[Federal Register Volume 79, Number 39 (Thursday, February 27, 2014)]
[Rules and Regulations]
[Pages 11227-11294]
[FR Doc No: 2014-02704]

Vol. 79

Thursday,

No. 39

February 27, 2014

Part III

Environmental Protection Agency

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40 CFR Parts 51, 60, 61, et al.

 Revisions to Test Methods and Testing Regulations; Final Rule

Federal Register / Vol. 79 , No. 39 / Thursday, February 27, 2014 /
Rules and Regulations

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ENVIRONMENTAL PROTECTION AGENCY

40 CFR Parts 51, 60, 61, and 63

[EPA-HQ-OAR-2010-0114; FRL-9906-23-OAR]
RIN 2060-AQ01

Revisions to Test Methods and Testing Regulations

AGENCY: Environmental Protection Agency (EPA).

ACTION: Final rule.

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SUMMARY: This action promulgates technical and editorial corrections
for source testing of emissions and operations. Some current testing
provisions contain inaccuracies and outdated procedures, and new
alternatives that have been approved are being added. These revisions
will improve the quality of data and will give testers additional
flexibility to use the newly approved alternative procedures.

DATES: This final rule is effective on February 27, 2014. The
incorporation by reference materials listed in the rule are approved by
the Director of the Federal Register as of February 27, 2014.

ADDRESSES: The EPA has established a docket for this action under
Docket ID No. EPA-HQ-OAR-2010-0114. All documents in the docket are
listed in the http://www.regulations.gov index. Although listed in the
index, some information is not publicly available, e.g., confidential
business information (CBI) or other information whose disclosure is
restricted by statute. Certain other material, such as copyrighted
material, is not placed on the Internet and will be publicly available
only in hard copy form. Publicly available docket materials are
available either electronically at www.regulations.gov or in hard copy
at the Air Docket, EPA/DC, William Jefferson Clinton (WJC) Building,
Room 3334, 1301 Constitution Avenue NW., Washington, DC. The Docket
Facility and the Public Reading Room are open from 8:30 a.m. to 4:30
p.m., Monday through Friday, excluding legal holidays. The telephone
number for the Public Reading Room is<PHONE_NUMBER>, and the telephone
number for the Air Docket is<PHONE_NUMBER>.

FOR FURTHER INFORMATION CONTACT: Ms. Lula Melton, U.S. Environmental
Protection Agency, Office of Air Quality Planning and Standards, Air
Quality Assessment Division, Measurement Technology Group (E143-02),
Research Triangle Park, North Carolina 27711; telephone number: (919)
541-2910; fax number:<PHONE_NUMBER>; email address:
<EMAIL_ADDRESS>
SUPPLEMENTARY INFORMATION:

Table of Contents

I. General Information
    A. Does this action apply to me?
    B. Where can I obtain a copy of this action?
    C. Judicial Review
II. Background
III. Summary of Amendments
    A. Appendix M of Part 51
    B. Method 201A of Appendix M of Part 51
    C. Method 202 of Appendix M of Part 51
    D. General Provisions (Subpart A) Part 60
    E. Industrial-Commercial-Institutional Steam Generating Units
(Subpart Db) Part 60
    F. Hospital/Medical/Infectious Waste Incinerators (Subpart Ec)
Part 60
    G. Sulfuric Acid Plants (Subpart H) Part 60
    H. Sewage Treatment Plants (Subpart O) Part 60
    I. Kraft Pulp Mills (Subpart BB) Part 60
    J. Stationary Gas Turbines (Subpart GG) Part 60
    K. Lead-Acid Battery Manufacturing Plants (Subpart KK) Part 60
    L. Metallic Mineral Processing Plants (Subpart LL) Part 60
    M. Asphalt Processing and Asphalt Roofing Manufacture (Subpart
UU) Part 60
    N. Volatile Organic Chemical (VOC) Emissions From Synthetic
Organic Compound Manufacturing Industry (SOCMI) Distillation
Operations (Subpart NNN) Part 60
    O. Stationary Compression Ignition Internal Combustion Engines
(Subpart IIII) Part 60
    P. Stationary Spark Ignition Internal Combustion Engines
(Subpart JJJJ) Part 60
    Q. Method 1 of Appendix A-1 of Part 60
    R. Method 2 of Appendix A-1 of Part 60
    S. Method 2A of Appendix A-1 of Part 60
    T. Method 2B of Appendix A-1 of Part 60
    U. Method 2D of Appendix A-1 of Part 60
    V. Method 3A of Appendix A-2 of Part 60
    W. Method 3C of Appendix A-2 of Part 60
    X. Method 4 of Appendix A-3 of Part 60
    Y. Method 5 of Appendix A-3 of Part 60
    Z. Method 5A of Appendix A-3 of Part 60
    AA. Method 5E of Appendix A-3 of Part 60
    BB. Method 5H of Appendix A-3 of Part 60
    CC. Method 6 of Appendix A-4 of Part 60
    DD. Method 6C of Appendix A-4 of Part 60
    EE. Method 7 of Appendix A-4 of Part 60
    FF. Method 7A of Appendix A-4 of Part 60
    GG. Method 7E of Appendix A-4 of Part 60
    HH. Method 8 of Appendix A-4 of Part 60
    II. Method 10 of Appendix A-4 of Part 60
    JJ. Methods 10A and 10B of Appendix A-4 of Part 60
    KK. Method 11 of Appendix A-5 of Part 60
    LL. Method 12 of Appendix A-5 of Part 60
    MM. Method 14A of Appendix A-5 of Part 60
    NN. Method 16A of Appendix A-6 of Part 60
    OO. Method 16C of Appendix A-6 of Part 60
    PP. Method 18 of Appendix A-6 of Part 60
    QQ. Method 23 of Appendix A-7 of Part 60
    RR. Method 24 of Appendix A-7 of Part 60
    SS. Method 25 of Appendix A-7 of Part 60
    TT. Method 25C of Appendix A-7 of Part 60
    UU. Method 25D of Appendix A-7 of Part 60
    VV. Method 26 of Appendix A-8 of Part 60
    WW. Method 26A of Appendix A-8 of Part 60
    XX. Method 29 of Appendix A-8 of Part 60
    YY. Method 30B of Appendix A-8 of Part 60
    ZZ. Performance Specification 3 of Appendix B of Part 60
    AAA. Performance Specification 4 of Appendix B of Part 60
    BBB. Performance Specification 4B of Appendix B of Part 60
    CCC. Performance Specification 7 of Appendix B of Part 60
    DDD. Performance Specification 11 of Appendix B of Part 60
    EEE. Performance Specification 12B of Appendix B of Part 60
    FFF. Performance Specification 15 of Appendix B of Part 60
    GGG. Performance Specification 16 of Appendix B of Part 60
    HHH. Procedure 1 of Appendix F of Part 60
    III. Procedure 2 of Appendix F of Part 60
    JJJ. Procedure 5 of Appendix F of Part 60
    KKK. General Provisions (Subpart A) Part 61
    LLL. Beryllium (Subpart C) Part 61
    MMM. Beryllium Rocket Motor Firing (Subpart D) Part 61
    NNN. Mercury (Subpart E) Part 61
    OOO. Inorganic Arsenic Emissions From Glass Manufacturing Plants
(Subpart N) Part 61
    PPP. Method 101 of Appendix B of Part 61
    QQQ. Method 101A of Appendix B of Part 61
    RRR. Method 102 of Appendix B of Part 61
    SSS. Method 104 of Appendix B of Part 61
    TTT. Methods 108 and 108A of Appendix B of Part 61
    UUU. General Provisions (Subpart A) Part 63
    VVV. Synthetic Organic Chemical Manufacturing Industry (Subpart
G) Part 63
    WWW. Chromium Emissions From Hard and Decorative Chromium
Electroplating and Chromium Anodizing Tanks (Subpart N) Part 63
    XXX. Ethylene Oxide Emissions Standards for Sterilization
Facilities (Subpart O) Part 63
    YYY. Marine Tank Vessel Loading Operations (Subpart Y) Part 63
    ZZZ. Aerospace Manufacturing and Rework Facilities (Subpart GG)
Part 63
    AAAA. Pharmaceuticals Production (Subpart GGG) Part 63
    BBBB. Secondary Aluminum Production (Subpart RRR) Part 63
    CCCC. Manufacturing of Nutritional Yeast (Subpart CCCC) Part 63
    DDDD. Petroleum Refineries: Catalytic Cracking Units, Catalytic
Reforming Units, and Sulfur Recovery Units (Subpart UUUU) Part 63

    EEEE. Stationary Reciprocating Internal Combustion Engines
(Subpart ZZZZ) Part 63
    FFFF. Method 306 of Appendix A of Part 63
    GGGG. Method 306A of Appendix A of Part 63
    HHHH. Methods 308, 315, and 316 of Appendix A of Part 63
    IIII. Method 321 of Appendix A of Part 63
IV. Public Comments on the Proposed Amendments
V. Statutory and Executive Order Reviews
    A. Executive Order 12866: Regulatory Planning and Review and
Executive Order 13563: Improving Regulation and Regulatory Review
    B. Paperwork Reduction Act
    C. Regulatory Flexibility Act
    D. Unfunded Mandates Reform Act
    E. Executive Order 13132: Federalism
    F. Executive Order 13175: Consultation and Coordination With
Indian Tribal Governments
    G. Executive Order 13045: Protection of Children From
Environmental Health Risks and Safety Risks
    H. Executive Order 13211: Actions Concerning Regulations That
Significantly Affect Energy Supply, Distribution or Use
    I. National Technology Transfer and Advancement Act
    J. Executive Order 12898: Federal Actions To Address
Environmental Justice in Minority Populations and Low-Income
Populations
    K. Congressional Review Act

I. General Information

A. Does this action apply to me?

    The revisions promulgated in this final rule apply to testing at a
number of source categories. If you have any questions regarding the
applicability of this action to a particular entity, consult the person
listed in the preceding FOR FURTHER INFORMATION CONTACT section.

B. Where can I obtain a copy of this action?

    In addition to being available in the docket, an electronic copy of
this rule will also be available on the Worldwide Web (WWW) through the
Technology Transfer Network (TTN). Following the Administrator's
signature, a copy of the final rule will be placed on the TTN's policy
and guidance page for newly proposed or promulgated rules at http://www.epa.gov/ttn/oarpg. The TTN provides information and technology
exchange in various areas of air pollution control.

C. Judicial Review

    Under section 307(b)(1) of the Clean Air Act (CAA), judicial review
of this final rule is available by filing a petition for review in the
U.S. Court of Appeals for the District of Columbia Circuit by April 28,
2014. Under section 307(d)(7)(B) of the CAA, only an objection to this
final rule that was raised with reasonable specificity during the
period for public comment can be raised during judicial review.
Moreover, under section 307(b)(2) of the CAA, the requirements
established by this action may not be challenged separately in any
civil or criminal proceedings brought by EPA to enforce these
requirements.

