCs p    x         n    Acids/ BN              n    TTO1 n   x      x x       TROPs2              n    TOPPOCs3              n    Cyanide n           n  n  n  Arsenic n           n  n  n  Cadmium n x x x x x      n  n x n  Chromium + 6              n  n  Chromium n x x x x x      n  n x n  Copper n x x x x x      n  n x n  Lead n x x x x x      n  n x n  Mercury n           n  n  n  Molybdenum              n    Nickel n x x x x x      n  n x n  Selenium n                 Silver n x x x x x      n  n  n  Zinc n x x x x x      n  n x n

p = prohibition adopted from Section 403.5( b) n = numeric limit s = monitored as a basis for calculating POTW IU surcharge x = monitored at textile user  = local limit unspecified/ not monitored at textile user POTW at: 1. East Providence, RI ( Bucklin Point) Monitors parameters at 18 textile users. a. 1 textile SIU d. 1 textile SIU g. 2 textile SIUs j. 2 textile SIU b. 2 textile SIUs e. 1 textile SIUs h. 1 textile SIU c. 5 textile SIUs f. 2 textile SIUs i. 1 textile SIU 2. Elizabeth, NJ Monitors parameters at: a. Fablok Mills, Inc. 3. Rockford, IL Monitors parameters at: a. Cellusuede Products, Inc. 4. Nashville, TN Monitors parameters at: a. 1 textile SIU ( Springs)

1. TTO = total " toxic" organics. A collective parameter for the organic priority pollutants, i. e., VOCs ( volatiles) and Acids/ Base Neutrals ( extractables) measured by EPA Methods 624 and 625. 2. TROPs = " Toxic reactive" organic pollutants. Specific chemicals defined in Appendix A of local limits. 3. TOPPOCs = Total organic priority pollutants of concern. Specific chemicals defined in Appendix B of local limits. 16 APPENDIX II 3 Flow Data for Textile Users Discharging to AMSA POTWs Average POTW/ Textile Users Flow, mgd POTW1a 300 Synthon Industries 0.0085 TYCA Corp. 0.0085 Emtex 0.011 Total from textile users 0.0280 0.009% POTW POTW1b 150 International Paper 0.0095 Draper Properties 0.085 Tamfelt 0.0005 Total from textile users 0.0950 0.06% POTW POTW2 135 Phoenix Dye Works 0.17605 Ohio Knitting 0.005 Total from textile users 0.181 0.13% POTW POTW3 19 Western Piece Dyers & Finishers 0.189 Industrial Coatings Group 0.224 Rubens & Marble 0.004 Total from textile users 0.417 2.2% POTW POTW4 28 Bibb Co. 0.030 Fieldcrest Mills  Broad. 0.614 Fieldcrest Mills  E& P 3.045 Swift Textiles  6th Ave. 0.342 Swift Textiles  Flatrock 0.700 Meritas Yarns 0.0036 Omi Georgia 0.00063 Swift Spinning Mills 0.0728 Wellington Sears  1st Ave 0.0042 Wellington Sears  Cusseta 0.015 Columbus Mills 1.010 Total from textile users 5.837 20.8% POTW 1. Boston, MA  Massachusetts Water Resources Authority. 1a. Deer Island POTW 1b. Nut Island POTW 2. Cuyahoga, OH  Southerly Water Pollution Control Facility 3. Chicago, IL  Metro. Water Reclamation District of Greater Chicago. 4. Columbus, GA  Columbus Water Works. 17 Flow Data for Textile Users Discharging to AMSA POTWs ( cont.)

Average POTW/ Textile Users Flow, mgd POTW5 160 Rocky Mountain Dye & Finishing 0.032 0.02% POTW POTW6 67 Fablok Mills 0.040 0.06% POTW POTW7a 20 Carisbrook Yarns 0.993 JPS Industrial Fabrics Dunean Front 0.041 JPS Industrial Fabrics Dunean Back 0.205 JPS Automotive Fabrics Parker 0.020 Judson 0.021 KM Fabrics 0.072 Krieger Textile 0.073 M Tex 0.073 Specialty Shearing & Dyeing 0.545 U. S. Finishing 0.849 Woven Electronics 0.182 Wunda Weve 0.322 Total from textile users 3.396 17.0% POTW POTW7b 0.35 Bibb Towels 0.031 8.8% POTW POTW7c 5.2 Cardinal Garmet Dye 0.012 0.2% POTW POTW7d 3.3 Greenville Finishing 0.160 JPS Automotive Fabrics Bleachery 0.077 JPS Automotive Fabrics Kuster 0.207 Orion Finishing 0.030 Total from textile users 0.474 14.3% POTW 5. Denver, CO  Metro Wastewater Reclamation District 6. Elizabeth, NJ  Joint Meeting of Essex & Union Counties. 7. Greenville, SC  Western Carolina Regional Sewer Authority 7a. Mauldin POTW 7b. Lakeside POTW 7c. Pelham POTW 7d. Taylor POTW 18 Flow Data for Textile Users Discharging to AMSA POTWs ( cont.)

Average POTW/ Textile Users Flow, mgd POTW7e 0.35 JPS Industrial Fabrics Slater 0.055 15.7% POTW POTW8 21 Appalachian Finishing Werk ( Mag.) 0.225 Appalachian Finishing Work ( Gill) 0.200 Total from textile users 0.425 0.02% POTW POTW9 76 Advanced Fibers 0.0052 Beacon Looms 0.0018 H& W Shoe Supplies 0.00025 Marijon Dyeing & Finishing 0.680 Spinnerin Yarn 0.250 Total from textile users 0.937 1.2% POTW POTW10a 16 Long Beach Dyeing & Finishing 0.098 0.6% POTW POTW10b 33 Formosa Dyeing & Finishing 0.060 SS Dyeing & Finishing 0.019 Tuftex Carpet Mills 0.700 Total from textile users 0.779 2.4% POTW POTW10c 13 Pomona Textile Co. 0.0405 0.3% POTW POTW10d 85 Bentley Mills 0.650 United Thread Manufacturing 0.003 Total from textile users 0.653 0.8% POTW 7e. Slater Marietta POTW 8. Knoxville, TN  Knoxville Utilities Board. 9. Little Ferry, NJ  Bergen County Utilities Authority. 10. Los Angeles, CA  L. A. Sanitation District. 10a. Long Beach  Wastewater Reclamation Plant. 10b. Los Coyotes  Wastewater Reclamation Plant. 10c. Pomona  Wastewater Reclamation Plant. 10d. San Jose Creek  Wastewater Reclamation Plant. 19 Flow Data for Textile Users Discharging to AMSA POTWs ( cont.)

Average POTW/ Textile Users Flow, mgd POTW10e 11 Artistic Dyers 0.0087 Rainbow Textile Co. 0.0095 Shing Jye Supplies 0.0005 Total from textile users 0.0187 0.2% POTW POTW10f ( Carson Joint WPCP, LA San. Dist.) 328 American International 0.100 Artesia Dyeing & Printing ( 13066) 0.017 Artesia Dyeing & Printing ( 12330) 0.0895 Atlas Carpet 0.00005 Cal Pacific Dyeing & Finishing 0.211 California Webbing Industries 0.016 Care Tex Industries 0.017 ChemTex Print USA 0.00967 Coloramerica Textile Processing 0.260 Colortex Dyeing & Finishing 0.720 Cotton Club 0.020 Delta Dyeing & Finishing 0.145 Downtown Dyers 0.010 E& J Dye House 0.060 EKPG 0.004 E. T. C. Carpet Mills 0.180 F& J Metro Dyeing 0.006 Factory Inc. 0.0185 Flamingo Textile Mills 0.0198 Giant Merchandising 0.001 Grace Kimmy Designs 0.0002 LA Dye & Print ( 12817) 0.010 LA Dye & Print ( 12818) 0.200 LA Airline Inc. 0.00015 LA Print Works 0.020 LA Dye & Wash Co. ( 12943) 0.037 LA Dye & Wash Co. ( 13074) 0.0001 Lorber Industries 0.600 Louie Bernard 0.0035 Pacific Combining 0.0025 Pacific Continental 0.450 Pacific Fabrics 0.090 10e. Whittier Narrows  Wastewater Reclamation Plant. 10f. Los Angeles Sanitation Dist.  Carson Joint Water Pollution Control Plant. 20 Flow Data for Textile Users Discharging to AMSA POTWs ( cont.)

Average POTW/ Textile Users Flow, mgd POTW10f ( continued) Pan Pacific Yarn 0.0015 PolyTex Thread Mills 0.011 Sumitex Prints of California 0.350 Spectrum Dyeing & Finishing 0.012 Sun Dyeing & Finishing 0.0038 Sung Do International 0.195 Texlon Corp. 0.017 Texollini Inc. 0.050 Tissurama Industries 0.970 Uni Hosiery Co. 0.015 US Boys Inc. 0.046 Western Dyeing & Finishing 0.778 WesternTex Industries 0.300 Total from textile users 6.066 1.85% POTW POTW11 232 Anaheim Mills 0.357 Chroma Systems Partners 0.350 Crazy Shirts 0.007 Dye Technique 0.029 Pharr Palomar 0.001 Royal Carpet 0.370 Saba Textiles 0.200 Sees Color Textile 0.300 US Dyeing & Finishing 0.400 Vans, Inc. 0.0006 Total from textile users 2.015 0.87% POTW POTW12 32.9 Springs Industries 0.250 0.76% POTW POTW13 227 Anchor Dyeing & Finishing 0.225 Delaware Valley Wool Scouring 0.011 General Felt Industries 0.001 Globe Dye Works 0.094 Total from textile users 0.331 0.15% POTW 10f. Los Angeles Sanitation Dist.  Carson Joint Water Pollution Control Plant. 11. Orange County, CA  O. C. Sanitation Districts 12. Nashville, TN  Metropolitan Water Services. 13. Philadelphia, PA  Northeast Water Pollution Control Facility 21 Flow Data for Textile Users Discharging to AMSA POTWs ( cont.)

Average POTW/ Textile Users Flow, mgd POTW14 150 Arizona Garment Finishers 0.0096 < 0.001% POTW POTW15 57 Columbia Wool Scouring 0.0502 0.09% POTW POTW16a 332 ABC Dye House 0.0549 Bruck Braid 0.010 California Dye House 0.0352 City Dyeing & Finishing 0.4257 Coast Arrow 0.0002 Colormax Industries 0.132 Coloring Button Dyers 0.0002 Color Master Garment Dyeing & Fin. 0.0016 Dara Inc. 0.0005 David S. Gibson 0.0017 Dixie Trimming Co. 0.0024 Double " A" Wash & Dye 0.170 DyeTech Corp. 0.0065 Dye to Match 0.0191 Fashion Art International 0.0005 Foid Garment Dyeing 0.0425 In LA California 0.0209 J& J Tee Shirts & Fashions 0.0021 Kesbaf Knitting Co. 0.0504 Koo's Manufacturing Co. 0.020 LA Dye Works 0.0002 LA Dye Works ( Rainbow) 0.2868 LA Dye & Print Works 0.2945 M& D Buttons & Lace Dyers 0.0002 Maria Kipp 0.0011 Matchmaster Inc. 0.0005 Matchmaster Dyeing & Finishing 0.697 MW Graphics 0.0001 Modern Button Co. of California 0.001 Only in USA 0.0012 Pico Dyeing & Finishing 0.0059 Pour le Bebe 0.0069 14. Phoenix, AZ 15. Portland, OR 16a. Hyperion Treatment Plant, City of Los Angeles, CA. 22 Flow Data for Textile Users Discharging to AMSA POTWs ( cont.)