II. Background

    The revisions to test methods and testing regulations were proposed
in the Federal Register on January 9, 2012, with a public comment
period that ended March 9, 2012. Thirty-eight comment letters were
received from the public. Changes were made to this final rule based on
the public comments.

III. Summary of Amendments

A. Appendix M of Part 51

    In the introduction of Appendix M of part 51, Methods 3A and 19 are
added to the list of methods not requiring the use of audit samples.

B. Method 201A of Appendix M of Part 51

    Revisions are made to Method 201A as published on December 21,
2010. Typographical errors in references to acetone blanks, isokinetic
sampling rate, source gas temperatures, stack blockage dimensions by
the sampling heads, and particulate matter with an aerodynamic diameter
less than or equal to 10 micrometers (PM10) in Sections
7.2.1, 8.3.4(b), <IP_ADDRESS>, <IP_ADDRESS>, and <IP_ADDRESS>(a), respectively, are
corrected. An erroneous reference to Methods 4A and 5 in Section 10.1
when using a standard pitot tube is corrected to refer to Methods 1 and
2. Section 10.5, which addresses Class A volumetric glassware is
deleted because it is not needed. For those filters that cannot be
weighed to a constant weight in Section 11.2.1, instructions are added
to flag and report the data as a minimum value. It is noted that the
nozzle, front half, and in-stack filter samples need to be speciated
into organic and inorganic fractions similar to the practice in Method
17. The method now notes that neither Method 17 nor 201A require a
separate analysis of the filter for inorganic and organic particulate
matter. Clarity is added for using Method 17 for quantifying
condensable particulate matter. An incorrect term in Equation 9 of
Section 12.5 is corrected. In the nomenclature in Section 12.1,
Vb, the volume of aliquot taken for ion chromatography (IC)
analysis, is deleted.

C. Method 202 of Appendix M of Part 51

    Revisions are made to Method 202 as published on December 21, 2010.
In Sections 7.2.1 and 7.2.2, an error in the units of the acetone blank
is corrected. In Section <IP_ADDRESS>, the text erroneously referring to
empty impingers is deleted. Section 11.2.1 is clarified concerning the
use of Method 17 for quantifying condensable particulate matter.
Figures 2 and 3 are revised to correctly show the first impinger with
an extended stem instead of a shortened one to be consistent with the
method text, and the condensed moisture and sample portion of the
sampling train are labeled to make it easy to identify. Figures 4, 5,
and 6 are republished because of the poor print quality in the December
21, 2010, publication.

D. General Provisions (Subpart A) Part 60

    In the General Provisions of part 60, Section 60.13(d)(1) is
revised to remove the phrase ``automatically, intrinsic to the opacity
monitor.'' Methods 3A and 19 are added to the list of methods not
requiring the use of audit samples in Section 60.8(g). A new Section
60.8(i) is added to allow the use of Method 205 of 40 CFR part 51,
Appendix M, ``Verification of Gas Dilution Systems for Field Instrument
Calibrations,'' as an alternative provision whenever multiple
calibration gases are required under part 60. The agency notes,
however, that the use of calibration gas dilution devices continues to
be disallowed for part 75 applications (see 40 CFR 75.22(a)(5)(i)).
Section 60.17 is revised to arrange the consensus standards that are
incorporated by reference in alpha-numeric order.

E. Industrial-Commercial-Institutional Steam Generating Units (Subpart
Db) Part 60

    In subpart Db, Method 320 is allowed as an alternative for
determining nitrogen oxides (NOX) concentration in Section
60.46b(f)(1)(ii), (h)(1) and (2), and sulfur dioxide (SO2)
concentration in Section 60.47b(b)(2).

F. Hospital/Medical/Infectious Waste Incinerators (Subpart Ec) Part 60

    In subpart Ec, the definition of medical/infectious wastes in
Section 60.51c is revised to correct the misspelling of ``cremation.''

G. Sulfuric Acid Plants (Subpart H) Part 60

    In subpart H, an equation for calculating the SO2
emission rate in Section 60.84(d) is corrected.

H. Sewage Treatment Plants (Subpart O) Part 60

    In subpart O, a reference to Method 209F in Section 60.154(b)(5) is
revised to reflect a newer available version of the method (i.e.,
2540G).

I. Kraft Pulp Mills (Subpart BB) Part 60

    In subpart BB, a typographical error is corrected in the equation
for correcting the total reduced sulfur concentration to 10 percent
oxygen.

J. Stationary Gas Turbines (Subpart GG) Part 60

    In subpart GG, the definitions of terms for the equation in Section
60.335(b)(l) are revised to allow the reference combustor inlet
absolute pressure to be measured in millimeters of mercury (mm Hg). The
site barometric pressure is allowed as an alternative to the observed
combustor inlet absolute pressure for calculating the mean
NOX emission concentration.

K. Lead-Acid Battery Manufacturing Plants (Subpart KK) Part 60

    In subpart KK, Method 29 is allowed as an alternative to Method 12
in Section 60.374(b)(1) and (c)(2) for determining the lead
concentration and flow rate of the effluent gas. An error in the
equation for calculating the lead emission concentration in
60.374(b)(2) is corrected.

L. Metallic Mineral Processing Plants (Subpart LL) Part 60

    In subpart LL, an error in the value of the particulate matter
standard in Section 60.382(a)(1) is corrected from 0.02 g/dscm to 0.05
g/dscm. An alternative procedure, wherein a single visible emission
observer can conduct visible emission observations for up to three
fugitive, stack, or vent emission points within a 15-second interval,
is allowed.

M. Asphalt Processing and Asphalt Roofing Manufacture (Subpart UU) Part
60

    In subpart UU, an error in the value of the particulate matter
standard for saturated felt or smooth-surfaced roll roofing is
corrected from 0.04 kg/Mg to 0.4 kg/Mg.

N. Volatile Organic Compound (VOC) Emissions from Synthetic Organic
Chemical Manufacturing Industry (SOCMI) Distillation Operations
(Subpart NNN) Part 60

    In subpart NNN, references to paragraphs in Section 60.660(c)(4)
and Section 60.665(h)(2) and (3) are corrected.

O. Stationary Compression Ignition Internal Combustion Engines (Subpart
IIII) Part 60

    In Subpart IIII, the requirement to use Method 1 or 1A for sampling
point selection in testing gaseous emission from engines with smaller
ducts is dropped, and single- or three-point sampling, depending on
duct size, is added.

P. Stationary Spark Ignition Internal Combustion Engines (Subpart JJJJ)
Part 60

    In Subpart JJJJ, the requirement to use Method 1 or 1A for sampling
point selection in testing gaseous emissions from engines with smaller
ducts is dropped, and single- or three-point sampling, depending on
duct size, is added.

Q. Method 1 of Appendix A-1 of Part 60

    In Method 1, the distances from the sampling point to flow
disturbances is clarified in Figure 1-1, and Figure 1-2 is corrected to
show the proper demarcation between the requirement for 12 and 16
sampling points.

R. Method 2 of Appendix A-1 of Part 60

    In Method 2, a pressure stability specification for the pitot tube
leak-check is added. An erroneous reference to Figure 2-6B is corrected
to reference Figure 2-7B. An error in a term in the denominator of
Equation 2-7 is corrected. The velocity constant in English units used
in Equation 2-7 is corrected by changing the units from m/sec to ft/
sec. The term for absolute temperature in Equations 2-7 and 2-8 is
corrected to represent the average of the absolute temperatures; an
inadvertently omitted term is added to Section 12.1 for the average
absolute temperature; and calibrating a barometer against a NIST-
traceable barometer is allowed as an alternative to calibrating against
a mercury barometer.

S. Method 2A of Appendix A-1 of Part 60

    In Method 2A, calibrating a barometer against a NIST-traceable
barometer is allowed as an alternative to calibrating against a mercury
barometer.

T. Method 2B of Appendix A-1 of Part 60

    In Method 2B, nomenclature errors are corrected and the assumed
ambient carbon dioxide concentration used in the calculations is
changed from 300 to 380 ppm to closer approximate current ambient
levels.

U. Method 2D of Appendix A-1 of Part 60

    In Method 2D, calibrating a barometer against a NIST-traceable
barometer is allowed as an alternative to calibrating against a mercury
barometer.

V. Method 3A of Appendix A-2 of Part 60

    In Method 3A, a redundant sentence noting that pre-cleaned air may
be used for the high-level calibration gas is deleted.

W. Method 3C of Appendix A-2 of Part 60

    In Method 3C, an equation for correcting the sample nitrogen
concentration for tank dilution is added as a supplemental calculation
option for Method 25C samples.

X. Method 4 of Appendix A-3 of Part 60

    In Method 4, the English value for the leak rate exceedance in
Section 9.1 is corrected from 0.20 cfm to 0.020 cfm. Method 6A, Method
320, and a calculation using F-factors are added as alternatives to
Method 4 for the moisture determination.

Y. Method 5 of Appendix A-3 of Part 60

    In Method 5, it is clarified that the deionized water used in the
analysis of material caught in the impingers must have <=0.001 percent
residue; the factor K is corrected to read K' in Equation 5-13;
calibrating a barometer against a NIST-traceable barometer is allowed
as an alternative to calibrating against a mercury barometer;
calibrating a temperature sensor against a thermometer equivalent to a
mercury-in-glass thermometer is allowed as an alternative to
calibrating against a mercury-in-glass thermometer; rechecking
temperature sensors for the filter holder and metering system after
each test is allowed in place of having sensors calibrated within 3
[deg]F; the option to check the probe heater calibration after a test
at a single point using a reference thermometer is added; the use of
weather station barometric pressure corrected to testing point
elevation is added as an option to having an on-site barometer; a
single acetone blank per container is allowed in place of a blank from
each wash bottle; Section 10.3.3 is clarified as a post-test metering
system calibration check rather than a metering system calibration, and
an alternative metering check procedure is added; the use of filter
holder supports or frits made of Teflon is allowed without having to
first obtain the Administrator's approval; and Reference 13 for post-
test calibration is added to the method.

Z. Method 5A of Appendix A-3 of Part 60

    In Method 5A, mercury-free thermometers are allowed as an
alternative to mercury-in-glass thermometers.

AA. Method 5E of Appendix A-3 of Part 60

    In Method 5E, the requirement to use the Rosemount Model 2100A
total organic content analyzer is replaced with the Tekmar-Dohrmann or
equivalent analyzer. In Section 12.5, the equation for total
particulate concentration is correctly labeled as Eq. 5E-5.

BB. Method 5H of Appendix A-3 of Part 60

    In Method 5H, Section 12.1 is revised to add missing terms
Ci, Co, Qi, and Qo; and
procedures for the determination of an alternative tracer gas flow rate
are added.

CC. Method 6 of Appendix A-4 of Part 60

    In Method 6, calibrating a temperature sensor against a thermometer
equivalent to a mercury-in-glass thermometer is allowed as an
alternative to using a mercury-in-glass thermometer, and calibrating a
barometer against a NIST-traceable barometer is allowed as an
alternative to calibrating against a mercury barometer.

DD. Method 6C of Appendix A-4 of Part 60

    In Section 4.0 of Method 6C, an incorrect reference to Section 4.1
of Method 6 is corrected to reference Section 4.0 of Method 7E.
Provisions that were removed from the original method that addressed
potential quenching effects in fluorescence analyzers are added to the
method.

EE. Method 7 of Appendix A-4 of Part 60

    In Method 7, procedures are added to avoid biasing the results when
sampling under conditions of high SO2 concentrations;
calibrating a barometer against a NIST-traceable barometer is added as
an alternative to calibrating against a mercury barometer; and
calibrating a temperature sensor against a thermometer equivalent to a
mercury-in-glass thermometer is an acceptable alternative to using a
mercury-in-glass thermometer.

FF. Method 7A of Appendix A-4 of Part 60

    In Method 7A, new procedures are added to avoid biasing the results
when sampling under conditions of high SO2 concentrations,
and calibrating a temperature sensor against a thermometer equivalent
to a mercury-in-glass thermometer is added as an acceptable alternative
to using a mercury-in-glass thermometer.

GG. Method 7E of Appendix A-4 of Part 60

    In Method 7E, the instructions for choosing the high-level
calibration gas are clarified. Instructions are added to minimize
contact of the sample with any condensate to reduce the chance of
sample loss, and an error in the traverse point locations used to
determine stratification across large stacks is corrected. The basis of
a stable response for measurements in the system response time
determination is revised in Section 8.2.5 to conform with Section
8.2.6. Alternative sampling bags made of materials other than Tedlar
are allowed if the materials are applicable for retaining the compounds
of interest.

HH. Method 8 of Appendix A-4 of Part 60

    In Method 8, an error in the definition of Vsoln is
corrected. Figure 8-1 is clarified to identify which impingers collect
sulfuric acid/sulfur trioxide and which collect SO2.

II. Method 10 of Appendix A-4 of Part 60

    Method 10 is revised to allow the use of sample tanks as an
alternative to flexible bags for sample collection.

JJ. Methods 10A and 10B of Appendix A-4 of Part 60

    In Methods 10A and 10B, sampling bags made of materials other than
Tedlar are allowed if the materials have the sample retaining qualities
of Tedlar.

KK. Method 11 of Appendix A-5 of Part 60

    Method 11 is revised to address sample breakthrough at high
concentrations by using an additional collection impinger. Calibrating
a temperature sensor against a thermometer equivalent to a mercury-in-
glass thermometer is an acceptable alternative to using a mercury-in-
glass thermometer.

LL. Method 12 of Appendix A-5 of Part 60

    Method 12 is revised to allow for analysis by inductively coupled
plasma-atomic emission spectrometry (ICP-AES) and cold vapor atomic
fluorescence spectrometry (CVAFS) as alternatives to atomic absorption
(AA) analysis.

MM. Method 14A of Appendix A-5 of Part 60

    In Section 10.1.1 of Method 14A, an incorrect reference to Figure
5-6 is corrected to reference Figure 5-5.

NN. Method 16A of Appendix A-6 of Part 60

    In Method 16A, the applicability section notes that method results
may be biased low if used at sources other than kraft pulp mills where
stack oxygen levels may be lower.

OO. Method 16C of Appendix A-6 of Part 60

    In Method 16C, errors in the nomenclature and the equation for
calculating the total reduced sulfur concentration are corrected.

PP. Method 18 of Appendix A-6 of Part 60

    In Method 18, sampling bags made of materials other than Tedlar are
allowed if the materials are applicable for retaining the compounds of
interest.

QQ. Method 23 of Appendix A-7 of Part 60

    In Method 23, the requirement in Section 2.2.7 that silica gel be
stored in metal containers has been deleted. Section 4.2.7 is clarified
to note that the used silica gel should be transferred to its original
container or other suitable vessel if moisture is being determined or
discarded if not needed. Mercury-free thermometers are allowed as
alternatives to mercury-in-glass thermometers. Section 8.0, which was
inadvertently removed in a previous rulemaking, has been added.

RR. Method 24 of Appendix A-7 of Part 60

    In Method 24, ASTM Method D2369 is cited without referencing
specific sections to preclude confusion if the method sections are
revised in the future.

SS. Method 25 of Appendix A-7 of Part 60

    In Method 25, more detailed information is given to describe the
filters used for sample collection.

TT. Method 25C of Appendix A-7 of Part 60

    Method 25C is revised to allow sampling lines made of Teflon.
Probes that have closed points and are driven below the surface in a
single step and withdrawn a distance to create a gas gap are allowed as
acceptable substitutes to pilot probes and the auger procedure.

UU. Method 25D of Appendix A-7 of Part 60

    In Method 25D, errors in cross-references within the method are
corrected.

VV. Method 26 of Appendix A-8 of Part 60

    Method 26 is revised to allow the use of heated Teflon probes in
place of glass-lined probes. Conflicting temperature requirements for
the sampling system are clarified, and the note to keep the probe and
filter temperature at least 20 [deg]C above the source temperature is
removed. The location of the thermocouple that monitors the collected
gas temperature is clarified as being as close to the filter holder as
practicable instead of in the gas stream. Method 26A is allowed as an
acceptable alternative when Method 26 is required.

WW. Method 26A of Appendix A-8 of Part 60

    Method 26A is revised to clearly state that the temperature of the
probe and filter must be maintained between 120 and 134 [deg]C.

XX. Method 29 of Appendix A-8 of Part 60

    Method 29 is revised to allow sample analysis by CVAFS as an
alternative to AA analysis.

YY. Method 30B of Appendix A-8 of Part 60

    In Method 30B, calibrating a barometer against a NIST-traceable
barometer is allowed as an alternative to calibrating against a mercury
barometer. Table 9-1 and the method text are revised to amend the
quality assurance/quality control criteria for sorbent trap section 2
breakthrough and sample analysis to address compliance testing and
relative accuracy testing of mercury monitoring systems currently being
conducted at much lower emission concentrations. The method is revised
to include the most up-to-date citation for determining the method
detection limit.

ZZ. Performance Specification 3 of Appendix B of Part 60

    In Performance Specification 3, a statement that was inadvertently
removed that allows the relative accuracy to be within 20 percent of
the reference method mean value is added to establish the original
intent of the rule.

AAA. Performance Specification 4 of Appendix B of Part 60

    Performance Specification 4 is revised to remove the interference
trap specified in Method 10 when evaluating non-dispersive infrared
continuous emission monitoring systems against Method 10.

BBB. Performance Specification 4B of Appendix B of Part 60

    Performance Specification 4B is clarified to note that Equation 1
in Section 7.1.1 for calculating calibration error only applies to the
carbon monoxide monitor and not the oxygen monitor. It is noted for the
oxygen monitor that the calibration error should be expressed as the
oxygen concentration difference between the mean monitor and reference
value at three levels.

CCC. Performance Specification 7 of Appendix B of Part 60

    Performance Specification 7 is revised to allow Methods 15 and 16
as reference methods in addition to Method 11.

DDD. Performance Specification 11 of Appendix B of Part 60

    In Performance Specification 11, errors in the denominators of
Equations 11-1 and 11-2 are corrected.

EEE. Performance Specification 12B of Appendix B of Part 60

    In Performance Specification 12B, allowance is made for using a
single good trap when one is lost, broken or damaged. More flexibility
is also allowed in meeting the stack flow-to-sample flow ratio.

FFF. Performance Specification 15 of Appendix B of Part 60

    In Performance Specification 15, the general references to 40 CFR
part 60, Appendix B, for the relative accuracy analysis procedure are
revised to specifically cite Performance Specification 2 of 40 CFR part
60, Appendix B.

GGG. Performance Specification 16 of Appendix B of Part 60

    Performance Specification 16 is revised to clarify the retesting of
a predictive emission monitoring system (PEMS) after a sensor is
replaced. Relative accuracy testing at three load or production rate
levels is allowed in cases where the key operating parameter is not
readily alterable. Additional instruction is added for performing the
relative accuracy audit (RAA). An error in the RAA acceptance criterion
is corrected, and an alternative acceptance criterion for low
concentration measurements is added. The yearly relative accuracy test
audit clearly notes that the statistical tests in Section 8.3 are not
required for this test. An incorrect reference to Equation 16-4 in
Section 12.4 is corrected.

HHH. Procedure 1 of Appendix F of Part 60

    In Procedure 1, the relevant performance specification would be
cited for the RAA calculation instead of using the current Equation 1-
1, which is not appropriate for all pollutants.

III. Procedure 2 of Appendix F of Part 60

    In Procedure 2, Equations 2-2 and 2-3 are revised to have the full-
scale value in the denominator, which is more appropriate than the up-
scale check value. The denominator of equation 2-4 is revised to
include the volume of the reference device rather than the full-scale
value.

JJJ. Procedure 5 of Appendix F of Part 60

    In Procedure 5, the second section listed as Section 6.2.6 is
correctly numbered as Section 6.2.7.

KKK. General Provisions (Subpart A) Part 61

    In the General Provisions of part 61, Methods 3A and 19 are added
to the list of methods not requiring the use of audit samples in
Section 61.13(e).

LLL. Beryllium (Subpart C) Part 61

    In the Beryllium National Emission Standards for Hazardous Air
Pollutants (NESHAP), Method 29 of part 60 is added as an acceptable
alternative to Method 104 in Section 61.33(a) for emissions testing.

MMM. Beryllium Rocket Motor Firing (Subpart D) Part 61

    In the beryllium rocket motor firing NESHAP, a conversion error in
the emission standard in Section 61.42(a) is corrected.

NNN. Mercury (Subpart E) Part 61

    In the mercury NESHAP, Method 29 of part 60 is added as an
acceptable alternative to Method 101A in Section 61.53(d)(2) for
emissions testing.

OOO. Inorganic Arsenic Emissions From Glass Manufacturing Plants
(Subpart N) Part 61

    In the glass manufacturing plants NESHAP, Method 29 in Appendix A
of part 60 is added as an acceptable alternative to Method 108 in
Section 61.164(d)(2)(i) for determining the arsenic emissions rate and
in Section 61.164(e)(1)(i) and (e)(2) for determining

the arsenic concentration in a gas stream.

PPP. Method 101 of Appendix B of Part 61

    Method 101 is revised to allow analysis by ICP-AES or CVAFS as
alternatives to AA analysis.

QQQ. Method 101A of Appendix B of Part 61

    Method 101A is revised to allow analysis by ICP-AES or CVAFS as
alternatives to AA analysis.

RRR. Method 102 of Appendix B of Part 61

    In Method 102, mercury-free thermometers are allowed in place of
mercury-in-glass thermometers.