Average POTW/ Textile Users Flow, mgd POTW16a ( continued) Rainbow Button 0.0001 S& A Button Dyers 0.0004 Sealmaster W. T. 0.0048 Sharon & Joyces Clothing 0.0012 SNS Brothers 0.0003 S& S Dyehouse 0.001 Super Yarn Mart 0.0072 Uni Hosiery 0.0057 Washington Garment Dyeing & Finish. 0.1068 Western Dye House 0.181 2.43 0.73% POTW POTW16b 20.3 A& H California 0.004 Almore Dye House 0.1389 Avi Levy 0.004 Caravan Fashion Enterprises 0.0008 Color Fabric Processing 0.094 New Hero 0.0067 0.2484 0.01% POTW POTW17 290 A& L Dyers 0.01 Apollo Dyeing & Finishing 0.078 Baltic Dyeing & Finishing 0.078 Champion Dyeing & Finishing 0.107 Columbia Textile Service 3.099 Como Textile Prints 0.274 Coral Dyeing & Finishing 0.26 Craft Textile Printing 0.242 Crestany Textile Processors 0.019 Dye Tex Corp. 0.499 E& W Textile Processors 0.06 Fairfield Textiles 0.046 International Veeling Corp. 0.092 Interstate Dyeing & Finishing 0.117 Leader Dyeing & Finishing 0.714 Manner Textile Processing 0.102 16a. Hyperion Treatment Plant, City of Los Angeles, CA. 16b. Glendale Treatment Plant, City of Los Angeles, CA. 17. Newark, NJ, Passaic Valley Sewerage Commissioners 23 Flow Data for Textile Users Discharging to AMSA POTWs ( cont.) Average POTW/ Textile Users Flow, mgd POTW17 ( continued) Messbrenner Prints 0.528 North Jersey Skein Dye 0.034 Paragon Dyeing & Finishing 0.055 Paterson Bleachery & Chemicals 0.051 Pauls Dyeing 0.043 Perennial Print 0.249 Poughkeepsie Finishing 0.706 Rainbow Dye & Finishing 0.116 Renco Finishing 0.07 Safer Textile Processing 0.338 Signature Cloth 0.249 Sunbrite Dye 0.111 Superior Dyeing Corp. 0.114 Thomas Henshall Silk Finishing 0.002 Thorn Inc. 0.139 Tico Dyeing & Finishing 0.27 Uni Trade Co. 0.015 United Veil Dyeing & Finishing 0.09 Zenith Dyeing & Finishing 0.133 Total from textile users 9.11 3.14% POTW POTW18 29 Cellusuede 0.040 0.14% POTW POTW19 75 Johnson & Johnson 0.015 0.02% POTW POTW20 180 Webb Designs < 0.0005 California Dept. of Corrections 0.014 Total from textile users 0.0145 < 0.0001% POTW POTW21 21.8 Crown Yarn Dye 0.110 Elizabeth Webbing, Health Tex 0.00001 Elizabeth Webbing Mills 0.240 Glencairn Mfg. 0.00001 17. Newark, NJ  Passaic Valley Sewerage Commissioners 18. Rockford, IL  Rock River Water Reclamation District. 19. Sayreville, NJ  Middlesex County Utilities Authority 20. San Diego, CA  Point Loma Plant. 21. East Providence, RI  Bucklin Point Facility 24 Flow Data for Textile Users Discharging to AMSA POTWs ( cont.) Average POTW/ Textile Users Flow, mgd POTW21 ( cont.) Conrad Jarvis Corp. 0.0000211 Greenhalgh Mills 0.105 Hope Webbing 0.017 Microfibres 0.167 Murdock Webbing 0.020 Providence Braid Co. 0.00003 R. I. Textile Co. 0.0012 Rochambeau Worsted 0.116 Slater Finishing 0.0226 Slater Dye Works 0.2805 Slater Screen Print 0.264 Tastex Corp. 0.0003 Union Wadding Co. 0.040 Worcester Textile Co. 0.150 Total from textile users 1.544 7.0% POTW POTW22 67 Color Me ( Simply Cotton) 0.003 Hueline 0.009 Total from textile users 0.012 < 0.02% POTW POTW23 120 Marchem  Coated Fabrics Div. 0.0055 St. Louis Dyeing & Processing 0.013 Total from textile users 0.0185 0.015% POTW POTW24 235 Minnesota Knitting 0.0235 Bro Tex 0.010 Total from textile users 0.0335 0.01% POTW POTW25 23 Post Industrial Press 0.000276 Otto Screen Printing 0.000242 Total from textile users 0.000518 0.002% POTW 21. Providence, RI  Bucklin Point Facility 22. San Francisco, CA  Southeast Water Pollution Control Plant. 23. St. Louis, MO  Metropolitan St. Louis Sewer District. 24. St. Paul, MN  Metropolitan Waste Control Commission. 25. Tacoma, WA  Central Wastewater Treatment Plant. 25 Flow Data for Textile Users Discharging to POTW at Valdese, NC Average Textile Users Flow, mgd Valdese POTW 6.0  6.25 Alba Waldensian 0.16 Burke Mills 0.476 Carolina Mills 0.84 Dolly Hosiery 0.01 Kathy Hosiery 0.021 OMS Textiles 0.613 Valdese Manuf. ( Meridian) 0.846 Robinson Hosiery 0.034 Valdese Textiles 0.234 Valdese Weavers 0.312 Neuville Industries 0.116 Total from textile users 3.662 58.6% POTW Notes: Flow: Daily average 6  6.5 mgd ( 5.5 mgd, or 88%, is industrial wastewater). Valdese has a population of 3000. Number employed by textile users was not investigated.

Flow Data for Textile Users Discharging to POTW at Star, NC 1993 1994 Average Average Textile Users Flow, mgd Flow, mgd POTW 0.594 0.558 Clayson Knitting 0.0922 0.0881 Fruit of the Loom 0.2936 0.27035 Montgomery Hosiery Mills 0.0266 0.0278 Pine Hosiery Mills 0.0155 ( assumed) 0.0155 Total from textile users 0.4279 72% POTW 0.4018 72% POTW Notes: Flow: Design 0.6 mgd; Daily average 0.55  0.6 mgd ( 72% is industrial wastewater). Star, NC, has a population of only 200, but 2000 are employed at the four textile users. Thus, the community and surrounding area are heavily dependent on the textile users for employment. Special problem: Textile user discharges are saline (> 6000 mg/ L chloride). POTW discharges to a small stream with 7q10 approximating 0 cfs. For this reason, it has been required to use 99% treated effluent ( only 1% dilution allowed) in the WET, and has had trouble meeting this water quality standard in its NPDES permit. 26 APPENDIX II 4 Analyses of Textile User Discharges to POTW ( Bucklin Point) at East Providence, RI POTW Flow Capacity: 46 mgd; Current Average Daily Flow: 23 mgd Sampling Episode Parameter LL* 1 2 3 4 5 6 7 8 9 Cadmium 110       3  7 Chromium 2770         494 Copper 1200 40 32 770 1070 1610 1230 422 884 2640 Lead 690        28 215 Nickel 1620      20 12 16 648 Silver 400     70 40  16  Zinc 1670 230 150 480 460 370 220 334 315 1110 Sampling Episode 10 11 12 13 14 15 16 17 18 19 20 Copper 1160 69 880 680 530 850 300 530 380 800 280 21 22 23 24 25 26 27 28 29 30 31 Copper 220 900 730 390 530 500 840 530 460 950 560 32 33 34 35 36 37 38 39 40 41 42 Copper 1190 900 600 840 460 380 650 1110 1170 2260 1590 43 44 45 46 47 48 49 50 51 52 53 Copper 3820 560 3750 1180 2720 320 890 610 530 460 300 Sampling Episode Parameter 54 55 56 57 58 59 60 61 62 63 64 Cadmium  13  1  2     Chromium 68 14  93      Copper 361 500 175 190 8 79 152  33 1160 69 Lead          Nickel 45 138        Silver 67 4      40 46 Zinc 788 262 102 85 3 34 66 30 105 Code:  = not detected; Blank = metal not analyzed in episode. Concentration unit = ug/ L ( ppb) * Local limit, max. conc. ( 24 hr. composite sample).

Sampling Episodes: 1 53: Slater Screen Print Corp. ( 020 030 0697) 54 57: Crown Yarn Dye Co., Inc. 58 60: Rochambeau Worsted 61 64: Slater Dye Works ( 020 029 0697) 27 Analyses of Textile User Discharges to POTW at East Providence, RI ( cont.)

Sampling Episode Parameter LL* 1 2 3 4 5 6 7 8 9 10 11 Cadmium 110     4    1370 12  Chromium 2770 164 19 27 61 446 197 694  49 18 42 Copper 1200 90 22 40 30 247 232 296 220 7120 43 71 Lead 690 22    42  11  1100   Nickel 1620   80 140 40  4  680 379 22 Silver 400 51 2    7 42  200   Zinc 1670 56 5 600 620 502 456 407 65 5810 363 241 Sampling Episode Parameter LL* 12 13 14 15 16 17 18 19 20 21 22 Cadmium 110  7  1  7    Chromium 2770 40 15 56   236  50 88 Copper 1200 20 60 106 15 54 129 156 54 76 30 87 Lead 690  123  7  90   25 Nickel 1620 10 175 25  17 40    Silver 400    4 93 11    Zinc 1670 620 373 232 190 246 250 229 830 145 Sampling Episode Parameter LL* 23 24 25 26 27 28 29 30 31 32 Cadmium 110   20 20 Chromium 2770 100 100 180 130 100 110 120 310 390 170 Copper 1200 70 70 80 Lead 690 50 Nickel 1620  70  Silver 400    Zinc 1670 130 80 60 70 90 140 280 110 30 160 Code:  = not detected; Blank = metal not analyzed that episode. Concentration unit: ug/ L ( ppb) * Local limit, maximum concentration ( 24 hr. composite sample)

Sampling Episodes: 1 5: Microfibres, Inc. 6,7: Murdock Webbing 8,9: R. I. Textile Co. 10 14: Elizabeth Webbing Mills, Health Tex facility 15 21: Elizabeth Webbing Mills, dyehouse facility 22 32: Worcester Textile Co. ( discharges to Field's Point POTW in Providence, RI and is subject to different local limits). 28 Analyses of Textile User Discharges to POTW at Valdese, NC Sampling Episode Parameters LL1 1a 1b 1c 1d Chloroform x  14

Di( 2 ethylhexyl) phthalate x *

Antimony x 16890 940 1000 550 Arsenic 100 2    Cadmium 200  4 2  Chromium 500 170 160 8 203 Copper 500 4080 602 220 397 Lead 100 200 80 20  Mercury 100 1 1  0.4 Nickel 250 320 20 20 40 Silver 30     Zinc 500 5200 2160 620 80 Code: x = unspecified; * = detected2; () = not detected. Concentration = ug/ L ( ppb)

Textile User: 1. Burke Mills3 1a. 1990  Lab: Burlington Research Labs, Blue Ridge Labs ( metals) 1b. 1991  Lab: Blue Ridge Labs 1c. 1992  Lab: Blue Ridge Labs 1d. 1993  Lab: Blue Ridge Labs 1. Local limit, maximum concentration allowed. 2. The textile user's process was not the source of phthalates detected in these wastewater samples. The phthalates detected are attributable to contamination of sample ( by use of plasticized tubing in sampling device), and/ or laboratory procedures ( leaching from anhydrous sodium sulfate used to dry extract). Phthalate concentrations reported by the lab are not given here, so that statistical summaries will not inadvertently include data that would inaccurately characterize the textile user's process wastewater. 3. Reduction in metal concentrations over time are attributable to a more judicious use of progressively higher quality process chemicals, and switch to non metallized dyes.

Source of metals:

Zinc salts were used as a dyeing auxillary chemical. Lower concentration of zinc reflects a switch to other metal salts. Also, zinc ( up to 1 ppm) is often added to potable water supplies to inhibit corrosion in pumps and in the distribution system.

Antimony is applied to fabric as a flame retardant. Only those textile facilities that so treat fabrics are a source of this metal. This is the reason the metal is seldom detected in textile user wastewater. 29 Analyses of Textile User Discharges to POTW at Valdese, NC. ( cont.)

Sampling Episode Parameters LL1 1a 1b 1c 1d 2a Acrolein x  527    Chloroform x 1100  203 838 9 Naphthalene x      Di( 2 ethylhexyl) phthalate x * *

Antimony x    204 Arsenic 100   27  Beryllium x   100  Cadmium 200   40  Chromium 500   120  Copper 500   30 31 Lead 100   160  Mercury 100     Nickel 250   140  Selenium x   8  Silver 30   20  Zinc 500   100 109 Code: x = unspecified; * = detected2; () = not detected. Concentration = ug/ L ( ppb)

Textile Users: 1. Neuville Industries3 1a. 1990  Lab: PACE 1b. 1991  Lab: Bold Research Labs 1c. 1992  Lab: 1d. 1993  Lab:

2. Valdese Textiles 2a. 1991  Lab: PACE 1. Local limit, maximum concentration allowed. 2. The textile user's process was not the source of phthalates detected in these wastewater samples. The phthalates detected are attributable to contamination of sample ( by use of plasticized tubing in sampling device), and/ or laboratory procedures ( leaching from anhydrous sodium sulfate used to dry extract). Phthalate concentrations reported by the lab are not given here, so that statistical summaries will not inadvertently include data that would inaccurately characterize the textile user's process wastewater. 3. Two different labs failed to detect metals in ' 90 and ' 91, but metals were detected in ' 92 by an unidentified lab. Since the ' 92 concentrations were below local limits, the POTW did not require analysis of metals in 1993. 30 Analyses of Textile User Discharges to POTW at Valdese, NC ( cont.)

Sampling Episode Parameters LL1 1a 1b 1c 1d 2a 2b 2c Chloroform x 24 7 29     Ethylbenzene x 33 18      Xylenes x 438

Naphthalene x 45 255 253 69    Di n butyl phthalate x  *      Di( 2 ethylhexyl) phthalate x    *

Antimony x   22   40 20 Arsenic 100 10 5    16 20 Cadmium 200 12  10 2 5 2 5 Chromium 500 14  10 10 3  Copper 500 53 33 85 37 220 74 536 Lead 100 152  20  20 10  Mercury 100    0.2 0.4 0.2  Nickel 250 40  8  20   Silver 30 15  5     Zinc 500 166 136 75 40 100 180 600 Concentration = ug/ L ( ppb) Code: x = unspecified; * = detected2; () = not detected Textile Users: 1. OMS Textiles3 1a. 1990  Lab: Water Technology and Controls 1b. 1991  Lab: WT& C ( metals), Burlington Research ( organics) 1c. 1992  Lab: AAES Labs 1d. 1993  Lab: Blue Ridge Labs 2. Valdese Weavers 2a. 1990  Lab: Dexter Corp 2b. 1991  Lab: Blue Ridge Labs 2c. 1992  Lab: Blue Ridge Labs 1. Local limit, maximum concentration allowed. 2. The textile user's process was not the source of phthalates detected in these wastewater samples. The phthalates detected are attributable to contamination of sample ( by use of plasticized tubing in sampling device), and/ or laboratory procedures ( leaching from anhydrous sodium sulfate used to dry extract). Phthalate concentrations reported by the lab are not given here, so that statistical summaries will not inadvertently include data that would inaccurately characterize the textile user's process wastewater. 3. In 1993, OMS Textiles was in bankruptcy. For this reason, the facility could not legally function under that name. Consequently, they submitted samples of wastewater for analysis under the name Quality Textile Finishers of America. 31 Analyses of Textile User Discharges to POTW at Valdese, NC. ( cont.)

Sampling Episode Parameters LL1 1a 2a 3a 4a 4b Chloroform x 4  23 5  Toluene x  7

Di n butyl phthalate x     * Di( 2 ethylhexyl) phthalate x *    *

Antimony x     5 Arsenic 100 12  2   Cadmium 200   6   Chromium 500 31 135 9 143 4 Copper 500 328 212 319 143 132 Lead 100 100  40  8 Mercury 100      Nickel 250 238  20 81 61 Silver 30      Zinc 500 367 60 120 66 145 Code: x = unspecified; * = detected2; () = not detected. Concentration = ug/ L ( ppb)

Textile Users: 1. Alba Waldensian 1a. 1990  Lab: Gen. Eng. Labs ( organics); PACE ( metals)

2. Adams Millis Drexel 2a. 1991  Lab: Research & Analytical Labs 3. Carolina Mills 3a. 1992  Lab: Blue Ridge Labs 4. Valdese Manufacturing 4a. 1991  Lab: 4b. 1992  Lab: PACE 1. Local limit, maximum concentration allowed. 2. The textile user's process was not the source of phthalates detected in these wastewater samples. The phthalates detected are attributable to contamination of sample ( by use of plasticized tubing in sampling device), and/ or laboratory procedures ( leaching from anhydrous sodium sulfate used to dry extract). Phthalate concentrations reported by the lab are not given here, so that statistical summaries will not inadvertently include data that would inaccurately characterize the textile user's process wastewater. 32 Analyses of Textile User Discharges to POTW at Star, NC Clayson Knitting Co. Average Flow: 0.0881 mgd = 15% of POTW's average flow.