SSS. Method 104 of Appendix B of Part 61

    Method 104 is revised to allow analysis by ICP-AES and CVAFS as
alternatives to AA analysis. A new alternative procedures section is
added to address ICP-AES.

TTT. Methods 108 and 108A of Appendix B of Part 61

    Methods 108 and 108A are revised to allow analysis by ICP-AES as an
alternative to AA analysis. A new alternative procedures section is
added to address ICP-AES.

UUU. General Provisions (Subpart A) Part 63

    In the General Provisions of part 63, Methods 3A and 19 are added
to the list of methods not requiring the use of audit samples in
Section 63.7(c). In Section 63.8(f)(6)(iii), an incorrect reference to
a section of Performance Specification 2 is corrected. Section 63.14 is
revised to arrange the materials that are incorporated by reference in
alpha-numeric order.

VVV. Synthetic Organic Chemical Manufacturing Industry (Subpart G) Part
63

    Subpart G is revised to allow the use of Method 316 or Method 8260B
in the SW-846 Compendium of Methods to determine hazardous air
pollutant concentrations in wastewater streams in Section
63.144(b)(5)(i).

WWW. Chromium Emissions From Hard and Decorative Chromium
Electroplating and Chromium Anodizing Tanks (Subpart N) Part 63

    South Coast Air Quality Management District Method 205.1 is added
as a testing option for measuring total chromium.

XXX. Ethylene Oxide Emissions Standards for Sterilization Facilities
(Subpart O) Part 63

    The ethylene oxide emissions standard for sterilization facilities
is revised to allow California Air Resources Board (CARB) Method 431 as
an alternative to the procedures in Section 63.365(b) for determining
the efficiency at the sterilization chamber vent. An error in a
reference to a section in Performance Specification 8 is also
corrected.

YYY. Marine Tank Vessel Loading Operations (Subpart Y) Part 63

    The marine tank vessel loading operations emissions standard is
revised to allow Method 25B as an alternative to Method 25A in Section
63.565(d)(5) for determining the average VOC concentration upstream and
downstream of recovery devices. Method 25B is allowed as an alternative
to Methods 25 and 25A for determining the percent reduction in VOC in
Section 63.565(d)(8), and the requirement that Method 25B be validated
according to Method 301 in Section 63.565(d)(10) is added. Method 25B
is also added as an alternative to Method 25A in determining the
baseline outlet VOC concentration in Section 63.565(g).

ZZZ. Aerospace Manufacturing and Rework Facilities (Subpart GG) Part 63

    The aerospace manufacturing and rework facilities emissions
standard is revised to remove an incorrect reference to the location of
Method 319 in Section 63.750(o).

AAAA. Pharmaceuticals Production (Subpart GGG) Part 63

    The pharmaceuticals production emissions standard is revised to
allow Method 320 as an alternative to Method 18 for demonstrating that
a vent is not a process vent.

BBBB. Secondary Aluminum Production (Subpart RRR) Part 63

    The secondary aluminum production emissions standard is revised to
allow Method 26 as an alternative to Method 26A in Section
63.1511(c)(9) for determining hydrochloric acid (HCl) concentration.

CCCC. Manufacturing of Nutritional Yeast (Subpart CCCC) Part 63

    Table 2 in the manufacturing of nutritional yeast emissions
standard is revised to delete the requirement to use Methods 1, 2, 3,
and 4 when measuring VOC by Method 25A.

DDDD. Petroleum Refineries: Catalytic Cracking Units, Catalytic
Reforming Units, and Sulfur Recovery Units (Subpart UUUU) Part 63

    Table 4 in the petroleum refineries emissions standard is revised
to allow Method 320 as an alternative to Method 18 for determining
control device efficiency for organic compounds.

EEEE. Stationary Reciprocating Internal Combustion Engines (Subpart
ZZZZ) Part 63

    Table 4 in the stationary reciprocating internal combustion engines
emissions standard is revised to clarify that a heated probe is not
necessary when using ASTM D6522 to measure oxygen or carbon dioxide
concentrations. The requirement to use Method 1 or 1A for sampling site
and sampling point selection in testing gaseous emissions from engines
with smaller ducts is deleted, and single- or three-point sampling,
depending on duct size, is added.

FFFF. Method 306 of Appendix A of Part 63

    Method 306 is revised to remove references to two figures that do
not exist and to clarify the conditions under which ICP is appropriate
for sample analysis. Alternative mercury-free thermometers are allowed
as alternatives to mercury-in-glass thermometers.

GGGG. Method 306A of Appendix A of Part 63

    In Method 306A, information is added to clarify the conditions
under which sample filtering is required.

HHHH. Methods 308, 315, and 316 of Appendix A of Part 63

    In Methods 308, 315, and 316, calibrating a temperature sensor
against a thermometer equivalent to a mercury-in-glass thermometer is
added as an alternative to mercury-in-glass thermometers. Alternative
mercury-free thermometers are allowed as alternatives to mercury-in-
glass thermometers.

IIII. Method 321 of Appendix A of Part 63

    In Method 321, the term for dilution factor in the calculations is
clarified.

IV. Public Comments on the Proposed Amendments

    Thirty-eight comment letters were received on the proposed rule.
The public comments and the agency's responses are summarized in the
Summary of Comments and Responses Document that has been added to the

docket that is accessible at the address given in the ADDRESSES section
of this preamble.

V. Statutory and Executive Order Reviews

A. Executive Order 12866: Regulatory Planning and Review and Executive
Order 13563: Improving Regulation and Regulatory Review

    This action is not a ``significant regulatory action'' under the
terms of Executive Order 12866 (58 FR 51735, October 4, 1993) and is,
therefore, not subject to review under Executive Orders 12866 and 13563
(76 FR 3821, January 21, 2011). It does not involve the expenditure of
$100 million in a year and does not raise significant issues. This
final rule amends current testing regulations by removing errors and
obsolete provisions and adding approved alternative procedures.

B. Paperwork Reduction Act

    This action does not impose an information collection burden under
the provisions of the Paperwork Reduction Act, 44 U.S.C. 3501 et seq.
Burden is defined at 5 CFR 1320.3(b). This final rule does not add
information collection requirements beyond those currently required
under the applicable regulations. This final rule amends current
testing regulations by removing errors and obsolete provisions and
adding approved alternative procedures.

C. Regulatory Flexibility Act

    The Regulatory Flexibility Act (RFA) generally requires an agency
to prepare a regulatory flexibility analysis of any rule subject to
notice and comment rulemaking requirements under the Administrative
Procedure Act or any other statute unless the agency certifies that the
rule will not have a significant economic impact on a substantial
number of small entities. Small entities include small businesses,
small organizations, and small governmental jurisdictions.
    For purposes of assessing the impacts of this rule on small
entities, small entity is defined as: (1) A small business as defined
by the Small Business Administration's (SBA) regulations at 13 CFR
121.201; (2) a small governmental jurisdiction that is a government of
a city, county, town, school district or special district with a
population of less than 50,000; and (3) a small organization that is
any not-for-profit enterprise which is independently owned and operated
and is not dominant in its field.
    After considering the economic impacts of this final rule on small
entities, I certify that this action will not have a significant
economic impact on a substantial number of small entities. This final
rule will not impose any requirements on small entities since it only
corrects and updates current requirements and adds new testing options.

D. Unfunded Mandates Reform Act

    This action contains no federal mandates under the provisions of
Title II of the Unfunded Mandates Reform Act of 1995 (UMRA), 2 U.S.C.
1531-1538, for state, local, or tribal governments or the private
sector. This action imposes no enforceable duty on any state, local or
tribal governments or the private sector. Therefore, this action is not
subject to the requirements of sections 202 or 205 of the UMRA. This
action is also not subject to the requirements of section 203 of UMRA
because it contains no regulatory requirements that might significantly
or uniquely affect small governments. The alternative procedure being
added will give small entities more flexibility in choosing testing
procedures in applicable situations.

E. Executive Order 13132: Federalism

    This action does not have federalism implications. It will not have
substantial direct effects on the states, on the relationship between
the national government and the states, or on the distribution of power
and responsibilities among the various levels of government, as
specified in Executive Order 13132. This final rule corrects and
updates current testing requirements. Thus, Executive Order 13132 does
not apply to this action.

F. Executive Order 13175: Consultation and Coordination With Indian
Tribal Governments

    This action does not have tribal implications, as specified in
Executive Order 13175 (65 FR 67249, November 9, 2000). This final rule
corrects and updates testing provisions that are already currently
mandated. It does not add any new requirements and does not affect
pollutant emissions or air quality. Thus, Executive Order 13175 does
not apply to this action.

G. Executive Order 13045: Protection of Children From Environmental
Health Risks and Safety Risks

    The EPA interprets EO 13045 (62 FR 19885, April 23, 1997) as
applying only to those regulatory actions that concern health or safety
risks, such that the analysis required under section 5-501 of the EO
has the potential to influence the regulation. This action is not
subject to EO 13045 because it does not establish an environmental
standard intended to mitigate health or safety risks.

H. Executive Order 13211: Actions Concerning Regulations That
Significantly Affect Energy Supply, Distribution, or Use

    This rule is not subject to Executive Order 13211 (66 FR 28355 (May
22, 2001)), because it is not a significant regulatory action under
Executive Order 12866.

I. National Technology Transfer and Advancement Act

    Section 12(d) of the National Technology Transfer and Advancement
Act of 1995 (``NTTAA''), Public Law 104-113, 12(d) (15 U.S.C. 272 note)
directs the EPA to use voluntary consensus standards in its regulatory
activities unless to do so would be inconsistent with applicable law or
otherwise impractical. Voluntary consensus standards are technical
standards (e.g., materials specifications, test methods, sampling
procedures, and business practices) that are developed or adopted by
voluntary consensus standards bodies. The NTTAA directs the EPA to
provide Congress, through OMB, explanations when the agency decides not
to use available and applicable voluntary consensus standards. This
action does not involve technical standards. Therefore, the EPA did not
consider the use of any voluntary consensus standards.

J. Executive Order 12898: Federal Actions To Address Environmental
Justice in Minority Populations and Low-Income Populations

    Executive Order (EO) 12898 (59 FR 7629 (Feb. 16, 1994)) establishes
federal executive policy on environmental justice. Its main provision
directs federal agencies, to the greatest extent practicable and
permitted by law, to make environmental justice part of their mission
by identifying and addressing, as appropriate, disproportionately high
and adverse human health or environmental effects of their programs,
policies, and activities on minority populations and low-income
populations in the United States.
    The EPA has determined that this final rule will not have
disproportionately high and adverse human health or environmental
effects on minority or low-income populations because it does not
affect the level of protection provided to human health or the
environment. This final rule does not relax the control measures on
sources regulated by the rule and,

therefore, will not cause emissions increases from these sources.

K. Congressional Review Act

    The Congressional Review Act, 5 U.S.C. 801 et seq., as added by the
Small Business Regulatory Enforcement Fairness Act of 1996, generally
provides that before a rule may take effect, the agency promulgating
the rule must submit a rule report, which includes a copy of the rule,
to each House of the Congress and to the Comptroller General of the
United States. The EPA will submit a report containing this rule and
other required information to the U.S. Senate, the U.S. House of
Representatives, and the Comptroller General of the United States prior
to publication of the rule in the Federal Register. A major rule cannot
take effect until 60 days after it is published in the Federal
Register. This action is not a ``major rule'' as defined by 5 U.S.C.
804(2). This rule will be effective on February 27, 2014.

List of Subjects

40 CFR Parts 51 and 61

    Air pollution control, Environmental protection, Performance
specifications, and Test methods and procedures.

40 CFR Parts 60 and 63

    Air pollution control, Environmental protection, Incorporation by
reference, Performance specifications, and Test methods and procedures.

    Dated: January 28, 2014.
Gina McCarthy,
Administrator.

    For the reasons set out in the preamble, Title 40, Chapter I of the
Code of Federal Regulations is amended as follows:

PART 51--REQUIREMENTS FOR PREPARATION, ADOPTION, AND SUBMITTAL OF
IMPLEMENTATION PLANS

0
1. The authority citation for part 51 continues to read as follows:

    Authority: 42 U.S.C. 7401, et. seq.

0
2. Amend appendix M to part 51 as follows:
0
a. By revising section 4.0.a.
0
b. By amending Method 201A as follows:
0
i. By revising section 7.2.1.
0
ii. By revising paragraph 8.3.4(b).
0
iii. By revising section <IP_ADDRESS>.
0
iv. By revising section <IP_ADDRESS>.
0
v. By revising paragraph <IP_ADDRESS>(a).
0
vi. By revising the introductory text of section 10.1.
0
vii. By removing section 10.5.
0
viii. By revising section 11.2.1.
0
ix. By removing the term ``Vb'' and its definition from section 12.1.
0
x. By revising Equations 8 and 9 in section 12.5.
0
c. By amending Method 202 as follows:
0
i. By revising sections 7.2.1 and 7.2.2.
0
ii. By revising section 8.5.1.
0
iii. By revising section <IP_ADDRESS>.
0
iv. By revising sections 11.2.1 and 11.2.2.
0
vi. By revising Figures 2, 3, 4, 5, and 6 in section 18.0.

Appendix M to Part 51--Recommended Test Methods for State
Implementation Plans

* * * * *
    4.0. * * *
    a. The source owner, operator, or representative of the tested
facility shall obtain an audit sample, if commercially available,
from an AASP for each test method used for regulatory compliance
purposes. No audit samples are required for the following test
methods: Methods 3A and 3C of appendix A-3 of part 60, Methods 6C,
7E, 9, and 10 of appendix A-4 of part 60, Methods 18 and 19 of
appendix A-6 of part 60, Methods 20, 22, and 25A of appendix A-7 of
part 60, and Methods 303, 318, 320, and 321 of appendix A of part 63
of this chapter. If multiple sources at a single facility are tested
during a compliance test event, only one audit sample is required
for each method used during a compliance test. The compliance
authority responsible for the compliance test may waive the
requirement to include an audit sample if they believe that an audit
sample is not necessary. ``Commercially available'' means that two
or more independent AASPs have blind audit samples available for
purchase. If the source owner, operator, or representative cannot
find an audit sample for a specific method, the owner, operator, or
representative shall consult the EPA Web site at the following URL,
http://www.epa.gov/ttn/emc, to confirm whether there is a source
that can supply an audit sample for that method. If the EPA Web site
does not list an available audit sample at least 60 days prior to
the beginning of the compliance test, the source owner, operator, or
representative shall not be required to include an audit sample as
part of the quality assurance program for the compliance test. When
ordering an audit sample, the source owner, operator, or
representative shall give the sample provider an estimate for the
concentration of each pollutant that is emitted by the source or the
estimated concentration of each pollutant based on the permitted
level and the name, address, and phone number of the compliance
authority. The source owner, operator, or representative shall
report the results for the audit sample along with a summary of the
emission test results for the audited pollutant to the compliance
authority and shall report the results of the audit sample to the
AASP. The source owner, operator, or representative shall make both
reports at the same time and in the same manner or shall report to
the compliance authority first and report to the AASP. If the method
being audited is a method that allows the samples to be analyzed in
the field, and the tester plans to analyze the samples in the field,
the tester may analyze the audit samples prior to collecting the
emission samples provided a representative of the compliance
authority is present at the testing site. The tester may request and
the compliance authority may grant a waiver to the requirement that
a representative of the compliance authority must be present at the
testing site during the field analysis of an audit sample. The
source owner, operator, or representative may report the results of
the audit sample to the compliance authority and then report the
results of the audit sample to the AASP prior to collecting any
emission samples. The test protocol and final test report shall
document whether an audit sample was ordered and utilized and the
pass/fail results as applicable.
* * * * *

Method 201A--Determination of PM10 and PM2.5
Emissions From Stationary Sources (Constant Sampling Rate Procedure)

* * * * *
    7.2.1 Acetone. Use acetone that is stored in a glass bottle. Do
not use acetone from a metal container because it will likely
produce a high residue in the laboratory and field reagent blanks.
You must use acetone with blank values less than 1 part per million
by weight residue. Analyze acetone blanks prior to field use to
confirm low blank values. In no case shall a blank value of greater
than 0.0001 percent (1 part per million by weight) of the weight of
acetone used in sample recovery be subtracted from the sample weight
(i.e., the maximum blank correction is 0.1 mg per 100 g of acetone
used to recover samples).
* * * * *
    8.3.4 * * *
    (b) The appropriate nozzle to maintain the required gas sampling
rate for the velocity pressure range and isokinetic range. If the
isokinetic range cannot be met (e.g., batch processes, extreme
process flow or temperature variation), void the sample or use
methods subject to the approval of the Administrator to correct the
data. The acceptable variation from isokinetic sampling is 80 to 120
percent and no more than 100  21 percent (2 out of 12 or
5 out of 24) sampling points outside of this criteria.
* * * * *
    <IP_ADDRESS> Preliminary traverse. You must use an S-type pitot tube
with a conventional thermocouple to conduct the traverse. Conduct
the preliminary traverse as close as possible to the anticipated
testing time on sources that are subject to hour-by-hour gas flow
rate variations of approximately  20 percent and/or gas
temperature variations of approximately  28 [deg]C
( 50 [deg]F). (Note: You should be aware that these
variations can cause errors in the cyclone cut diameters and the
isokinetic sampling velocities.)
* * * * *
    <IP_ADDRESS> Probe blockage factor. You must use Equation 26 to
calculate an average probe blockage correction factor
(bf) if the diameter

of your stack or duct is between 25.7 and 36.4 inches for the
combined PM2.5/PM10 sampling head and pitot
and between 18.8 and 26.5 inches for the PM2.5 cyclone
and pitot. A probe blockage factor is calculated because of the flow
blockage caused by the relatively large cross-sectional area of the
cyclone sampling head, as discussed in Section <IP_ADDRESS> and
illustrated in Figures 8 and 9 of Section 17. You must determine the
cross-sectional area of the cyclone head you use and determine its
stack blockage factor. (Note: Commercially-available sampling heads
(including the PM10 cyclone, PM2.5 cyclone,
pitot and filter holder) have a projected area of approximately 31.2
square inches when oriented into the gas stream.) As the probe is
moved from the outermost to the innermost point, the amount of
blockage that actually occurs ranges from approximately 13 square
inches to the full 31.2 square inches plus the blockage caused by
the probe extension. The average cross-sectional area blocked is 22
square inches.
* * * * *
    <IP_ADDRESS> * * *
    (a) Container 1, Less than or equal to PM2.5
micrometer filterable particulate. Use tweezers and/or clean
disposable surgical gloves to remove the filter from the filter
holder. Place the filter in the Petri dish that you labeled with the
test identification and Container 1. Using a dry brush and/
or a sharp-edged blade, carefully transfer any PM and/or filter
fibers that adhere to the filter holder gasket or filter support
screen to the Petri dish. Seal the container. This container holds
particles less than or equal to 2.5 micrometers that are caught on
the in-stack filter. (Note: If the test is conducted for
PM10 only, then Container 1 would be for less
than or equal to PM10 micrometer filterable particulate.)
* * * * *
    10.1 Gas Flow Velocities. You must use an S-type pitot tube that
meets the required EPA specifications (EPA Publication 600/4-77-
0217b) during these velocity measurements. (Note: If, as specified
in Section <IP_ADDRESS>, testing is performed in stacks less than 26.5
inches in diameter, testers may use a standard pitot tube according
to the requirements in Method 1 or 2 of appendix A-3 to part 60 of
this chapter.) You must also complete the following:
* * * * *
    11.2.1 Container 1, Less than or Equal to
PM2.5 Micrometer Filterable Particulate. Transfer the
filter and any loose particulate from the sample container to a
tared weighing dish or pan that is inert to solvent or mineral
acids. Desiccate for 24 hours in a dessicator containing anhydrous
calcium sulfate. Weigh to a constant weight and report the results
to the nearest 0.1 mg. (See Section 3.0 for a definition of Constant
weight.) If constant weight requirements cannot be met, the filter
must be treated as described in Section 11.2.1 of Method 202 of
appendix M to this part. Note: The nozzle and front half wash and
filter collected at or below 30 [deg]C (85 [deg]F) may not be heated
and must be maintained at or below 30 [deg]C (85 [deg]F).
* * * * *
    12.5 * * *
    [GRAPHIC] [TIFF OMITTED] TR27FE14.001

* * * * *

Method 202--Dry Impinger Method for Determining Condensable Particulate
Emissions From Stationary Sources