1993 Sampling Episodes Parameter July August Sept. Oct. Nov. Dec.

BOD, mg/ L 167 90 179 153 324 195 67 COD, mg/ L 561 TSS, mg/ L 16 13 34 25 22 Total Solids, mg/ L 34 pH 9.4 8.4 9.2 9.0 O& G, mg/ L 15 41 28 37 44 Chloride, mg/ L 606 731 1040 822 1320 Conductance, umho 3660 3920 4760 4700 5880 Arsenic   6 6 Cadmium 0.6    Chromium 15    11  Copper 18 30 103 272 135 270 760 40 12 190 176 28 23 140 117 230 22 46 135 21 100 28 13 22 20 10 Lead 2 10 9 20  Mercury 0.2    Molybdenum 38 15 14 10  Zinc 443 180 447 186 277 240 467 195 17 177 188 274 17 242 128 248 204 162 277 320 215 277 249 257 126 Code:  = not detected; metal concentration = ug/ L ( ppb) 33 Analyses of Textile User Discharges to POTW at Star, NC Clayson Knitting Co. ( cont.)

1994 Sampling Episodes Parameter January February March April May June BOD, mg/ L 187 367 187 246 165 248 TSS, mg/ L 29 20 34 11 20 32 pH 9.7 9.2 10 10.6 9.4 8.4 O& G, mg/ L 16 12 25 11 28 Chloride, mg/ L 1030 849 829 749 768 722 Conductance, umho 5500 4230 4270 4240 4260 3800 Copper 110 40 280 310 80 50 Lead 10 5 6 9  19 Molybdenum 70      Nickel  5     Zinc 180 191 276 214 160 370 Code:  = not detected. Concentration of metals = ug/ L ( ppb)

Fruit of the Loom Average Flow: 0.27035 mgd = 45% of POTW's average flow.

1993 Sampling Episodes Parameters July August Sept. Oct. Nov. Dec.

BOD, mg/ L 190 184 292 352 353 271 COD, mg/ L 711 TSS, mg/ L 20 64 56 48 59 Total Solids, mg/ L 22 pH 7.8 7.8 7.8 9.0 7.4 5.6 O& G, mg/ L 42 106 54 59 23 Chloride, mg/ L 783 474 363 353 264 Conductance, umho 4230 3520 2900 3410 3280 Cadmium 1  0.6  Chromium 8 9 17 12 13 70 Copper 335 278 354 517 317 560 360 520 773 270 378 178 882 334 38 767 376 598 630 315 521 622 649 300 546 396 460 455 410 470 498 910 545 683 664 333 249 354 432 560 332 Lead  5 14   Mercury 0.3

Code:  = not detected. Concentration of metals = ug/ L ( ppb) 34 Analyses of Textile User Discharges to POTW at Star, NC Fruit of the Loom ( cont.)

1993 Sampling Episodes Parameters July August Sept. Oct. Nov. Dec.

Zinc 790 480 505 506 514 333 818 561 605 415 394 495 805 161 290 586 17601 338 440 514 360 520 806 377 549 507 464 752 562 526 568 586 370 789 743 367 393 505 607 804 469 1994 Sampling Episodes Parameters Jan. Feb. March April May June BOD, mg/ L 235 586 314 268 214 421 TSS, mg/ L 71 80 75 64 38 102 pH 7.9 7.2 7.7 7.3 7.4 O& G, mg/ L 25 27 13 27 Chloride, mg/ L 259 258 220 284 360 334 Conductance, umho 3110 2830 2910 3190 3410 3800 Chromium      140 Copper 290 280 350 250 520 560 Lead 4     8 Zinc 380 14201 16201 934 750 37001 Code:  = not detected. Concentration of metals = ug/ L ( ppb)

1. Zinc concentration spikes resulted from the use of zinc contaminated sample bottles by Burlington Research ( lab that performed the analyses). Upon resampling with bottles that were pre washed with acid, zinc analyzed at nominal levels. 35 Analyses of Textile User Discharges to POTW at Star, NC Montogmery Hosiery Mills Average Flow: 0.0278 mgd = 4.6% of POTW's average flow.

1993 Sampling Episodes Parameter July August Sept. Oct. Nov. Dec.

BOD, mg/ L 102 85 100 90 188 134 COD, mg/ L 409 TSS, mg/ L 8 26 16 7 6 Total Solids, mg/ L 2 pH 8.3 6.9 9.0 8.5 6.0 O& G, mg/ L 9 11 18 7 17 Chloride, mg/ L 1280 1530 988 1680 1500 Conductance, umho 4660 5810 4040 6390 5780 Arsenic   21 10 Cadmium     Chromium 22 7 11 25 69  Copper 150 50 20 160 120 70 Lead 8 33 7   Mercury 0.3    Zinc 181 181 162 65 93 448 1994 Sampling Episodes Parameters Jan. Feb. March April May June BOD, mg/ L 146 396 131 107 114 91 TSS, mg/ L 13 18 10 24 24 22 pH 9.5 7.0 7.4 8.0 7.7 7.3 O& G, mg/ L 24 30 21 3 10 Chloride, mg/ L 1870 1280 109 218 297 607 Conductance, umho 7210 4610 3840 3900 4550 3200 Copper 50 90 70 40 80 40 Zinc 250 133 409 70 80 120 Code:  = not detected. Concentration of metals = ug/ L ( ppb) 36 Analyses of Textile User Discharges to POTW at Star, NC ( cont.)

Pine Hosiery Mills Average Flow: 0.0155 mgd = 2.6% of POTW's average flow 1993 Sampling Episodes Parameter July August Sept. Oct. Nov. Dec.

BOD, mg/ L 13 58 12 104 33 72 COD, mg/ L 249 TSS, mg/ L 2 14 12 5 Total Solids, mg/ L 14 5 pH 7.4 7.4 8.2 7.6 7.4 O& G, mg/ L 4 40 39 23 13 Chloride, mg/ L 1300 1160 567 574 400 Conductance, umho 5030 4400 2440 2600 1700 Copper 40 70 70 90   Lead  3 9   Mercury 0.2    Zinc 78 190 257 165 116 88 1994 Sampling Episodes Parameter Jan Feb March April May June BOD, mg/ L 107 72 146 156 118 141 TSS, mg/ L 13 9 33 18 10 16 pH 8.2 7.6 9.4 9.5 6.0 8.7 O& G 9 6 5 1 29 Chloride, mg/ L 1360 95 995 2160 32 992 Conductance, umho 7400 568 4220 8090 553 3970 Copper 430   1280  30 Lead 2      Zinc 490 16901 34 65 120 50 1. Zinc spike resulted from the use of zinc contaminated sample bottle by Burlington Research ( lab that performed the analyses). Upon resampling with bottles that were pre washed with acid, zinc was analyzed at nominal levels.

Code:  = not detected. Concentration of metals = ugm/ L ( ppb) 37 APPENDIX III 1 Textile Mill NPDES Permits in the North Carolina APAM Database NC0000094 Cranston Print Works  Fletcher NC0000876 Cone Mills  Greensboro NC0001210 Monarch Hosiery Mills  Burlington NC0001376 Burlington Industries  Wake Forest NC0001406 Swift Textiles  Erwin NC0001627 National Spinning  Washington NC0001643 Fieldcrest Cannon  Eden NC0001961 WestPoint Pepperell  Hamilton NC0002305 Guilford Mills  Kenansville NC0003450 StevcoKnit Fabrics  Wallace NC0003522 WestPoint Pepperell  Elizabethtown NC0003867 United Piece Dye Works  Edenton NC0003913 Glen Raven Mills  Altamahaw NC0004120 Cleveland Mills  Lawndale NC0004235 Minnette Textiles  Grover NC0004243 American Thread  Charlotte NC0004286 Tuscarora Yarns  China Grove NC0004391 Grover Industries  Grover NC0004405 Cone Mills  Cliffside NC0004618 WestPoint Pepperell  Lumberton NC0004812 Stowe Pharr Mills  McAdenville NC0005312 Chatham Manufacturing  Elkin NC0005479 Fieldcrest Cannon  Laurel Hill NC0005487 Fieldcrest Cannon  Salisbury NC0005762 WestPoint Pepperell  Wagram NC0006025 Burlington Industries  Forest City NC0006190 Delta Mills  Maiden NC0025135 Huffman Finishing  Granite Falls NC0034860 Schneider Mills  Taylorsville NC0043320 Burlington Industries  Cordova 38 APPENDIX III 2 North Carolina Annual Pollutant Analysis Monitoring ( APAM) Data Sampling Episodes Parameters 1a 1b 1c 1d 2a 2b 2c 2d 2e Chloroform      17 16 12  Dibromochloromethane      5    Methylene chloride    9

Di( 2 ethylhexyl) phthalate  x x x x x x x x Di n butyl phthalate       x x

Antimony  330        Cadmium      7    Chromium 17         Copper 116 94 69 47 40 20   4 Mercury  0.2     0.2  0.6 Nickel     40     Zinc 27 72 22 37 100 21

Concentration unit: ug/ L ( ppb) Codes: x = detected, but attributable to sample contamination. () = not detected above " quantitation limit target" concentration specified in the APAM reporting form.

1. NC 0004243 Plant: American Thread  Charlotte 1a. 1989  Lab: Environmental Testing 1b. 1991  Lab: Commonwealth Labs of SC, Greenville, SC. 1c. 1992  Lab: Pace Labs, Asheville, NC. 1d. 1993  Lab: Pace Labs 2. NC 0004286 Plant: Tuscarora Yarns  China Grove ( Fieldcrest Cannon, Kannapolis, NC) 2a. 1988  Lab: EMS Labs, Charlotte, NC. 2b. 1989  Lab: Burlington Research, Burlington, NC 2c. 1990  Lab: Burlington Research 2d. 1991  Lab: Burlington Research 2e. 1992  Lab: Burlington Research Notes: Anhydrous sodium sulfate used to dry the solvent extract. Received in plastic jars, anhydrous sodium sulfate often has plasticizer adhering to its surface. Unless precautions are taken to remove the phthalates by prewashing with solvent and/ or by baking, phthalates will leach into the concentrated extract. Other sources of phthalate contamination are: use of plasticized tubing in the automatic sampler; and heavily plasticized rubber gloves that may be worn by sampling personnel. The plant admitted having used Tygon ( plasticized) tubing in the automatic sampler in 1992 ( 2e), which could account for phthalates found in samples previous to 1992. In 1988 ( 2a), 32 ppb di( 2 ethylhexyl) phthalate was reported in the sample, but 66 ppb was found in the blank! The blank was obtained by drawing reagent water through the sampling pump prior to the commencement of sampling. In 1a, the detection limit for the base/ neutral analytes was 100 ug/ L ( sample diluted because of interference), which may be the reason phthalates were not detected in this sample. In 1c, di( 2 ethylhexyl) phthalate was footnoted as a " possible laboratory contaminant." 39 North Carolina APAM Data ( cont.)

Sampling Episodes Parameters 1a 1b 1c 2a 2b 2c 2d 3a 3b 3c Bromodichloromethane  9         Chloroform 54 660 16   5     1,1,1 Trichloroethane  7         Trichloroethylene          24 Di( 2 ethylhexyl) phthalate  x        x Di n butyl phthalate  x        x 1,2,4 Trichlorobenzene 30 540

Antimony         51  Arsenic  20 20        Cadmium 10          Chromium  100 5 260 320 980 470    Copper  160 190  10 30 20 240 220 360 Lead 70  8 11  14     Mercury     1.1 0.7  0.3  0.4 Nickel 50  52 19       Zinc  88 139 36 31 172 142 219 46 53 Concentration unit: ug/ L ( ppb) Codes: x = detected, but attributable to sample contamination. () = not detected above " quantitation limit target" concentration specified in the APAM reporting form.

1. NC 0004235 Plant: Minnette Textiles  Grover 1a. 1988  Lab: Burlington Research 1b. 1990  Lab: Burlington Research 1c. 1992  Lab: HydroLogic, Asheville, NC/ Morrisville, NC 2. NC 0001210 Plant: Monarch Hosiery Mills  Burlington 2a. 1989  Lab: Burlington Research, Burlington, NC 2b. 1990  Lab: Burlington Research 2c. 1991  Lab: Burlington Research 2d. 1992  Lab: Burlington Research 3. NC 0004120 Plant: Cleveland Mills  Lawndale 3a. 1990  Lab: Burlington Research, Burlington, NC. 3b. 1991  Lab: Burlington Research 3c. 1992  Lab: Burlington Research Notes: 1,2,4 trichlorobenzene ( TCB) is used as a carrier solvent for disperse dyes. Although it was not identified in 1c ( 1992) when analyzed by a different lab, it is also possible that the plant discontinued the use of the product that was the source of TCB. The source of chloroform and bromodichloromethane is likely to be the potable water supply. 40 North Carolina APAM Data ( cont.)

Sampling Episodes Parameters 1a 1b 1c 1d 2a 2b 2c 2d Chloroform     20    Ethylbenzene        88 Methylene chloride 26        Toluene    12    17 1,1,2 Trichloroethane        13 Di( 2 ethylhexyl) phthalate   x      Di n butyl phthalate   x

Arsenic 17        Cadmium  6   2.5    Chromium  5 80  100  210 160 Copper 1100 170 200 240 24  30 50 Lead  90   5   20 Mercury 0.6 5.4  0.3    0.6 Nickel     19   20 Zinc 62 71 59 36 70  103 144 Concentration unit: ug/ L ( ppb) Codes: x = detected, but attributable to sample contamination. () = not detected above " quantitation limit target" concentration specified in the APAM reporting form.