* * * * *
    7.2.1 Acetone. Use acetone that is stored in a glass bottle. Do
not use acetone from a metal container because it normally produces
a high residual mass in the laboratory and field reagent blanks. You
must use acetone that has a blank value less than 1.0 ppmw (0.1 mg/
100 g) residue.
    7.2.2 Hexane, American Chemical Society grade. You must use
hexane that has a blank residual mass value less than 1.0 ppmw (0.1
mg/100 g) residue.
* * * * *
    8.5.1 Impinger and CPM Filter Assembly.
    <IP_ADDRESS> Monitor the moisture condensation in the knockout and
backup impingers. If the accumulated water from moisture
condensation overwhelms the knockout impinger, i.e., the water level
is more than approximately one-half the capacity of the knockout
impinger, or if water accumulates in the backup impinger sufficient
to cover the impinger insert tip, then you may interrupt the
sampling run, recover and weigh the moisture accumulated in the
knockout and backup impinger, reassemble and leak check the sampling
train, and resume the sampling run. You must purge the water
collected during the test interruption as soon as practical
following the procedures in Section 8.5.3.
    <IP_ADDRESS> You must include the weight or volume of the moisture in
your moisture calculation and you must combine the recovered water
with the appropriate sample fraction for subsequent CPM analysis.
    <IP_ADDRESS> Use the field data sheet for the filterable particulate
method to record the CPM filter temperature readings at the
beginning of each sample time increment and when sampling is halted.
Maintain the CPM filter greater than 20 [deg]C (greater than 65
[deg]F) but less than or equal to 30 [deg]C (less than or equal to
85 [deg]F) during sample collection. (Note: Maintain the temperature
of the CPM filter assembly as close to 30 [deg]C (85 [deg]F) as
feasible.)
* * * * *
    <IP_ADDRESS> If you choose to conduct a pressurized nitrogen purge at
the completion of CPM sample collection, you may purge the entire
CPM sample collection train from the condenser inlet to the CPM
filter holder outlet or you may quantitatively transfer the water
collected in the condenser and the water dropout impinger to the
backup impinger and purge only the backup impinger and the CPM
filter. You must measure the water in the knockout and backup
impingers and record the volume or weight as part of the moisture
collected during sampling as specified in Section <IP_ADDRESS>.
    <IP_ADDRESS>.1 If you choose to conduct a purge of the entire CPM
sampling train, you must replace the short stem impinger insert in
the knock out impinger with a standard modified Greenburg Smith
impinger insert.
    <IP_ADDRESS>.2 If you choose to combine the knockout and backup
impinger catch prior to purge, you must purge the backup impinger
and CPM filter holder.
    <IP_ADDRESS>.3 If the tip of the impinger insert does not extend
below the water level (including the water transferred from the
first impinger if this option was chosen), you must add a measured
amount of degassed, deionized ultra-filtered water that contains 1
ppmw (1 mg/L) residual mass or less until the impinger tip is at
least 1 centimeter below the surface of the water. You must record
the amount of water added to the water dropout impinger (Vp)(see
Figure 4 of Section 18) to correct the moisture content of the
effluent gas. (Note: Prior to use, water

must be degassed using a nitrogen purge bubbled through the water
for at least 15 minutes to remove dissolved oxygen).
    <IP_ADDRESS>.4 To perform the nitrogen purge using positive pressure
nitrogen flow, you must start with no flow of gas through the clean
purge line and fittings. Connect the filter outlet to the input of
the impinger train and disconnect the vacuum line from the exit of
the silica moisture collection impinger (see Figure 3 of Section
18). You may purge only the CPM train by disconnecting the moisture
train components if you measure moisture in the field prior to the
nitrogen purge. You must increase the nitrogen flow gradually to
avoid over-pressurizing the impinger array. You must purge the CPM
train at a minimum of 14 liters per minute for at least one hour. At
the conclusion of the purge, turn off the nitrogen delivery system.
* * * * *
    11.2.1 Container 3, CPM Filter Sample. If the sample
was collected by Method 17 or Method 201A with a stack temperature
below 30 [deg]C (85 [deg]F), transfer the filter and any loose PM
from the sample container to a tared glass weighing dish. (See
Section 3.0 for a definition of constant weight.) Desiccate the
sample for 24 hours in a desiccator containing anhydrous calcium
sulfate. Weigh to a constant weight and report the results to the
nearest 0.1 mg. [Note: In-stack filter samples collected at 30
[deg]C (85 [deg]F) may include both filterable insoluble particulate
and condensable particulate. The nozzle and front half wash and
filter collected at or below 30 [deg]C (85 [deg]F) may not be heated
and must be maintained at or below 30 [deg]C (85 [deg]F).]
    11.2.2 CPM Container 1, Aqueous Liquid Impinger
Contents. Analyze the water soluble CPM in Container 1 as
described in this section. Place the contents of Container
1 into a separatory funnel. Add approximately 30 ml of
hexane to the funnel, mix well, and pour off the upper organic
phase. Repeat this procedure twice with 30 ml of hexane each time
combining the organic phase from each extraction. Each time, leave a
small amount of the organic/hexane phase in the separatory funnel,
ensuring that no water is collected in the organic phase. This
extraction should yield about 90 ml of organic extract. Combine the
organic extract from Container 1 with the organic train
rinse in Container 2.
* * * * *
    18.0 * * *
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BILLING CODE 6560-50-C
* * * * *

PART 60--STANDARDS OF PERFORMANCE FOR NEW STATIONARY SOURCES

0
3. The authority citation for part 60 continues to read as follows:

    Authority: 42 U.S.C. 7401, et. seq.

Subpart A--[Amended]

0
4. Amend Sec.  60.8 by revising paragraph (g)(1) and adding new
paragraphs (h) and (i) to read as follows:

Sec.  60.8  Performance tests.

* * * * *
    (g) * * *
    (1) The source owner, operator, or representative of the tested
facility shall obtain an audit sample, if commercially available, from
an AASP for each test method used for regulatory compliance purposes.
No audit samples are required for the following test methods: Methods
3A and 3C of appendix A-3 of part 60, Methods 6C, 7E, 9, and 10 of
appendix A-4 of part 60, Methods 18 and 19 of appendix A-6 of part 60,
Methods 20, 22, and 25A of appendix A-7 of part 60, Methods 30A and 30B
of appendix A-8 of part 60, and Methods 303, 318, 320, and 321 of
appendix A of part 63 of this chapter. If multiple sources at a single
facility are tested during a compliance test event, only one audit
sample is required for each method used during a compliance test. The
compliance authority responsible for the compliance test may waive the
requirement to include an audit sample if they believe that an audit
sample is not necessary. ``Commercially available'' means that two or
more independent AASPs have blind audit samples available for purchase.
If the source owner, operator, or representative cannot find an audit
sample for a specific method, the owner, operator, or representative
shall consult the EPA Web site at the following URL, www.epa.gov/ttn/emc, to confirm whether there is a source that can supply an audit
sample for that method. If the EPA Web site does not list an available
audit sample at least 60 days prior to the beginning of the compliance
test, the source owner, operator, or representative shall not be
required to

include an audit sample as part of the quality assurance program for
the compliance test. When ordering an audit sample, the source owner,
operator, or representative shall give the sample provider an estimate
for the concentration of each pollutant that is emitted by the source
or the estimated concentration of each pollutant based on the permitted
level and the name, address, and phone number of the compliance
authority. The source owner, operator, or representative shall report
the results for the audit sample along with a summary of the emission
test results for the audited pollutant to the compliance authority and
shall report the results of the audit sample to the AASP. The source
owner, operator, or representative shall make both reports at the same
time and in the same manner or shall report to the compliance authority
first and then report to the AASP. If the method being audited is a
method that allows the samples to be analyzed in the field and the
tester plans to analyze the samples in the field, the tester may
analyze the audit samples prior to collecting the emission samples
provided a representative of the compliance authority is present at the
testing site. The tester may request and the compliance authority may
grant a waiver to the requirement that a representative of the
compliance authority must be present at the testing site during the
field analysis of an audit sample. The source owner, operator, or
representative may report the results of the audit sample to the
compliance authority and report the results of the audit sample to the
AASP prior to collecting any emission samples. The test protocol and
final test report shall document whether an audit sample was ordered
and utilized and the pass/fail results as applicable.
* * * * *
    (h) Unless otherwise specified in the applicable subpart, each test
location must be verified to be free of cyclonic flow and evaluated for
the existence of emission gas stratification and the required number of
sampling traverse points. If other procedures are not specified in the
applicable subpart to the regulations, use the appropriate procedures
in Method 1 to check for cyclonic flow and Method 7E to evaluate
emission gas stratification and selection of sampling points.
    (i) Whenever the use of multiple calibration gases is required by a
test method, performance specification, or quality assurance procedure
in a part 60 standard or appendix, Method 205 of 40 CFR part 51,
appendix M of this chapter, ``Verification of Gas Dilution Systems for
Field Instrument Calibrations,'' may be used.

0
5. Amend Sec.  60.13 by revising paragraph (d)(1) to read as follows:

Sec.  60.13  Monitoring requirements.

* * * * *
    (d)(1) Owners and operators of a CEMS installed in accordance with
the provisions of this part, must check the zero (or low level value
between 0 and 20 percent of span value) and span (50 to 100 percent of
span value) calibration drifts at least once each operating day in
accordance with a written procedure. The zero and span must, at a
minimum, be adjusted whenever either the 24-hour zero drift or the 24-
hour span drift exceeds two times the limit of the applicable
performance specification in appendix B of this part. The system must
allow the amount of the excess zero and span drift to be recorded and
quantified whenever specified. Owners and operators of a COMS installed
in accordance with the provisions of this part must check the zero and
upscale (span) calibration drifts at least once daily. For a particular
COMS, the acceptable range of zero and upscale calibration materials is
defined in the applicable version of PS-1 in appendix B of this part.
For a COMS, the optical surfaces, exposed to the effluent gases, must
be cleaned before performing the zero and upscale drift adjustments,
except for systems using automatic zero adjustments. The optical
surfaces must be cleaned when the cumulative automatic zero
compensation exceeds 4 percent opacity.
* * * * *

0
6. Revise Sec.  60.17 to read as follows:

Sec.  60.17  Incorporations by reference.

    (a) Certain material is incorporated by reference into this part
with the approval of the Director of the Federal Register under 5
U.S.C. 552(a) and 1 CFR part 51. To enforce any edition other than that
specified in this section, the EPA must publish notice of change in the
Federal Register and the material must be available to the public. All
approved material is available for inspection at the Air and Radiation
Docket and Information Center, U.S. EPA, 401 M St. SW., Washington, DC,
telephone number 202-566, and is available from the sources listed
below. It is also available for inspection at the National Archives and
Records Administration (NARA). For information on the availability of
this material at NARA, call<PHONE_NUMBER> or go to http://www.archives.gov/federal_register/code_of_federal_regulations/ibr_locations.html.
    (b) American Gas Association, available through ILI Infodisk, 610
Winters Avenue, Paramus, New Jersey 07652:
    (1) American Gas Association Report No. 3: Orifice Metering for
Natural Gas and Other Related Hydrocarbon Fluids, Part 1: General
Equations and Uncertainty Guidelines (1990), IBR approved for Sec.
60.107a(d).
    (2) American Gas Association Report No. 3: Orifice Metering for
Natural Gas and Other Related Hydrocarbon Fluids, Part 2: Specification
and Installation Requirements (2000), IBR approved for Sec.
60.107a(d).
    (3) American Gas Association Report No. 11: Measurement of Natural
Gas by Coriolis Meter (2003), IBR approved for Sec.  60.107a(d).
    (4) American Gas Association Transmission Measurement Committee
Report No. 7: Measurement of Gas by Turbine Meters (Revised February
2006), IBR approved for Sec.  60.107a(d).
    (c) American Hospital Association (AHA) Service, Inc., Post Office
Box 92683, Chicago, Illinois 60675-2683. You may inspect a copy at the
EPA's Air and Radiation Docket and Information Center (Docket A-91-61,
Item IV-J-124), Room M-1500, 1200 Pennsylvania Ave. NW., Washington, DC
20460.
    (1) An Ounce of Prevention: Waste Reduction Strategies for Health
Care Facilities. American Society for Health Care Environmental
Services of the American Hospital Association. Chicago, Illinois. 1993.
AHA Catalog No. 057007. ISBN 0-87258-673-5. IBR approved for Sec. Sec.
60.35e and 60.55c.
    (2) [Reserved]
    (d) American Petroleum Institute (API), 1220 L Street NW.,
Washington, DC 20005.
    (1) API Publication 2517, Evaporation Loss from External Floating
Roof Tanks, Second Edition, February 1980, IBR approved for Sec. Sec.
60.111(i), 60.111a(f), and 60.116b(e).
    (2) API Manual of Petroleum Measurement Standards, Chapter 22--
Testing Protocol, Section 2--Differential Pressure Flow Measurement
Devices, First Edition, August 2005, IBR approved for Sec.  60.107a(d).
    (e) American Public Health Association, 1015 18th Street NW.,
Washington, DC 20036.
    (1) ``Standard Methods for the Examination of Water and
Wastewater,'' 16th edition, 1985. Method 303F: ``Determination of
Mercury by the Cold Vapor Technique.'' Incorporated by reference for
appendix A-8 to part 60, Method 29, Sec. Sec.  9.2.3, 10.3, and 11.1.3.