1. NC 0004618 Plant: WestPoint Pepperell  Lumberton 1a. 1987  Lab: Oxford Labs, Wilmington, NC 1b. 1989  Lab: Burlington Research, Burlington, NC 1c. 1990  Lab: Burlington Research 1d. 1992  Lab: Southern Testing & Research Labs, Wilson, NC 2. NC 0004812 Plant: Stowe Pharr Mills  McAdenville 2a. 1989  Lab: EMS Labs, Charlotte, NC 2b. 1990  Lab: Par Labs, Charlotte, NC 2c. 1991  Lab: Par Labs 2d. 1992  Lab: Par Labs 41 North Carolina APAM Data ( cont.)

Sampling Episodes Parameters 1a 2a 2b 2c 3a Methylene chloride 12

Di( 2 ethylhexyl) phthalate    x x Di n butyl phthalate

Antimony  * *  580 Arsenic  * *   Cadmium 6 * *   Chromium  * * 6 96 Copper 70 * * 45 290 Lead 90 * *   Nickel  * * 50  Zinc 128 * * 40 90 Concentration unit: ug/ L ( ppb) Codes: x = detected, but attributable to sample contamination. () = not detected above " quantitation limit target" concentration specified in the APAM reporting form. * = no data reported 1. NC 0004391 Plant: Grover Industries  Grover 1a. 1987  Lab: Burlington Research, Burlington, NC 2. NC 0005762 Plant: WestPoint Stevens (' 94)  Wagram ( J. P. Stevens > WestPoint Pepperell in ' 89) 2a. 1989  Lab: Microbac Environmental Lab, Fayetteville, NC 2b. 1991  Lab: Microbac Environmental Lab 2c. 1993  Lab: Microbac Environmental Lab 3. NC 0002305 Plant: Guilford Mills  Kenansville 3a. 1993  Lab: Heritage Labs 42 North Carolina APAM Data ( cont.)

Sampling Episodes Parameters 1a 1b 1c 1d 1e 2a 2b 3a 3b 3c Bromodichloromethane          18 Chloroform         18 9 Dibromochloromethane          16 Methylene chloride 15       11

Di( 2 ethylhexyl) phthalate x x x x x x  x   Di n octyl phthalate           Di n butyl phthalate  x     x  x x Antimony 830 380 520 330 321 300  300 24 46 Arsenic   11  26   13 26  Cadmium  3   3.5 5  8   Chromium 194 220 120 149 192  10  7  Copper 117 88 180 79 72 20 30  80 90 Lead   170   90  160   Mercury     0.5  0.2    Nickel  22 70        Zinc 76 150 100 39 58 51 20 141 15 73 Concentration unit: ug/ L ( ppb) Codes: x = detected, but attributable to sample contamination. () = not detected above the " quantitation limit target" concentration specified in the APAM reporting form.

1. NC 0005312 Plant: Chatham Manufacturing  Elkin 1a. 1988  Lab: CompuChem Labs ( sent data to Radian R& A) 1b. 1989  Lab: Radian Research & Analytical Labs, Kernersville, NC 1c. 1990  Lab: Radian R& A Labs 1d. 1991  Lab: Radian R& A Labs 1e. 1992  Lab: Radian R& A Labs 2. NC 0005479 Plant: Fieldcrest Cannon  Laurel Hill 2a. 1990  Lab: EnviroTech Mid Atlantic, Blacksburg, VA ( Virginia Tech Research Center) 2b. 1992  Lab: Burlington Research, Burlington, NC 3. NC 0005487 Plant: Fieldcrest Cannon  Salisbury ( North Carolina Finishing) 3a. 1990  Lab: EnviroTech Mid Atlantic, Blacksburg, VA 3b. 1991  Lab: Burlington Research, Burlington, NC 3c. 1992  Lab: Burlington Research 43 North Carolina APAM Data ( cont.)

Sampling Episodes Parameters 1a 1b 1c 1d 2a 2b 2c 2d 2e Bromomethane   85       Dibromochloromethane  7

Di( 2 ethylhexyl) phthalate  x   x x    Di n butyl phthalate       x

Antimony     300 187    Arsenic     18 40 31 74  Chromium 22 38 30 50   5   Copper 7 17   15 110  160 90 Mercury       1   Nickel 20         Zinc 50 54 57 79 21 71 24 28 13 Concentration unit: ug/ L ( ppb) Codes: x = detected, but attributable to sample contamination. () = not detected above the " quantitation limit target" concentration specified in the APAM reporting form.

1. NC 0006025 Plant: Burlington Industries  Forest City ( J. C. Cowan plant) 1a. 1989  Lab: EMS Labs, Charlotte, NC 1b. 1990  Lab: Pace Labs, Tampa, FL 1c. 1991  Lab: Pace Labs, Asheville, NC 1d. 1992  Lab: Pace Labs 2. NC 0006190 Plant: Delta Mills  Maiden 2a. 1989  Lab: EMS Labs, Charlotte, NC 2b. 1990  Lab: Burlington Research, Burlington, NC 2c. 1991  Lab: Burlington Research 2d. 1992  Lab: Burlington Research 2e. 1993  Lab: Burlington Research Note: Phthalates absent in 2d ( 1992) and 2e ( 1993). After studying the phthalate contamination problem in 1991, this lab began routinely prewashing ( hexane/ methylene chloride) the anhydrous sodium sulfate before using it to dry the solvent extract of the wastewater sample. 44 North Carolina APAM Data ( cont.)

Sampling Episodes Parameters 1a 1b 1c 1d 1e 2a 2b 2c 2d 2e Methylene chloride  13

Di( 2 ethylhexyl) phthalate x  x x       Di n octyl phthalate x          Di n butyl phthalate     x

Antimony       320    Arsenic      20 47 14 27 36 Cadmium      16 14    Chromium      74 23    Copper  100 20 196 137 27 12  9  Lead      40     Mercury       0.3    Nickel    25  22 42    Silver      10     Zinc  160  41 92 70 41 39 49 18 Concentration unit: ug/ L ( ppb) Code: x = detected, but attributable to sample contamination. () = not detected above the " quantitation limit target" concentration specified in the APAM reporting form.

1. NC 0001376 Plant: Burlington Industries  Wake Forest 1a. 1987  Lab: Industrial & Environmental Analysts ( IEA), RTP, NC 1b. 1989  Lab: IEA 1c. 1990  Lab: IEA 1d. 1991  Lab: Research & Analytical Labs 1e. 1992  Lab: Research & Analytical Labs 2. NC 0001406 Plant: Swift Textiles  Erwin 2a. 1989  Lab: " 37724" ? 2b. 1990  Lab: " 37724" ? 2c. 1991  Lab: Chemical & Environmental Technology, RTP, NC 2d. 1992  Lab: C & E Technology 2e. 1993  Lab: C & E Technology 45 North Carolina APAM Data ( cont.)

Sampling Episodes Parameters 1a 1b 2a 2b 3a 3b 4a 4b 4c Bromodichloromethane     10     Chloroform 6    25   11  1,1,1 Trichloroethane 106 310

Di( 2 ethylhexyl) phthalate   x  x  x x  Di n octyl phthalate     x     Di n butyl phthalate       x

Arsenic       190 44 106 Cadmium     6  4   Chromium   100  33  5   Copper 230 40 110 170 65 7  50 40 Lead 20    26     Mercury 0.4   0.3    0.6 3.4 Nickel     27   11  Silver       7 50  Zinc 665 161 43 29 275 18 427 89 26 Concentration unit: ug/ L ( ppb) Codes: x = detected, but attributable to sample contamination. () = not detected above the " quantitation limit target" concentration specified in the APAM reporting form.

1. NC 0003913 Plant: Glen Raven Mills  Altamahaw 1a. 1991  Lab: Burlington Research, Burlington, NC 1b. 1992  Lab: Burlington Research 2. NC 0003522 Plant: WestPoint Pepperell  Elizabethtown 2a. 1990  Lab: Burlington Research, Burlington, NC 2b. 1991  Lab: Southern Testing & Research Labs, Wilson, NC 3. NC 0001627 Plant: National Spinning  Washington 3a. 1987  Lab: Environment 1, Greenville, NC 3b. 1992  Lab: James R. Reed, Newport News, VA 4. NC 0004405 Plant: Cone Mills  Cliffside 4a. 1990  Lab: Burlington Research, Burlington, NC 4b. 1991  Lab: Burlington Research 4c. 1992  Lab: Burlington Research Notes: In Plant 1, the methylchloroform may have been used as a solvent, or may have had some other use, such as a dye carrier. In Plant 3, phthalates were detected in 1987 ( 3a), but not in 1992 ( 3b) by a different lab. In the interim, the source of phthalate contamination ( sodium sulfate) had become widely recognized. 46 North Carolina APAM Data ( cont.)

Sampling Episodes Parameters 1a 1b 1c 2a 2b 2c 2d 3a 3b 3c Bromodichloromethane         27 14 Bromoform         8  Chloroform        8 19 37 Dibromochloromethane         24 5 Di( 2 ethylhexyl) phthalate x x x   x x    Di n butyl phthalate      x  x x x Antimony     380    52  Arsenic    10    10  22 Cadmium     8 2     Chromium 5   60 8   9   Copper 40 20 80 162 340 280 330 140 170 120 Lead     110      Nickel      10    9 Selenium     15      Zinc 293 99 108 952 502 42 30 42  67 Concentration unit: ug/ L ( ppb) Codes: x = detected, but attributable to sample contamination. () = not detected above the " quantitation limit target" concentration specified in the APAM reporting form.

1. NC 0001643 Plant: Fieldcrest Cannon  Eden 1a. 1989  Lab: Burlington Research, Burlington, NC 1b. 1991  Lab: Burlington Research 1c. 1992  Lab: Burlington Research 2. NC 0001961 Plant: WestPoint Pepperell  Hamilton 2a. 1988  Lab: Oxford Labs, Wilmington, NC 2b. 1989  Lab: Burlington Research, Burlington, NC 2c. 1990  Lab: Burlington Research 2d. 1992  Lab: Southern Testing & Research Labs, Wilson, NC 3. NC 0003450 Plant: Stevcoknit Fabrics  Wallace 3a. 1990  Lab: Burlington Research, Burlington, NC 3b. 1991  Lab: Burlington Research 3c. 1992  Lab: Burlington Research 47 North Carolina APAM Data ( cont.)

Sampling Episodes Parameters 1a 1b 1c 1d 1e 2a 2b 2c 2d Methylene chloride        *  Toluene  6        Tetrachloroethylene  81        Trichlorofluoromethane        *

Di( 2 ethylhexyl) phthalate        x x Di n butyl phthalate    x x

Antimony 380         Arsenic 67         Cadmium 15 3       5 Chromium  13  7      Copper 150 170 250 79 110 60  105  Lead 100       31  Mercury  0.3 0.7 0.9     0.4 Nickel 50 11     76 73 31 Selenium 5         Silver  7 10      7 Zinc 167 89 113 94 84 190  268 416 Concentration unit: ug/ L ( ppb) Codes: x = detected, but attributable to sample contamination. () = not detected above the " quantitation limit target" concentration specified in the APAM reporting form. * = detected in method blank.

1. NC 0003867 Plant: United Piece Dye Works  Edenton 1a. 1988  Lab: Burlington Research, Burlington, NC 1b. 1990  Lab: Burlington Research 1c. 1991  Lab: Burlington Research 1d. 1992  Lab: Burlington Research 1e. 1993  Lab: Burlington Research 2. NC 0034860 Plant: Schneider Mills  Taylorsville 2a. 1989  Lab: General Engineering Lab ( Environmental Testing) 2b. 1990  Lab: Pace 2c. 1991  Lab: Hydro Analytical Labs 2d. 1992  Lab: Industrial & Environmental Analysts ( IEA), RTP, NC 48 North Carolina APAM Data ( cont.)

Sampling Episodes Parameters 1a 1b 1c 2a 2b 2c Bromodichloromethane   14    Chloroform 9 20 48

Di n butyl phthalate   x

Antimony     170  Arsenic 60 78 10 15  42 Cadmium    4   Chromium 16  6 17 40  Copper 90 50 20 69 480 140 Lead     40  Mercury 1.4   0.2   Nickel 20   35 50  Silver    6 100  Zinc 119 1240 680 112 890 320 Concentration unit: ug/ L ( ppb) Codes: x = detected, but attributable to sample contamination. () = not detected above the " quantitation limit target" concentration specified in the APAM reporting form.

1. NC 0025135 Plant: Huffman Finishing  Granite Falls 1a. 1990  Lab: Burlington Research, Burlingtonl, NC 1b. 1991  Lab: Burlington Research 1c. 1992  Lab: Burlington Research 2. NC 0000094 Plant: Cranston Printworks  Fletcher 2a. 1989  Lab: CompuChem 2b. 1992  Lab: Pace 2c. 1993  Lab: Pace 49 North Carolina APAM Data ( cont.)

Sampling Episodes Parameters 1a 1b 1c 1d 2a 2b 2c 2d Methylene chloride  14       1,1,1 Trichloroethane 11

Di( 2 ethylhexyl) phthalate x x  x x   x Di n butyl phthalate x    x  x x Butylbenzyl phthalate  x

Antimony    49     Arsenic      180 88 17 Chromium 7    8 5   Copper 20 10 10 10 51 10 10 10 Lead     38 10   Mercury    0.7     Nickel     44    Silver 9    5    Zinc 50 72 56 54 70 70 44 61 Concentration unit: ug/ L ( ppb) Codes: x = detected, but attributable to sample contamination. () = not detected above the " quantitation limit target" concentration specified in the APAM reporting form.

1. NC 0043320 Plant: Burlington Industries  Cordova 1a. 1989  Lab: Burlington Research 1b. 1990  Lab: Burlington Research 1c. 1991  Lab: Burlington Research 1d. 1992  Lab: Burlington Research 2. NC 0000876 Plant: Cone Mills  Greensboro 2a. 1989  Lab: Cone Mills Technical Center 2b. 1990  Lab: AquaTech Environmental Consultants 2c. 1991  Lab: Burlington Research 2d. 1992  Lab: Burlington Research Notes: Phthalates were generally not detected after labs began pre washing or baking the anhydrous sodium sulfate used to dry the solvent ( methylene chloride) extract. However, some plants were still using Tygon tubing with their compositing samplers. 50 APPENDIX III 3 Validated1 NPDES Permits from PCS Alabama AL0001627 Avondale Mills  Sylacauga AL0002968 WestPoint Stevens ( Pepperell)  Opelika AL0021997 Masland Carpets  Atmore Arkansas AR0000892 Burlington Industries  Monticello AR0045101 Fruit of the Loom  Mississippi Co.