    (2) 2540 G. Total, Fixed, and Volatile Solids in Solid and
Semisolid Samples, in Standard Methods for the Examination of Water and
Wastewater, 20th Edition, 1998, IBR approved for Sec.  60.154(b).
    (f) American Society of Mechanical Engineers (ASME), Three Park
Avenue, New York, NY 10016-5990, Telephone<PHONE_NUMBER>, http://www.asme.org.
    (1) ASME Interim Supplement 19.5 on Instruments and Apparatus:
Application, Part II of Fluid Meters, 6th Edition (1971), IBR approved
for Sec. Sec.  60.58a(h), 60.58b(i), 60.1320(a), and 60.1810(a).
    (2) ASME MFC-3M-2004, Measurement of Fluid Flow in Pipes Using
Orifice, Nozzle, and Venturi, IBR approved for Sec.  60.107a(d).
    (3) ASME/ANSI MFC-4M-1986 (Reaffirmed 2008), Measurement of Gas
Flow by Turbine Meters, IBR approved for Sec.  60.107a(d).
    (4) ASME/ANSI MFC-5M-1985 (Reaffirmed 2006), Measurement of Liquid
Flow in Closed Conduits Using Transit-Time Ultrasonic Flowmeters, IBR
approved for Sec.  60.107a(d).
    (5) ASME MFC-6M-1998 (Reaffirmed 2005), Measurement of Fluid Flow
in Pipes Using Vortex Flowmeters, IBR approved for Sec.  60.107a(d).
    (6) ASME/ANSI MFC-7M-1987 (Reaffirmed 2006), Measurement of Gas
Flow by Means of Critical Flow Venturi Nozzles, IBR approved for Sec.
60.107a(d).
    (7) ASME/ANSI MFC-9M-1988 (Reaffirmed 2006), Measurement of Liquid
Flow in Closed Conduits by Weighing Method, IBR approved for Sec.
60.107a(d).
    (8) ASME MFC-11M-2006, Measurement of Fluid Flow by Means of
Coriolis Mass Flowmeters, IBR approved for Sec.  60.107a(d).
    (9) ASME MFC-14M-2003, Measurement of Fluid Flow Using Small Bore
Precision Orifice Meters, IBR approved for Sec.  60.107a(d).
    (10) ASME MFC-16-2007, Measurement of Liquid Flow in Closed
Conduits with Electromagnetic Flowmeters, IBR approved for Sec.
60.107a(d).
    (11) ASME MFC-18M-2001, Measurement of Fluid Flow Using Variable
Area Meters, IBR approved for Sec.  60.107a(d).
    (12) ASME MFC-22-2007, Measurement of Liquid by Turbine Flowmeters,
IBR approved for Sec.  60.107a(d).
    (13) ASME PTC 4.1-1964 (Reaffirmed 1991), Power Test Codes: Test
Code for Steam Generating Units (with 1968 and 1969 Addenda), IBR
approved for Sec. Sec.  60.46b, 60.58a(h), 60.58b(i), 60.1320(a), and
60.1810(a).
    (14) ASME/ANSI PTC 19.10-1981, Flue and Exhaust Gas Analyses [Part
10, Instruments and Apparatus], (Issued August 31, 1981), IBR approved
for Sec. Sec.  60.56c(b), 60.63(f), 60.106(e), 60.104a(d), (h), (i),
and (j), 60.105a(d), (f), and (g), Sec.  60.106a(a), Sec.  60.107a(a),
(c), and (d), tables 1 and 3 to subpart EEEE, tables 2 and 4 to subpart
FFFF, table 2 to subpart JJJJ, Sec. Sec.  60.4415(a), 60.2145(s) and
(t), 60.2710(s), (t), and (w), 60.2730(q), 60.4900(b), 60.5220(b),
tables 1 and 2 to subpart LLLL, tables 2 and 3 to subpart MMMM,
Sec. Sec.  60.5406(c) and 60.5413(b).
    (15) ASME QRO-1-1994, Standard for the Qualification and
Certification of Resource Recovery Facility Operators, IBR approved for
Sec. Sec.  60.54b(a) and (b), 60.56a, 60.1185(a) and (c), and
60.1675(a) and (c).
    (g) American Society for Testing and Materials (ASTM), 100 Barr
Harbor Drive, Post Office Box C700, West Conshohocken, PA 19428-2959;
also available through ProQuest, 300 North Zeeb Road, Ann Arbor, MI
48106.
    (1) ASTM A99-76, Standard Specification for Ferromanganese, IBR
approved for Sec.  60.261.
    (2) ASTM A99-82 (Reapproved 1987), Standard Specification for
Ferromanganese, IBR approved for Sec.  60.261.
    (3) ASTM A100-69, Standard Specification for Ferrosilicon, IBR
approved for Sec.  60.261.
    (4) ASTM A100-74, Standard Specification for Ferrosilicon, IBR
approved for Sec.  60.261.
    (5) ASTM A100-93, Standard Specification for Ferrosilicon, IBR
approved for Sec.  60.261.
    (6) ASTM A101-73, Standard Specification for Ferrochromium, IBR
approved for Sec.  60.261.
    (7) ASTM A101-93, Standard Specification for Ferrochromium, IBR
approved for Sec.  60.261.
    (8) ASTM A482-76, Standard Specification for Ferrochromesilicon,
IBR approved for Sec.  60.261.
    (9) ASTM A482-93, Standard Specification for Ferrochromesilicon,
IBR approved for Sec.  60.261.
    (10) ASTM A483-64, Standard Specification for Silicomanganese, IBR
approved for Sec.  60.261.
    (11) ASTM A483-74 (Reapproved 1988), Standard Specification for
Silicomanganese, IBR approved for Sec.  60.261.
    (12) ASTM A495-76, Standard Specification for Calcium-Silicon and
Calcium Manganese-Silicon, IBR approved for Sec.  60.261.
    (13) ASTM A495-94, Standard Specification for Calcium-Silicon and
Calcium Manganese-Silicon, IBR approved for Sec.  60.261.
    (14) ASTM D86-78, Distillation of Petroleum Products, IBR approved
for Sec. Sec.  60.562-2(d), 60.593(d), 60.593a(d), 60.633(h).
    (15) ASTM D86-82, Distillation of Petroleum Products, IBR approved
for Sec. Sec.  60.562-2(d), 60.593(d), 60.593a(d), 60.633(h).
    (16) ASTM D86-90, Distillation of Petroleum Products, IBR approved
for Sec. Sec.  60.562-2(d), 60.593(d), 60.593a(d), 60.633(h).
    (17) ASTM D86-93, Distillation of Petroleum Products, IBR approved
for Sec. Sec.  60.562-2(d), 60.593(d), 60.593a(d), 60.633(h).
    (18) ASTM D86-95, Distillation of Petroleum Products, IBR approved
for Sec. Sec.  60.562-2(d), 60.593(d), 60.593a(d), 60.633(h).
    (19) ASTM D86-96, Distillation of Petroleum Products, (Approved
April 10, 1996), IBR approved for Sec. Sec.  60.562-2(d), 60.593(d),
60.593a(d), 60.633(h), and 60.5401(f).
    (20) ASTM D129-64, Standard Test Method for Sulfur in Petroleum
Products (General Bomb Method), IBR approved for Sec. Sec.  60.106(j)
and appendix A-7 to part 60: Method 19, Section <IP_ADDRESS>.3.
    (21) ASTM D129-78, Standard Test Method for Sulfur in Petroleum
Products (General Bomb Method), IBR approved for Sec. Sec.  60.106(j)
and appendix A-7 to part 60: Method 19, Section <IP_ADDRESS>.3.
    (22) ASTM D129-95, Standard Test Method for Sulfur in Petroleum
Products (General Bomb Method), IBR approved for Sec. Sec.  60.106(j)
and appendix A-7 to part 60: Method 19, Section <IP_ADDRESS>.3.
    (23) ASTM D129-00, Standard Test Method for Sulfur in Petroleum
Products (General Bomb Method), IBR approved for Sec.  60.335(b).
    (24) ASTM D129-00 (Reapproved 2005), Standard Test Method for
Sulfur in Petroleum Products (General Bomb Method), IBR approved for
Sec.  60.4415(a).
    (25) ASTM D240-76, Standard Test Method for Heat of Combustion of
Liquid Hydrocarbon Fuels by Bomb Calorimeter, IBR approved for
Sec. Sec.  60.46(c), 60.296(b), and appendix A-7 to part 60: Method 19,
Section <IP_ADDRESS>.3.
    (26) ASTM D240-92, Standard Test Method for Heat of Combustion of
Liquid Hydrocarbon Fuels by Bomb Calorimeter, IBR approved for
Sec. Sec.  60.46(c), 60.296(b), and appendix A-7: Method 19, Section
<IP_ADDRESS>.3.
    (27) ASTM D240-02 (Reapproved 2007), Standard Test Method for Heat
of Combustion of Liquid Hydrocarbon