Arizona AZ0022659 Bisbee Douglas Int'l Airport  Douglas Georgia GA0000060 Rabun Apparel  Rabun Gap GA0000213 Thomaston Mills  Thomaston GA0000345 Lindale Manuf.  Lindale GA0000850 Galey & Lord  Shannon GA0001791 Chicopee  Hall Co. GA0002038 Coats America  Stephens Co. GA0002224 Bibb Co.  Monroe Co. GA0002712 Jefferson Mills  Jackson Co. GA0003115 William Carter  Barnesville GA0003280 King Finishing  Screven Co. GA0003409 Dundee Mills  Spaulding Co. GA0003697 Mohawk Commercial Carpets  Laurens Co. GA0003760 Forstmann  Laurens Co. GA0003778 Forstmann  Louisville GA0024104 Fieldcrest Cannon  Lyerly Kentucky KY0002445 Jockey Int'l  Carlisle Maine ME0000116 Cascade Woolen Mill  Oakland ME0001902 Guilford of Maine  Guilford ME0002526 Robinson Manuf.  Oxford Massachusetts MA0001538 Guilford Industries  Douglas MA0003697 Veratec  Griswoldville MA0004171 Worcester Spinning & Finishing  Leicester MA0005355 Theave Inc.  Norton Mississippi MS0000876 Denton Mills  New Albany MS0001848 Burlington Denim  Stonewall MS0035882 Kimberly Clark  Corinth MS0047759 Greenville Manuf.  Greenville New Jersey NJ0004324 Fiber Technology Group  Buena ( Landisville) NJ0004901 Oxford Textile  Oxford 1. Selected from 413 textile ( SIC 22) NPDES permits extracted from PCS, 7/ 8/ 93. Validation means these permits were issued for control of pollutant parameters in textile process wastewater. 51 Validated NPDES Permits from PCS ( cont.)

North Carolina NC0000094 Cranston Print Works  Fletcher NC0000817 Wilmington Corp.  Wilmington NC0000876 Cone Mills  Greensboro NC0001210 Monarch Hosiery  Altamahaw NC0001376 Burlington Industries  Wake Forest NC0001406 Swift Textiles  Erwin NC0001627 National Spinning  Washington NC0001643 Fieldcrest Cannon  Eden ( Source: APAM data, not in PCS under SIC 22__) NC0001651 Culp Inc.  Guilford Co. NC0001961 WestPoint Pepperell  Hamilton NC0002305 Guilford Mills  Kenansville NC0003450 Stevcoknit Fabrics  Wallace NC0003522 WestPoint Stevens ( Pepperell)  Elizabethtown NC0003867 U. S. Piece Dye Works  Edenton NC0003913 Glen Raven Mills  Altamahaw NC0004120 Cleveland Mills  Lawndale NC0004235 New Minette Textiles  Grover NC0004243 Coats American  Charlotte NC0004286 Fieldcrest Cannon  China Grove NC0004391 Grover Industries  Tryon NC0004405 Cone Mills  Cliffside ( Source: APAM data, not in PCS under SIC 22__) NC0004618 WestPoint Pepperell  Lumberton NC0004812 Stowe Pharr Mills  McAdenville NC0005312 Chatham Manuf. Acquisition Corp.  Elkin NC0005355 Surratt Hosiery Mill  Denton NC0005479 Fieldcrest Cannon  Laurel Hill NC0005487 Fieldcrest Mills  Spencer NC0005762 J. P. Stevens  Wagram NC0006025 Burlington Industries  Forest City NC0006033 JPS Autoproducts  Cramerton ( Gaston Co.) NC0006190 Delta Mills  Maiden NC0007927 Arlene Hosiery Mill  Hickory NC0025135 Huffman Finishing  Granite Falls NC0034860 Schneider Mills  Taylorsville NC0043320 Burlington Industries  Cordova NC0080993 Spartan Mills  Cliffside Pennsylvania PA0008231 Gold Mills Dyehouse  Pine Grove PA0009172 Chloe Textiles  Middletown PA0013765 Industrial Parks, Ltd.  Bangor Rhode Island RI0000191 Kenyon Industries  Charlestown South Carolina SC0000213 Mohawk Commercial Carpet  Liberty SC0000264 Greenwood Mills  Liberty SC0000299 Fieldcrest Cannon  Abbeville SC0000353 Milliken  Abbeville SC0000426 Blair Mills  Belton SC0000477 Milliken  Pendleton SC0000485 La France Industry  La France 52 SC0000591 J. P. Stevens  Clemson Validated NPDES Permits from PCS ( cont.)

South Carolina ( cont.) SC0000990 Plusa  Jamestown SC0001163 Greenwood Mills  Orangeburg Co. SC0001341 Veratec  Bethune SC0001368 Cone Mills  Carlisle SC0001490 Reeves Bros.  Bishopville SC0001601 Woodside Mills  Fountain Inn SC0001805 Mohasco Industries  Dillon SC0002135 CCX Fiberglass Products  Walterboro SC0002151 Delta Mills  Wallace SC0002453 Spartan Mills  Startex SC0002500 Dixie Yarns  Chesterfield Co. SC0002569 Albany International  St. Stephens SC0002704 Galey & Lord  Society Hill SC0002747 Milliken  Valley Falls ( Spartanburg Co.) SC0003093 Milliken  Barnwell SC0003051 Milliken  Union Co. SC0003182 Milliken  Blacksburg SC0003191 Milliken  Marietta SC0003255 Springs Industries  Lancaster Co. SC0023264 Wateree Textiles  Camden SC0035157 Oneita Industries  Fingerville SC0035947 Spring City Knitting Co.  Gaffney SC0040363 National Dye Works  Lynchburg SC0043419 Fashion Fabrics of America  Orangeburg Texas TX0000698 WestPoint Pepperell ( Mission Valley)  New Braunfels TX0000701 WestPoint Pepperell  New Braunfels Virginia VA0001295 WestPoint Pepperell  Keysville VA0001376 Halifax Damask Mills  South Boston VA0001538 Bibb Co.  Brookneal VA0001554 Liberty Fabrics  Patrick Co. VA0001643 Burlington Industries  Halifax Co. VA0001651 Burlington Industries  Mecklenburg Co. VA0001678 Burlington Industries  Pittsylvania Co. VA0001864 Aileen Inc.  Edinburg VA0003051 Virginia Dyeing Corp.  Emporia VA0003069 Boykins Narrow Fabrics  Boykins VA0004677 Burlington Industries  Glasgow VA0050822 J. P. Stevens  Drakes Branch Washington WA0000230 Pendleton Woolen Mills  Washougal West Virginia WV0001261 Kellwood Co.  Spencer 53 APPENDIX III 4 Summary of Parameters With Data Reported to the PCS by Textile Mills Textile Mills Parameters 1 2 3 4 5 6 7 8 9 10 Ammonia * * * * Chlorine * * Sulfide * * * * * * * *

Bromodichloromethane * Chloroform * * Dibromochloromethane *

Antimony * * Arsenic * Cadmium * Chromium * * * * * * Copper * * * * * * * * Lead * * * Thallium * Zinc * * * * * * *

* = indicates data was available for the parameter Textile Mills: 1. Avondale Mills  Sylacauga, AL 2. WestPoint Pepperell  Opelika, AL 3. Masland Carpets Inc.  Atmore, AL 4. Rabun Apparel Inc.  Rabun Gap, GA 5. Thomaston Mills  Thomaston, GA 6. Chicopee  Gainesville, GA 7. Coats American Inc.  Toccoa, GA 8. Jefferson Mills  Jefferson, GA 9. William Carter Co.  Barnesville, GA 10. King Finishing Co.  Augusta, GA 54 Summary of Parameters With Data Reported to the PCS by Textile Mills ( cont.)

Textile Mills Parameters 11 12 13 14 15 16 17 18 19 20 Ammonia * * * * Chlorine * * * * Sulfide * * * * * * *

Chloroform * Di( 2 ethylhexyl) phthalate *

Arsenic * Chromium * * * * * * * Copper * * Lead * Silver * Zinc * *

Parameters 21 22 23 24 25 26 27 28 29 30 Ammonia * * * Chlorine * * * * Cyanide * Sulfide * * * * * * * * *

Formaldehyde * * Di( 2 ethylhexyl) phthalate *

Cadmium * Chromium * * * * * * * Copper * * Lead * Silver * Zinc * * * *

* = indicates data was available for the parameter Textile Mills: 11. Dundee Mills  Griffin, GA 21. Oxford Textile Inc.  Oxford, NJ 12. Forstman & Co. Dublin, GA 22. Gold Mills Dyehouse  Pine Grove, PA 13. Forstman & Co.  Louisville, GA 23. Chloe Textiles  Middletown, PA 14. Jockey Intrn'l  Carlisle, KY 24. Kenyon Industries  Kenyon, RI 15. Guilford of Maine  E. Douglas, MA 25. Greenwood Mills  Greenwood, SC 16. Veratec Inc.  Griswoldville, MA 26. Mohawk Industries  Bennettsville, SC 17. Tweave Inc.  Norton, MA 27. Milliken & Co.  Abbeville, SC 18. Robinson Manuf.  Oxford, ME 28. Milliken & Co.  Pendleton, SC 19. Burlington Denim  Stonewall, MS 29. LaFrance Industries  Mt. Vernon, SC 20. Kimberly Clark Corp.  Cornith, MS 30. WestPoint Stevens  Clemson, SC 55 Summary of Parameters With Data Reported to the PCS by Textile Mills ( cont.)

Textile Mills Parameters 31 32 33 34 35 36 37 38 39 40 Ammonia * * * Chlorine * * * * * Sulfide * * * * * * *

Chromium * * * * * * * * Copper * * Zinc * *

Textile Mills Parameters 41 42 43 44 45 46 47 48 49 50 Ammonia * * * * Chlorine * * * * * Sulfide * * * * * * *

Arsenic * * Chromium * * * * * *

* = indicates data was available for the parameter Textile Mills: 31. Plusa Inc.  Jamestown, SC 41. Milliken & Co.  Union, SC 32. Veratec  Bethune, SC 42. Milliken & Co.  Barnwell, SC 33. Cone Mills  Carlisle, SC 43. Milliken & Co.  Blacksburg, SC 34. Reeves Bros.  Bishopville, SC 44. Milliken & Co.  Marietta, SC 35. Mohawk Industries  Dillon, SC 45. Springs Industries  Grace, SC 36. CCX Fiberglass  Walterboro, SC 46. Wateree Textiles Co.  Camden, SC 37. Delta Mills  Wallace, SC 47. Milliken & Co.  Campobello, SC 38. Spartan Mills  Startex, SC 48. Spring City Knitting  Gaffney, SC 39. Dixie Yarns  Chesterfield, SC 49. Fash. Fabrics of America  Orangeburg, SC 40. Galey & Lord  Society Hill, SC 50. Mission Valley Textiles  New Braunfels, TX 56 Summary of Parameters With Data Reported to the PCS by Textile Mills ( cont.)

Textile Mills Parameters 51 52 53 54 55 56 57 58 59 Ammonia * * Chlorine * * * Sulfide * * * * * * * *

Chromium * * * * * * * * Chromium + 6 * * Copper * * Lead * Zinc * * *

* = indicates data was available for the parameter Textile Mills: 51. The Bibb Co.  Brookneal, VA 52. Liberty Fabrics  New York, VA 53. Burlington Industries  Halifax, VA 54. Burlington Industries  Clarksville, VA 55. Burlington Industries  Altavista, VA 56. Aileen Inc.  Edinburg, VA 57. Virginia Dyeing Corp.  Emporia, VA 58. Pendleton Woolen Manuf.  Washougal, WA 59. Kellwood Co.  Spencer, WV 57 APPENDIX IV 1 Estimated Loadings of Parameters From The PCS Database Methodology Limitations of the PCS Database 1. Industry classification of some NPDES permits is inaccurate. ( a) Some NPDES permits were originally encoded under an incorrect primary SIC code, and the permit's PCS record remains unrevised. Example: the NPDES permits of two OCPSF plants ( SIC 28) were retrieved as textile facilities ( SIC 22). Can cause the number of permits in an industry to be overstated or understated. ( b) Some NPDES permits are archaic, or currently invalid. Can cause the number of permits in an industry to be overstated.

2. The list of an industry's NPDES permits may be incomplete. ( a) Only facilities considered " major" ( defined as those with discharges posing " the greatest threat to human health or the environment") are required to submit monthly DMRs to the PCS. ( b) Both outfalls and pollutant parameters may be missing from the record of individual facilities, because they are only required to report data for those parameters that are specified in the NPDES permit conditions.

3. Data entry errors ( a) Manual transcription errors. ( b) Unit of measure in the monthly discharge reports ( DMRs) encoded incorrectly.

4. Several loading estimates based on the use of maximum concentration and flow were extremly large. Parameter loadings estimated from the PCS database are subject to these and other possible errors.

Assumptions in Data Selection 1. Loadings can only be estimated when records are available with valid concentration and corresponding flow. Depending on the monitoring requirements imposed by the permit, concentration may be reported in many different units in the PCS. EDS adjusts 26 different measures ( units) of concentration and three of flow to obtain units that are compatible for estimating parameter loadings. Gaps of incompatible data in the record of some parameters may cause loadings to be underestimated.

2. When both quantity and concentration are available, EDS first uses the reported parameter loading value. EDS then estimates parameter loading from discharge flow and concentration. The EDS routine selects concentration measurements from the PCS in the following order of preference:

Avg. daily conc.> Max. daily conc.> Min. daily conc.

3. In many cases, both a net ( excludes parameter loading of raw process water) and gross concentration for a single parameter and discharge outfall were reported to the PCS. When both net and gross values were reported, net concentrations were used. Gross values were used only when net concentrations were unavailable.

4. Multiple monitoring locations at a facility were assumed to represent independent outfalls. If two monitoring locations are actually on the same outfall, double counting can occur. Such estimates would overstate the actual loading of some parameters.

5. Thirty operating days per month were assumed in the calculations. 58 Editing Criteria for Estimated Loadings The parameter loading data obtained from the PCS by the EDS computer routine were edited according to the following criteria. 1. Exclude loadings for conventional and non conventional parameters ( e. g., BOD, TSS, Oil & Grease, COD, total phenols) that represent groups of chemicals. 2. Exclude loadings for " relatively non toxic" anion and cation parameters ( e. g., phosphorus, phosphate, chloride, sulfate, sulfite, nitrogen, nitrite, sodium chloride, and sodium). 3. When concentration and quantity of a chemical parameter are reported as " below the detection limit," process the data: as half the detection limit, if the parameter was detected at anytime; and as zero, if the parameter was never detected. 4. If multiple parameters are reported for the same chemical at the same discharge pipe, use the parameter with the maximum loading reported. 5. Calculate a facility's total loading of a chemical parameter by summing the parameter's loadings across all discharge pipes.

Editing Criteria for Outliers Loading values were identified as outliers and eliminated, if they met the following criteria: 1. Were at least 3X as large as the next highest PCS value and the highest TRI ( 1992) value for that chemical. 2. Failed Roxner's outlier test statistic, assuming a log normal distribution of values for a chemical across all of the industries. 3. Accounted for more than 30% of the total load for the chemical across all industries.

The contractor's memo, in summarizing outlier editing criteria, noted that loading values for some chemicals ( e. g., chlorine, copper and zinc) estimated from PCS data far exceeded the largest annual loading estimated from TRI data. The contractor further explains that " high" loading estimates from PCS data were retained, even though qualifying as an outlier because the estimate was at least 3X as large as the highest TRI loading estimate for that chemical. But this criterion is based on a faulty premise, namely that a chemical loading calculated from PCS data bears some consistency with loadings of the chemical that were reported to the TRI.

There is no reason to expect loading values estimated from PCS data would be similar to loading values from TRI data, because the two databases are founded upon dissimilar data. The TRI loadings derive from estimated losses of process chemicals to wastewater, where the amount that was released to surface waters ( includes treated effluent and stormwater runoff) or to POTWs was estimated by assuming the loss of a percentage of the total amount of the chemical used annually by the facility. In contrast, the PCS data derive from measured concentrations and flows ( treated effluent only) that were reported by NPDES permits. 59 Estimated Parameter Loadings  PCS Database Parameter NPDES LBYO1 LBYE2 Ammonia AL0001627 2119 2119 AL0002968 3382 3382 AL0021997 826 826 GA0000060 4112 4112 MA0003697 894 894 SC0000299 2993 2993 SC0000591 3771 3771 SC0002500 617 617 SC0003255 24120 24120 SC0043419 5950 5950 Chlorine GA0003115 1511 1511 GA0003409 1751 1751 SC0000264 73836 4045303 SC0000990 639 647 SC0001490 398 470 SC0001805 979 979 SC0002135 2902 2902 SC0002453 1099 1099 SC0035947 1036 1036 VA0001678 2447 2447 Sulfide AL0001627 4595 4595 GA0000213 6387 6387 PA0008231 4585 4585 SC0000477 3380 3380 SC0001341 291 28173 SC0002704 8121 8121 SC0003093 1526 1526 SC0003182 4910 4910 SC0003191 1872 1872 SC0003255 7569 7569 Bromodichloromethane GA0003115 2 2 Chloroform GA0000213 0.03 0.03 GA0003115 2 2 GA0003409 21 21 Dibromochloromethane GA0000213 0.01 0.01 Di( 2 ethylhexyl) phthalate GA0003409 3 3 RI0000191 11 13 SC0002135 3 3 Formaldehyde PA0009172 74 74 SC0000591 912 912 Cyanide SC0000485 4 5 Antimony GA0002038 44 44 GA0003115 28 72 Arsenic GA0000213 68 88 GA0003409 8 8 1. Amount discharged annually ( pounds per year). Calculation assumed a concentration value of ZERO, when reported concentration was below detection limit. 2. Amount discharged annually ( pounds per year). Calculation assumed a concentration value of HALF DETECTION LIMIT, when reported concentration was below detection limit. 60 Estimated Parameter Loadings  PCS ( cont.)

Parameter NPDES LBYO LBYE Arsenic SC0003191 6 12 TX0000698 33 111 Cadmium GA0003115 191 191 RI0000191 0.2 0.4 Chromium AL0002968 188 188 GA0003280 149 149 GA0003778 125 138 GA0003760 446 446 RI0000191 174 174 SC0001368 277 277 SC0003182 136 136 SC0003255 144 317 Chromium + 6 VA0001651 5135 5135 WV0001261 7 7 Copper GA0000060 46 46 GA0000213 170 180 GA0002038 206 206 GA0003115 8767 8767 GA0003280 14 14 GA0003409 610 610 NJ0004901 71 71 RI0000191 178 178 SC0001490 777 777 VA0001651 14379 14379 Lead AL0001627 3 3 AL0002968 2 2 GA0000060 13 13 MA0003697 5 6 RI0000191 5 5 VA0001538 0.1 0.1 Silver MA0003697 2 2 RI0000191 0.5 1 VA0001651 943 943 VA0001678 187 187 Zinc GA0000213 677 677 GA0002038 332 332 GA0003115 46168 46168 GA0003409 576 576 NJ0004901 277 277 RI0000191 124 124 SC0000477 576 576 SC0001490 1138 1138 SC0002500 146 146 VA0001651 183842 183842 61 APPENDIX IV 2 Textile Facilities in TRI Database Almore Dye House N. Hollywood, CA Anchor Dyeing & Finishing Philadelphia, PA Andrex Industries Asheville, NC Amerbelle Corp Vernon, CT American & Efird Inc Mount Holly, NC American & Efird Inc Salisbury, NC Amoco Fabrics Co Hazelhurst, GA Anglo Fabrics Co Webster, MA Anvil Knitwear Kings Mountain, NC Atlas Carpet Mills Los Angeles, CA Avon Mills Sylacauga, AL Baltic Dyeing & Finishing Passaic, NJ BASF Corp Sylvania, GA Bassett Walker Inc Martinsville, VA Bekaert Corp Rogers, AR Belding Corticelli Thread Hendersonville, NC BGF Industries Altavista, VA Bibb Co Rockingham, NC Bibb Co ( Whitehorse plant) Greenville, SC Bibb Co Columbus, GA Bloomsburg Mills Monroe, NC Burke Mills Valdese, NC Burlington House Finishing Burlington, NC Burlington House Monticello, AR Burlington Industries Rabun Gap, GA Burlington Industries Statesville, NC Burlington Menswear Raeford, NC Cascade Woolen Mill Oakland, ME Carisbrook Industries Glens Falls, NY Carleton Woolen Winthrop, ME Caron International Rochelle, IL Champion Dye & Finishing Paterson, NJ Chatham Mfg Elkin, NC Chem Tech Finishers Dalton, GA Cheraw Dyeing & Finishing Cheraw, SC Cinderella Knitting Gastonia, NC Clarksville Finishing Clarksville, VA Coats American Inc Toccoa, GA Collins & Aikman Roxboro, NC Collins & Aikman Dalton, GA Collins & Aikman Albemarle, NC Columbus Coated Fabrics Columbus, OH Concord Fabrics Washington, GA Copeland Inc Burlington, NC JC Cowan Finishing Forest City, NC Cramerton Automotive Fabrics Cramerton, NC Cranston Print Works Webster, MA Cranston Print Works Fletcher, NC Cross Creek Apparel Mount Airy, NC Dan River Inc Danville, VA 62 Delta Mills Marketing Wallace, SC Textile Facilities in TRI ( cont.)

Dixie Yarns Inc Tryon, NC Dixie Yarns Inc Chattanooga, TN Dorado Processing Woonsocket, RI Dumaine Towel Mill Fieldale, VA Duro Finishing Fall River, MA Duro Textile Printers Fall River, MA Dyersburg Fabrics Dyersburg, TN Dyersburg Steel Cord Dyersburg, TN Eastland Woolen Corinna, ME Facemate Corp Chicopee, MA Fashion Fabrics of America Orangeburg, SC Freudenberg Nonwoven Hopkinsville, KY Freudenberg Nonwoven Lowell, MA Fiberweb NA Inc Washougal, WA Fieldcrest Cannon Kannapolis, NC Fieldcrest Cannon Eden, NC Fieldcrest Cannon Calhoun Falls, NC Firestone Fiber & Textile Gastonia, NC Forstmann & Co E. Dublin, GA Forstmann & Co Milledgeville, GA Forstmann & Co Louisville, GA Galey & Lord Inc Society Hill, SC Gehring Tricot Dolgeville, NY GenCorp Polymer Columbus, MS General Tire Inc Barnesville, GA Glamourette Fashion Quebradillas, PR Glenoit Mills Inc Tarboro, NC Glen Raven Mills Anderson, SC Glen Raven Mills Altamahaw, NC Gold Mills Dyeing Pine Grove, PA Golding Industries Marion, SC Goldtex Inc Goldboro, NC Graniteville Co Graniteville, SC Graniteville Co ( Greg plant) Graniteville, SC GS Roofing Products N. Charleston, SC Guilford Mills Greensboro, NC Guilford Mills Kenansville, NC L. Hamrick Inc Gaffney, SC Hanes Dye & Finishing Winston Salem, NC Harriss & Covington High Point, NC Holliston Mills Inc Church Hill, TN Homestead Industries Claremont, NH Hope Valley Dyeing W. Warwick, RI Hornwood Inc Lilesville, NC Hurt Finishing Hurt, VA International Paper Lewisburg, PA International Woolen Sanford, ME Interstate Dye & Finishing Paterson, NJ Ithaca Industries Robbins, NC Ithaca Industries Wilkesboro, NC Ithaca Industries Clinton, SC 63 WG Humphrey Toccoa, GA Textile Facilities in TRI ( cont.)

Joan Fabrics Corp Lowell, MA Joan Fabrics Corp Fall River, MA Joan Fabrics Corp Newton, NC JP Stevens Wagram, NC Kayser Roth Corp Arecibo, PR Kayser Roth Corp Ashboro, NC Kayser Roth Corp Graham, NC Kayser Roth Corp Lumberton, NC Kayser Roth Corp Prosperity, SC Kimberly Clark La Grange, GA King Finishing Dover, GA Kingstree Kingstree, SC Lees Commercial Carpet Glasgow, VA Liberty Fabrics Jamesville, NC Liberty Fabrics Gordonsville, VA Liberty Fabrics Woolwine, VA LA Dye & Print Works ( 1 & 2) Los Angeles, CA Lowell Bleachery Griffin, GA Lyerly Rug Mill Lyerly, GA 3M Corp Freehold, NJ Magee Carpet Co Bloomsburg, PA Magnolia Finishing Blacksburg, SC Malden Mills Industries Lawrence, MA Manner Textile Haledon, NJ Marijon Dyeing & Finishing E. Rutherford, NJ JB Martin Co Leesville, SC Masland Industries Carlisle, PA Mayo Knitting Mill Tarboro, NC Microfibres South Winston Salem, NC Milliken & Co Belton, SC Milliken & Co Abbeville, SC Milliken & Co Marietta, SC Milliken & Co La Grange, GA Milliken & Co ( Elm plant) La Grange, GA Milliken & Co ( Valw plant) La Grange, GA Mohawk Carpet Corp Dillon, SC Mohican Mills Lincolnton, NC Moretz Mills Inc Newton, NC Morganton Dyeing & Finishing Morganton, NC Mount Vernon Mills Trion, GA Multitex Corp of America Calhoun, GA National Felt Co Easthampton, MA National Spinning Co Washington, NC North Bergen Piece Dye N. Bergen, NJ North Carolina Finishing Salisbury, NC Oxford Textile Oxford, NJ Park Avenue Finishing Burlington, NC Pennaco Hosiery Grenada, MS Perennial Print Corp Paterson, NJ Phoenix Mfg London, KY 64 Pioneer Finishing Fall River, MA Plusa Inc Jamestown, SC Poughkeepsie Finishers Paterson, NJ Textile Facilities in TRI ( cont.)

Precision Fabrics Greensboro, NC Renco Finishing Fair Lawn, NJ Rice Hosiery High Point, NC Robinson Mfg Oxford, ME Rochambeau Worsted Manville, RI Rock Hill Printing Rock Hill, SC Rockland Bamberg Inc Bamberg, SC Rockland Bleach & Dye Baltimore, MD Rogers Corp Rogers, CT Royalty Carpet Mills Irvine, CA Russell Corp Alexander City, AL Santee Print Works Sumter, SC Sara Lee Hosiery Winston Salem, NC Sara Lee Hosiery Lumberton, NC Sara Lee Hosiery Rockingham, NC Sara Lee Hosiery Florence, SC Sara Lee Hosiery Bennettsville, SC Sara Lee Hosiery Hartsville, SC Sara Lee Hosiery Marion, SC Scottsboro Rug Co Scottsboro, AL Schuylkill Haven Bleachery Schuylkill, PA Seville Dyeing Woonsocket, RI Shaw Industries ( Plants 1,2,4,8) Dalton, GA Shaw Industries Cartersville, GA Shaw Industries Andalusia, AL Slane Hosiery Mill High Point, NC South Carolina Elastic Co Landrum, SC Southern Phenix Textiles Phenix City, AL Spartan Mills Startex, SC Springs Bath Fashion Nashville, TN Springs Industries Calhoun, GA Springs Industries Lyman, SC Stanly Knitting Mills Oakboro, NC Sunbrite Dye Co Passaic, NJ Superba Print Works Mooresville, NC Swift Textiles Inc Columbus, GA Swift Textiles Inc Erwin, NC Synthetics Finishing Long View, NC Synthetics Finishing Hickory, NC Talon Inc Lake City, SC Tee Jays Mfg Co Florence, AL TexiLeather Toledo, OH TexPrint Inc Macon, GA Thomaston Mills Thomaston, GA Threads USA Gastonia, NC Tietex Corp Spartanburg, SC Travis Knits Inc Cherryville, NC Unifi Inc Madison, NC Unifi Inc Mayodan, NC 65 Unifi Inc Reidsville, NC United Piece Dye Works Edenton, NC US Finishing Greenville, SC US Textiles Corp Charlotte, NC Textile Facilities in TRI ( cont.)

Vanity Fair Mills Monroeville, AL Wansona Mfg Wadesboro, NC Warwick Dyeing W. Warwick, RI Wehadkee Yarn Mills Talladega, AL Wellman Inc Johnsonville, SC Western Piece Dyers Chicago, IL WestPoint Pepperell Columbus, GA WestPoint Pepperell Lumberton, NC WestPoint Pepperell La Grange, GA WestPoint Pepperell Opelika, AL WestPoint Pepperell Valley, AL WestPoint Pepperell Lanett, AL WestPoint Pepperell Hamilton, NC WestPoint Pepperell Biddeford, ME Winston Mills Inc Swannanoa, NC 66 APPENDIX IV 3 Estimated Loadings of Parameters from the TRI Database Description of TRI Database The TRI database of chemical " releases" from textile facilities was compiled from their 1992 submittals of the reporting form ( Form R), an annual requirement in order to comply with Section 313 of the Emergency Planning and Community Right to Know Act ( EPCRA, or Title III of the 1986 Superfund Amendments and Reauthorization Act). Section 313 contains a list of chemicals that are required to be reported on Form R. A completed Form R must be submitted for each chemical on the Section 313 list that is " manufactured or processed" at a facility in excess of 25,000 pounds per year. Chemicals that are " otherwise used" in excess of 10,000 pounds per year at a facility must also be reported.

Facilities must report estimated quantities of both " routine and accidental releases" of chemicals listed in Section 313, as well as the maximum amount of the listed chemicals on site during the calendar year. With the total amount of a chemical used each year as a maximum value, the so called " releases" are merely individual facility estimates of the amount that is annually lost to wastewater or other media. The estimates may be based on monitoring data ( e. g., of treated effluent) or measurements of the amount of a chemical that was transferred off site ( e. g., to a POTW). Estimates may also be based on mass balance calculations, such as the amount of a chemical in " wastes" entering and leaving process equipment. The accuracy of these estimates is likely to be marginal and the computation is not necessarily consistent from one facility to another.

Assumptions and Limitations of the Estimated Loadings 1. TRI does not include all process chemicals in use at all textile facilities. Only facilities reporting releases of chemicals listed in Section 313 and meeting minimum threshold requirements are required to report to TRI. 2. Includes only facilities identified by primary SIC codes for textile products. 3. Textile facilities releasing under 1000 pounds of a chemical may submit a range of the " release/ transfer" amount for the chemical. In this study, the OPPT criteria were followed by assuming: 5 pounds for loads reported as 0 to 10; 250 pounds for loads reported as 10 to 499; 750 pounds for loads reported as 500 to 999.

4. The accuracy and comparability of TRI loading estimates are unknown. There is no assurance that the loadings of chemicals in TRI records were consistently estimated by reporting textile facilities. 67 Estimated Parameter Loadings  TRI Database Parameter Textile Facility Location Loading1 Acetone Gehring Tricot Dolgeville, NY 1600 Goldtex Inc. Goldboro, NC 198 Guilford Mills Greensboro, NC 14654 L Hamrick Inc Gaffney, SC 2 SC Elastic Co Landrum, SC 750 Kingstree Kingstree, SC 45002 Glen Raven Mills Anderson, SC 250 Milliken & Co Belton, SC 290002 Kimberly Clark La Grange, GA 5 WG Humphrey Toccoa, GA 35002 Russell Corp Alexander City, AL 34 Acrylic acid Wehadkee Yarn Mills Talladega, AL 2463 Benzyl chloride Talon Inc Lake City, SC 12000 Biphenyl Malden Mills Ind. Lawrence, MA 37314 Dorado Processing Woonsocket, RI 10114 Seville Dyeing Woonsocket, RI 82160 Sunbrite Dye Co. Passaic, NJ 14883 Marijon Dyeing & Fin. E. Rutherford, NJ 15737 Gold Mills Dyeing Pine Grove, PA 232 Schuylkill Haven Blea Schuylkill, PA 2082 United Piece Dye Wrk Edenton, NC 52 Travis Knits Inc Cherryville, NC 35727 Cinderella Knitting Gastonia, NC 24258 Anvil Knitwear Kings Mountain, NC 9500 Bloomsburg Mills Monroe, NC 11100 Stanly Knitting Mills Oakboro, NC 4207 Burlington Industries Rabun Gap, GA 38262 Concord Fabrics Washington, GA 30400 Multitex Corp of Am Calhoun, GA 34270 Springs Industries Calhoun, GA 47350 Shaw Industries ( P 2) Dalton, GA 15800 Chem Tech Finishers Dalton, GA 223946 Wehadkee Yarn Mills Talladega, AL 19 Tee Jays Mfg Co ( P 1) Florence, AL 14088 Tee Jays Mfg Co ( P 2) Florence, AL 49870 Vanity Fair Mills Monroeville, AL 1813 n Butanol Lees Commercial Carp Glasgow, VA 15662 Butylbenzyl phthalate Collins & Aikman Roxboro, NC 250 Southern Phenix Tex Phenix City, AL 250 Cresol ( mixed isomers) Wehadkee Yarn Mills Talladega, AL 2 Cumene Oxford Textile Oxford, NJ 2452 Decabromodiphenyl oxide Malden Mills Ind. Lawrence, MA 750 Joan Fabrics Corp. Lowell, MA 16 Joan Fabrics Corp. Fall River, MA 4 Rockland Bleach & D Baltimore, MD 45970 Microfibres South Winston Salem, NC 250 Burlington House Fin Burlington, NC 660 1. Annual release ( pounds) to POTW. 2. Annual release ( pounds) to surface waters. This includes releases from on site treatment systems, process 68 outfalls ( e. g. pipes, open trenches) and stormwater runoff. 69 Estimated Parameter Loadings  TRI ( cont.)

Parameter Textile Facility Location Loading1 Decabromodiphenyl oxide Guilford Mills Greensboro, NC 4962 Precision Fabrics Greensboro, NC 6200 Collins & Aikman Roxboro, NC 1143 Superba Print Wrks Mooresville, NC 250 Joan Fabrics Newton, NC 250 Rockland Bamberg Inc Bamberg, SC 51451 Tietex Corp Spartanburg, SC 250 Milliken & Co Abbeville, SC 33002 Graniteville Co Graniteville, SC 250 WestPoint Pepperell Columbus, GA 250 Dichloromethane Wehadkee Yarn Mills Talladega, AL 9 Feudenberg Nonwoven Hopkinsville, KY 5 Diethanolamine Malden Mills Ind. Lawrence, MA 28000 Robinson Mfg. Oxford, ME 267002 Carleton Woolen Winthrop, ME 19800 Di( 2 ethylhexyl) phthalate Joan Fabrics Corp. Lowell, MA 3 Graniteville Co Graniteville, SC 3300 Southern Phenix Tex Phenix City, AL 250 Dyes: CI Basic Green 4 Dyersburg Fabrics Dyersburg, TN 2900 CI Disperse Yellow 3 Pioneer Finishing Fall River, MA 755 Ethylene glycol Cranston Print Works Webster, MA 8730 Marijon Dyeing & Fin. E. Rutherford, NJ 27776 BGF Industries Altavista, VA 1900 Dan River, Inc. Danville, VA 18802 Liberty Fabrics Jamesville, NC 13692 Fieldcrest Cannon Kannapolis, NC 7020 Mohican Mills Lincolnton, NC 10547 Burke Mills Inc Valdese, NC 65000 Cranston Print Wrks Fletcher, NC 132202 Wellman Inc Johnsonville, SC 374461 Galey & Lord Inc Society Hill, SC 2202 Delta Mills Marketing Wallace, SC 14562 Milliken & Co Marietta, SC 20302 Graniteville Co ( Greg) Graniteville, SC 50000 Kimberly Clark La Grange, GA 250 Mt. Vernon Mills Trion, GA 39269 Swift Textiles Inc Columbus, GA 11500 Wehadkee Yarn Mills Talladega, AL 327 Fiberweb NA Inc Washougal, WA 5580 Formaldehyde Renco Finishing Fair Lawn, NJ 180 Firestone Fib & Tex Gastonia, NC 250 WestPoint Pepperell Lumberton, NC 2422 Belding Corticelli Th Hendersonville, NC 82000 L Hamrick Inc Gaffney, SC 3600 GS Roofing Products N. Charleston, SC 1400 Magnolia Finishing Blacksburg, SC 2912 General Tire Inc Barnesville, GA 90 1. Annual release ( pounds) to POTW. 2. Annual release ( pounds) to surface waters. 70 Estimated Parameter Loadings  TRI ( cont.)

Parameters Textile Facility Location Loading1 Formaldehyde Milliken & Co La Grange, GA 200 Concord Fabrics Washington, GA 750 Wehadkee Yarn Mills Talladega, AL 72 Glycol ethers Liberty Fabrics Gordonsville, VA 9548 Dumaine Towel Mill Fieldale, VA 40500 Lees Commercial Carp Glasgow, VA 29962 Unifi Inc. Madison, NC 100 Guilford Mills Greensboro, NC 18445 National Spinning Co Washington, NC 75002 Fieldcrest Cannon Kannapolis, NC 29800 Mohican Mills Lincolnton, NC 11096 Swift Textiles Inc Erwin, NC 2502 Chatham Mfg Elkin, NC 6202 Golding Industries Marion, SC 9651 Galey & Lord Inc Society Hill, SC 18002 Milliken & Co Marietta, SC 9302 Magnolia Finishing Blacksburg, SC 7232 Graniteville Co Graniteville, SC 750 Graniteville Co ( Greg) Graniteville, SC 7800 Milliken & Co ( Elm) La Grange, GA 1171 King Finishing Dover, GA 250002 Burlington Industries Rabun Gap, GA 29352 Shaw Industries ( P 1) Dalton, GA 46159 Shaw Industries ( P 4) Dalton, GA 6300 Shaw Industries ( P 2) Dalton, GA 36600 Shaw Industries ( P 8) Dalton, GA 50000 Shaw Industries ( P 2) Dalton, GA 17500 Mt. Vernon Mills Trion, GA 26874 Russell Corp Alexander City, AL 17555 Avondale Mills Sylacauga, AL 7502 Isopropanol3 L Hamrick Inc Gaffney, SC 5000 Methanol BGF Industries Altavista, VA 1900 Firestone Fib & Tex Gastonia, NC 750 American & Efird Mount Holly, NC 71450 NC Finishing Salisbury, NC 2502 Bibb Co Rockingham, NC 250 Burlington Industries Statesville, NC 14000 Belding Corticelli Th Hendersonville, NC 100000 Galey & Lord Inc Society Hill, SC 502 Delta Mills Marketing Wallace, SC 25652 Bibb Co ( Whitehorse) Greenville, SC 200 Graniteville Co ( Greg) Graniteville, SC 3000 WestPoint Pepperell La Grange, GA 273 Concord Fabrics Washington, GA 3300 Bibb Co Columbus, GA 2129 Wehadkee Yarn Mills Talladega, AL 232 Tee Jays Mfg Co Florence, AL 21585 1. Annual release ( pounds) to POTW. 2. Annual release ( pounds) to surface waters. 71 3. Reporting error. Isopropanol not manufactured at this textile facility. 72 Estimated Parameter Loadings  TRI ( cont.)

Parameter Textile Facility Location Loading1 Methanol Vanity Fair Mills Monroeville, AL 708 WestPoint Pepperell Opelika, AL 12 WestPoint Pepperell Valley, AL 112 WestPoint Pepperell Lanett, AL 130 Methylethyl ketone Graniteville Co Graniteville, SC 2100 GenCorp Polymer Columbus, MS 4 TextiLeather Toledo, OH 250 Methylisobutyl ketone Graniteville Co Graniteville, SC 250 GenCorp Polymer Columbus, MS 5 Naphthalene Gold Mills Dyeing Pine Grove, PA 102 Galey & Lord Inc Society Hill, SC 64002 Toluene Graniteville Co Graniteville, SC 250 GenCorp Polymer Columbus, MS 5 TextiLeather Toledo, OH 5 Tetrachloroethlylene Park Avenue Finishing Burlington, NC 15316 Bloomsburg Mills Monroe, NC 5 American & Efird Inc Mount Holly, NC 3000 American & Efird Inc Salisbury, NC 1400 Synthetics Finishing Long View, NC 5 Synthetics Finishing Hickory, NC 5 Tetrachloroethylene Andrex Industries Asheville, NC 250 Delta Mills Marketing Wallace, SC 7702 Russell Corp Alexander City, AL 43942 Wehadkee Yarn Mills Talladega, AL 2758 1,2,4 Trichlorobenzene Hope Valley Dyeing W. Warwick, RI 2119 Clarksville Finishing Clarksville, VA 2502 Unifi Inc. Mayodan, NC 250 Unifi Inc. Reidsville, NC 250 WestPoint Pepperell Hamilton, NC 4472 United Piece Dye Wrk Edenton, NC 52 Travis Knits Inc Cherryville, NC 25278 JC Cowan Finishing Forest City, NC 2502 Hornwood Inc Lilesville, NC 2200 Mohican Mills Lincolnton, NC 9997 Wansona Mfg Wadesboro, NC 250 Cheraw Dyeing & Fin Cheraw, SC 33000 1,1,1 Trichloroethane Glen Raven Mills Altamahaw, NC 2502 Trichloroethylene Forstmann & Co E. Dublin, GA 2502 1,2,4 Trimethylbenzene Renco Finishing Fair Lawn, NJ 4000 Manner Textile Haledon, NJ 750 Oxford Textile Oxford, NJ 8172 Gold Mills Dyeing Pine Grove, PA 122 Park Avenue Finishing Burlington, NC 37597 Travis Knits Inc Cherryville, NC 25242 Guilford Mills Inc Kenansville, NC 52 Galey & Lord Inc Society Hill, SC 14002 1. Annual release ( pounds) to POTW. 2. Annual release ( pounds) to surface waters. 73 Estimated Parameter Loadings  TRI ( cont.)

Parameter Textile Facility Location Loadings1 Xylene ( mixed isomers) Anglo Fabrics Co. Webster, MA 17500 Pioneer Finishing Fall River, MA 19022 Amerbelle Corp. Vernon, CT 62400 N. Bergen Piece Dye N. Bergen, NJ 10615 Interstate Dye & Fin Passaic, NJ 6147 Poughkeepsie Finish Paterson, NJ 9200 Oxford Textile Oxford, NJ 1962 Park Avenue Finishing Burlington, NC 26655 Precision Fabrics Greensboro, NC 400 Threads USA Gastonia, NC 3226 Stanly Knitting Mills Oakboro, NC 16106 Santee Print Wrks Sumter, SC 48000 Galey & Lord Inc Society Hill, SC 21002 Graniteville Co Graniteville, SC 750 Ammonia National Felt Co. Easthampton, MA 16862 Malden Mills Ind. Lawrence, MA 125322 Freudenberg Nonwoven Lowell, MA 487 Duro Finishing Fall River, MA 250 Duro Textile Printers Fall River, MA 5 Baltic Dyeing & Fin. Passaic, NJ 13983 Sunbrite Dye Co. Passaic, NJ 1797 Marijon Dyeing & Fin. E. Rutherford, NJ 26700 Renco Finishing Fair Lawn, NJ 1200 Perennial Print Corp. Paterson, NJ 750 Champion Dye & Fin Paterson, NJ 3735 3M Corp. Freehold, NJ 270000 Carisbrook Ind. Glens Falls, NY 36428 International Paper Lewisburg, PA 490 Rockland Bleach & D Baltimore, MD 5142 Clarksville Finishing Clarksville, VA 36522 Lees Commercial Carp Glasgow, VA 34782 Hurt Finishing Hurt, VA 80002 Microfibres South Winston Salem, NC 12000 Sara Lee Hosiery Winston Salem, NC 12585 Copland Inc. Burlington, NC 3150 Rice Hosiery High Point, NC 15435 Fieldcrest Cannon Eden, NC 5600 Goldtex Inc. Goldsboro, NC 188212 Precision Fabrics Greensboro, NC 3000 Collins & Aikman Roxboro, NC 10787 JC Cowan Finishing Forest City, NC 23672 Firestone Fib & Tex Gastonia, NC 2200 Superba Print Wrks Mooresville, NC 250 American & Efird Mount Holly, NC 8533 NC Finishing Salisbury, NC 2502 Sara Lee Hosiery Lumberton, NC 12762 Sara Lee Hosiery Rockingham, NC 3272 1. Annual release ( pounds) to POTW. 2. Annual release ( pounds) to surface waters. 74 Estimated Parameter Loadings  TRI ( cont.)

Parameter Textile Facility Location Loading1 Ammonia Synthetics Finishing Long View, NC 750 Rockland Bamberg Inc Bamberg, SC 6342 Santee Print Wrks Sumter, SC 18000 L Hamrick Inc Gaffney, SC 2 Springs Industries Lyman, SC 750 Sara Lee Hosiery Florence, SC 10431 Sara Lee Hosiery Bennettsville, SC 5072 Sara Lee Hosiery Hartsville, SC 4665 Golding Industries Marion, SC 10204 Sara Lee Hosiery Marion, SC 26930 Fieldcrest Cannon Calhoun Falls, SC 61752 Rock Hill Printing Rock Hill, SC 1275 Graniteville Co Graniteville, SC 250 Graniteville Co ( Greg) Graniteville, SC 5 General Tire Inc Barnesville, GA 890 Milliken & Co ( Valw) La Grange, GA 200 BASF Corp Sylvania, GA 10000 Burlington Industries Rabun Gap, GA 43992 Collins & Aikman Dalton, GA 4214 Lyerly Rug Mill Lyerly, GA 40002 Forstmann & Co E. Dublin, GA 20002 Forstmann & Co Milledgeville, GA 7077 TexPrint Inc Macon, GA 4 WestPoint Pepperell Columbus, GA 250 Scottsboro Rug Mill Scottsboro, AL 13340 Southern Phenix Tex Phenix City, AL 10 Phoenix Mfg London, KY 250 Western Piece Dyers Chicago, IL 42500 Burlington House Monticello, AR 10 Ammonium nitrate ( solution) Lowell Bleachery Griffin, GA 14002 Thomaston Mills Thomaston, GA 2502 Coats American Inc Toccoa, GA 82162 Ammonium sulfate ( solution) Kayser Roth Corp. Arecibo, PR 113315 Duro Finishing Fall River, MA 2436 Warwick Dyeing W. Warwick, RI 1240 WestPoint Pepperell Biddeford, ME 78305 Cascade Woolen Mill Oakland, ME 21003 Amerbelle Corp. Vernon, CT 44350 Sunbrite Dye Co. Passaic, NJ 83900 Carisbrook Ind. Glens Falls, NY 83800 Hanes Dye & Finishing Winston Salem, NC 3800 Kayser Roth Corp. Ashboro, NC 26395 Park Avenue Finishing Burlington, NC 208254 Copland Inc. Burlington, NC 5000 Kayser Roth Corp. Graham, NC 47700 Ithaca Industries Robbins, NC 32000 Precision Fabrics Greensboro, NC 1900 Mohican Mills Lincolnton, NC 87250 1. Annual release ( pounds) to POTW. 75 2. Annual release ( pounds) to surface waters. 76 Estimated Parameter Loadings  TRI ( cont.)

Parameter Textile Facility Location Loading1 Ammonium sulfate ( solution) NC Finishing Salisbury, NC 2502 US Textile Corp Charlotte, NC 980 Kayser Roth Corp Lumberton, NC 50000 Ithaca Industries Wilkesboro, NC 130000 Kayser Roth Corp Prosperity, SC 54000 Ithaca Industries Clinton, SC 18000 Fieldcrest Cannon Calhoun Falls, SC 2502 Milliken & Co Marietta, SC 4602 Shaw Industries Cartersville, GA 179000 Springs Industries Calhoun, GA 156000 Shaw Industries ( P 4) Dalton, GA 18000 Shaw Industries ( P 1) Cartersville, GA 58000 Shaw Industries ( P 2) Dalton, GA 362000 Shaw Industries ( P 2) Dalton, GA 212000 Chem Tech Finishers Dalton, GA 42340 Lyerly Rug Mill Lyerly, GA 52 Forstmann & Co Milledgeville, GA 27458 Scottsboro Rug Mill Scottsboro, AL 1235 Vanity Fair Mills Monroeville, AL 210950 Pennaco Hosiery Grenada, MS 19400 Atlas Carpet Mills Los Angeles, CA 10703 Royalty Carpet Mills Irvine, CA 180700 Chlorine Glamourette Fashion Quebradillas, PR 591 Bassett Walker Inc. Martinsville, VA 17321 Hurt Finishing Hurt, VA 9002 Slane Hosiery Mill High Point, NC 58250 Harriss & Covington High Point, NC 500 Mayo Knitting Mill Tarboro, NC 5 Cramerton Automotive Cramerton, NC 320002 JC Cowan Finishing Forest City, NC 7502 Stanly Knitting Mills Oakboro, NC 660 NC Finishing Salisbury, NC 2502 Morganton Dyeing & F Morganton, NC 25500 Moretz Mills Inc Newton, NC 65000 Spartan Mills Startex, SC 11002 Plusa Inc Jamestown, SC 5502 Mohawk Carpet Corp Dillon, SC 7992 Wellman Inc Johnsonville, SC 640 Rock Hill Printing Rock Hill, SC 1410 Graniteville Co ( Greg) Graniteville, SC 2402 Lowell Bleachery Griffin, GA 12002 Holliston Mills Inc Church Hill, TN 12472 Almore Dye House N. Hollywood, CA 50688 Hydrochloric acid Facemate Corp. Chicopee, MA 5 Pioneer Finishing Fall River, MA 31 Dorado Processing Woonsocket, RI 1209 Seville Dyeing Woonsocket, RI 1294 Renco Finishing Fair Lawn, NJ 600 1. Annual release ( pounds) to POTW. 2. Annual release ( pounds) to surface waters 77 Estimated Parameter Loadings  TRI ( cont.)

Parameter Textile Facility Location Loading1 Hydrochloric acid Poughkeepsie Finish Paterson, NJ 41400 Wehadkee Yarn Mills Talladega, AL 330 Caron International Rochelle, IL 250 LA Dye & Print Wrks Los Angeles, CA 5 Phosphoric acid Perennial Print Corp. Paterson, NJ 100 Concord Fabrics Washington, GA 5 LA Dye & Print Wrks1 Los Angeles, CA 5 LA Dye & Print Wrks2 Los Angeles, CA 5 Sulfuric acid Glamourette Fashion Quebradillas, PR 1 Facemate Corp. Chicopee, MA 5 National Felt Co. Easthampton, MA 10718 Rochambeau Worsted Manville, RI 16200 Homestead Ind. Claremont, NH 750 International Woolen Sanford, ME 44950 Eastland Woolen Corinna, ME 280000 Anchor Dyeing & Fin Philadelphia, PA 27000 Firestone Fib & Tex Gastonia, NC 5 American & Efird Mount Holly, NC 20000 Winston Mills Inc Swannanoa, NC 11600 Dixie Yarns Inc Tryon, NC 250 Fashion Fabrics of Am Orangeburg, SC 60002 US Finishing Greenville, SC 841000 Kimberly Clark La Grange, GA 250 Swift Textiles Inc Columbus, GA 250 Vanity Fair Mills Monroeville, AL 25207 Dixie Yarns Inc Chattanooga, TN 3 Caron International Rochelle, IL 250 Antimony Collins & Aikman Roxboro, NC 250 Antimony compounds Joan Fabrics Corp. Lowell, MA 6 Rockland Bleach & D Baltimore, MD 22986 Burlington House Fin Burlington, NC 280 Superba Print Wrks Mooresville, NC 250 Synthetics Finishing Long View, NC 5 Joan Fabrics Newton, NC 5 Rockland Bamberg Inc Bamberg, SC 25726 Milliken & Co Abbeville, SC 15002 Graniteville Co Graniteville, SC 1500 Columbus Coated Fab Columbus, OH 212 TextiLeather Corp Toledo, OH 5 Western Piece Dyers Chicago, IL 250 Barium compounds Columbus Coated Fab Columbus, OH 242 TextiLeather Corp Toledo, OH 5 Cadmium compounds Columbus Coated Fab Columbus, OH 3 TextiLeather Corp Toledo, OH 5 Chromium Lees Commercial Carp Glasgow, VA 5122 1. Annual release ( pounds) to POTW. 2. Annual release ( pounds) to surface waters. 78 Estimated Parameter Loadings  TRI ( cont.)

Parameter Textile Facility Location Loading1 Chromium compounds Malden Mills Ind. Lawrence, MA 104288 Duro Finishing Fall River, MA 124 Carleton Woolen Winthrop, ME 190 Amerbelle Corp. Vernon, CT 5200 Masland Ind. Carlisle, PA 247 Magee Carpet Co. Bloomsburg, PA 250 Clarksville Finishing Clarksville, VA 7502 Liberty Fabrics Woolwine, VA 412 Hurt Finishing Hurt, VA 232 Guilford Mills Greensboro, NC 2729 Collins & Aikman Albemarle, NC 250 Burlington Menswear Raeford, NC 1289 Chatham Mfg Elkin, NC 11002 Graniteville Co Graniteville, SC 250 Graniteville Co ( Greg) Graniteville, SC 2900 Forstmann & Co Louisville, GA 7502 Forstmann & Co E. Dublin, GA 5402 Vanity Fair Mills Monroeville, AL 4536 Columbus Coated Fab Columbus, OH 4 TextiLeather Corp Toledo, OH 5 Cobalt compounds Masland Ind. Carlisle, PA 161 Collins & Aikman Albemarle, NC 250 Guilford Mills Inc Kenansville, NC 2502 Copper Wehadkee Yarn Mills Talladega, AL 278 Copper compounds Malden Mills Ind. Lawrence, MA 4100 Duro Textile Printers Fall River, MA 1326 Seville Dyeing Woonsocket, RI 5166 Rogers Corp. Rogers, CT 250 Schuylkill Haven Blea Schuylkill, PA 33 Bassett Walker Inc. Martinsville, VA 40739 Cross Creek Apparel Mount Airy, NC 267 WestPoint Pepperell Hamilton, NC 1822 WestPoint Pepperell Lumberton, NC 2482 JP Stevens Wagram, NC 6322 Galey & Lord Inc Society Hill, SC 14002 Graniteville Co ( Greg) Graniteville, SC 3100 Russell Corp Alexander City, AL 2285 Wehadkee Yarn Mills Talladega, AL 2835 Tee Jays Mfg Co Florence, AL 18130 Dyersburg Fabrics Dyersburg, TN 8100 Bekaert Steel Cord Dyersburg, TN 5 Bekaert Corp Rogers, AR 13 Lead compounds Amoco Fabrics Co Hazlehurst, GA 5 Shaw Industries Andalusia, AL 1 TextiLeather Corp Toledo, OH 5 Columbus Coated Fab Columbus, OH 30 1. Annual release ( pounds) to POTW. 2. Annual release ( pounds) to surface waters. 79 Estimated Parameter Loadings  TRI ( cont.)

Parameter Textile Facility Location Loading1 Nickel Wehadkee Yarn Mills Talladega, AL 131 Nickel compounds Russell Corp Alexander City, AL 137 Wehadkee Yarn Mills Talladega, AL 2536 Zinc ( fume or dust) 3 Glenoit Mills Inc. Tarboro, NC 250 Zinc compounds Joan Fabrics Corp. Lowell, MA 4 JB Martin Co Leesville, SC 750 Wellman Inc Johnsonville, SC 1133 Graniteville Co ( Greg) Graniteville, SC 250 Springs Industries Calhoun, GA 9082 Scottsboro Rug Mill Scottsboro, AL 4300 Shaw Industries Andalusia, AL 66 Springs Bath Fashion Nashville, TN 12385 Bekaert Steel Cord Dyersburg, TN 250 Columbus Coated Fab Columbus, OH 250 TextiLeather Corp Toledo, OH 250 Burlington House Monticello, AR 3600 Bekaert Corp Rogers, AR 14 1. Annual release ( pounds) to POTW. 2. Annual release ( pounds) to surface waters. 3. Reporting error. Not used in textile processing.