Fuels by Bomb Calorimeter, (Approved May 1, 2007), IBR approved for
Sec.  60.107a(d).
    (28) ASTM D270-65, Standard Method of Sampling Petroleum and
Petroleum Products, IBR approved for appendix A-7 to part 60: Method
19, Section <IP_ADDRESS>.1.
    (29) ASTM D270-75, Standard Method of Sampling Petroleum and
Petroleum Products, IBR approved for appendix A-7 to part 60: Method
19, Section <IP_ADDRESS>.1.
    (30) ASTM D323-82, Test Method for Vapor Pressure of Petroleum
Products (Reid Method), IBR approved for Sec. Sec.  60.111(l),
60.111a(g), 60.111b, and 60.116b(f).
    (31) ASTM D323-94, Test Method for Vapor Pressure of Petroleum
Products (Reid Method), IBR approved for Sec. Sec.  60.111(l),
60.111a(g), 60.111b, and 60.116b(f).
    (32) ASTM D388-77, Standard Specification for Classification of
Coals by Rank, IBR approved for Sec. Sec.  60.41, 60.45(f), 60.41Da,
60.41b, 60.41c, and 60.251.
    (33) ASTM D388-90, Standard Specification for Classification of
Coals by Rank, IBR approved for Sec. Sec.  60.41, 60.45(f), 60.41Da,
60.41b, 60.41c, and 60.251.
    (34) ASTM D388-91, Standard Specification for Classification of
Coals by Rank, IBR approved for Sec. Sec.  60.41, 60.45(f), 60.41Da,
60.41b, 60.41c, and 60.251.
    (35) ASTM D388-95, Standard Specification for Classification of
Coals by Rank, IBR approved for Sec. Sec.  60.41, 60.45(f), 60.41Da,
60.41b, 60.41c, and 60.251.
    (36) ASTM D388-98a, Standard Specification for Classification of
Coals by Rank, IBR approved for Sec. Sec.  60.41, 60.45(f), 60.41Da,
60.41b, 60.41c, and 60.251.
    (37) ASTM D388-99 (Reapproved 2004) [egr],\1\ Standard
Specification for Classification of Coals by Rank, IBR approved for
Sec. Sec.  60.41, 60.45(f), 60.41Da, 60.41b, 60.41c, and 60.251.
    (38) ASTM D396-78, Standard Specification for Fuel Oils, IBR
approved for Sec. Sec.  60.41b, 60.41c, 60.111(b), and 60.111a(b).
    (39) ASTM D396-89, Standard Specification for Fuel Oils, IBR
approved for Sec. Sec.  60.41b, 60.41c, 60.111(b), and 60.111a(b).
    (40) ASTM D396-90, Standard Specification for Fuel Oils, IBR
approved for Sec. Sec.  60.41b, 60.41c, 60.111(b), and 60.111a(b).
    (41) ASTM D396-92, Standard Specification for Fuel Oils, IBR
approved for Sec. Sec.  60.41b, 60.41c, 60.111(b), and 60.111a(b).
    (42) ASTM D396-98, Standard Specification for Fuel Oils, IBR
approved for Sec. Sec.  60.41b, 60.41c, 60.111(b), and 60.111a(b).
    (43) ASTM D975-78, Standard Specification for Diesel Fuel Oils, IBR
approved for Sec. Sec.  60.111(b) and 60.111a(b).
    (44) ASTM D975-96, Standard Specification for Diesel Fuel Oils, IBR
approved for Sec. Sec.  60.111(b) and 60.111a(b).
    (45) ASTM D975-98a, Standard Specification for Diesel Fuel Oils,
IBR approved for Sec. Sec.  60.111(b) and 60.111a(b).
    (46) ASTM D975-08a, Standard Specification for Diesel Fuel Oils,
IBR approved for Sec. Sec.  60.41b and 60.41c.
    (47) ASTM D1072-80, Standard Test Method for Total Sulfur in Fuel
Gases, IBR approved for Sec.  60.335(b).
    (48) ASTM D1072-90 (Reapproved 1994), Standard Test Method for
Total Sulfur in Fuel Gases, IBR approved for Sec.  60.335(b).
    (49) ASTM D1072-90 (Reapproved 1999), Standard Test Method for
Total Sulfur in Fuel Gases, IBR approved for Sec.  60.4415(a).
    (50) ASTM D1137-53, Standard Method for Analysis of Natural Gases
and Related Types of Gaseous Mixtures by the Mass Spectrometer, IBR
approved for Sec.  60.45(f).
    (51) ASTM D1137-75, Standard Method for Analysis of Natural Gases
and Related Types of Gaseous Mixtures by the Mass Spectrometer, IBR
approved for Sec.  60.45(f).
    (52) ASTM D1193-77, Standard Specification for Reagent Water, IBR
approved for appendix A-3 to part 60: Method 5, Section 7.1.3; Method
5E, Section 7.2.1; Method 5F, Section 7.2.1; appendix A-4 to part 60:
Method 6, Section 7.1.1; Method 7, Section 7.1.1; Method 7C, Section
7.1.1; Method 7D, Section 7.1.1; Method 10A, Section 7.1.1; appendix A-
5 to part 60: Method 11, Section 7.1.3; Method 12, Section 7.1.3;
Method 13A, Section 7.1.2; appendix A-8 to part 60: Method 26, Section
7.1.2; Method 26A, Section 7.1.2; and Method 29, Section 7.2.2.
    (53) ASTM D1193-91, Standard Specification for Reagent Water, IBR
approved for appendix A-3 to part 60: Method 5, Section 7.1.3; Method
5E, Section 7.2.1; Method 5F, Section 7.2.1; appendix A-4 to part 60:
Method 6, Section 7.1.1; Method 7, Section 7.1.1; Method 7C, Section
7.1.1; Method 7D, Section 7.1.1; Method 10A, Section 7.1.1; appendix A-
5 to part 60: Method 11, Section 7.1.3; Method 12, Section 7.1.3;
Method 13A, Section 7.1.2; appendix A-8 to part 60: Method 26, Section
7.1.2; Method 26A, Section 7.1.2; and Method 29, Section 7.2.2.
    (54) ASTM D1266-87, Standard Test Method for Sulfur in Petroleum
Products (Lamp Method), IBR approved for Sec. Sec.  60.106(j) and
60.335(b).
    (55) ASTM D1266-91, Standard Test Method for Sulfur in Petroleum
Products (Lamp Method), IBR approved for Sec. Sec.  60.106(j) and
60.335(b).
    (56) ASTM D1266-98, Standard Test Method for Sulfur in Petroleum
Products (Lamp Method), IBR approved for Sec. Sec.  60.106(j) and
60.335(b).
    (57) ASTM D1266-98 (Reapproved 2003) [egr],\1\ Standard
Test Method for Sulfur in Petroleum Products (Lamp Method), IBR
approved for Sec.  60.4415(a).
    (58) ASTM D1475-60 (Reapproved 1980), Standard Test Method for
Density of Paint, Varnish Lacquer, and Related Products, IBR approved
for Sec.  60.435(d), appendix A-8 to part 60: Method 24, Section 6.1;
and Method 24A, Sections 6.5 and 7.1.
    (59) ASTM D1475-90, Standard Test Method for Density of Paint,
Varnish Lacquer, and Related Products, IBR approved for Sec.
60.435(d), appendix A-8 to part 60: Method 24, Section 6.1; and Method
24A, Sec. Sec.  6.5 and 7.1.
    (60) ASTM D1552-83, Standard Test Method for Sulfur in Petroleum
Products (High-Temperature Method), IBR approved for Sec. Sec.
60.106(j), 60.335(b), and appendix A-7 to part 60: Method 19, Section
<IP_ADDRESS>.3.
    (61) ASTM D1552-95, Standard Test Method for Sulfur in Petroleum
Products (High-Temperature Method), IBR approved for Sec. Sec.
60.106(j), 60.335(b), and appendix A-7 to part 60: Method 19, Section
<IP_ADDRESS>.3.
    (62) ASTM D1552-01, Standard Test Method for Sulfur in Petroleum
Products (High-Temperature Method), IBR approved for Sec. Sec.
60.106(j), 60.335(b), and appendix A-7 to part 60: Method 19, Section
<IP_ADDRESS>.3.
    (63) ASTM D1552-03, Standard Test Method for Sulfur in Petroleum
Products (High-Temperature Method), IBR approved for Sec.  60.4415(a).
    (64) ASTM D1826-77, Standard Test Method for Calorific Value of
Gases in Natural Gas Range by Continuous Recording Calorimeter, IBR
approved for Sec. Sec.  60.45(f), 60.46(c), 60.296(b), and appendix A-7
to part 60: Method 19, Section <IP_ADDRESS>.
    (65) ASTM D1826-94, Standard Test Method for Calorific Value of
Gases in Natural Gas Range by Continuous Recording Calorimeter, IBR
approved for Sec. Sec.  60.45(f), 60.46(c), 60.296(b), and appendix A-7
to part 60: Method 19, Section <IP_ADDRESS>.
    (66) ASTM D1826-94 (Reapproved 2003), Standard Test Method for

Calorific (Heating) Value of Gases in Natural Gas Range by Continuous
Recording Calorimeter, (Approved May 10, 2003), IBR approved for Sec.
60.107a(d).
    (67) ASTM D1835-87, Standard Specification for Liquefied Petroleum
(LP) Gases, IBR approved for Sec. Sec.  60.41Da, 60.41b, and 60.41c.
    (68) ASTM D1835-91, Standard Specification for Liquefied Petroleum
(LP) Gases, IBR approved for Sec. Sec.  60.41Da, 60.41b, and 60.41c.
    (69) ASTM D1835-97, Standard Specification for Liquefied Petroleum
(LP) Gases, IBR approved for Sec. Sec.  60.41Da, 60.41b, and 60.41c.
    (70) ASTM D1835-03a, Standard Specification for Liquefied Petroleum
(LP) Gases, IBR approved for Sec. Sec.  60.41Da, 60.41b, and 60.41c.
    (71) ASTM D1945-64, Standard Method for Analysis of Natural Gas by
Gas Chromatography, IBR approved for Sec.  60.45(f).
    (72) ASTM D1945-76, Standard Method for Analysis of Natural Gas by
Gas Chromatography, IBR approved for Sec.  60.45(f).
    (73) ASTM D1945-91, Standard Method for Analysis of Natural Gas by
Gas Chromatography, IBR approved for Sec.  60.45(f).
    (74) ASTM D1945-96, Standard Method for Analysis of Natural Gas by
Gas Chromatography, IBR approved for Sec.  60.45(f).
    (75) ASTM D1945-03 (Reapproved 2010), Standard Method for Analysis
of Natural Gas by Gas Chromatography, (Approved January 1, 2010), IBR
approved for Sec. Sec.  60.107a(d) and 60.5413(d).
    (76) ASTM D1946-77, Standard Method for Analysis of Reformed Gas by
Gas Chromatography, IBR approved for Sec. Sec.  60.18(f), 60.45(f),
60.564(f), 60.614(e), 60.664(e), and 60.704(d).
    (77) ASTM D1946-90 (Reapproved 1994), Standard Method for Analysis
of Reformed Gas by Gas Chromatography, IBR approved for Sec. Sec.
60.18(f), 60.45(f), 60.564(f), 60.614(e), 60.664(e), and 60.704(d).
    (78) ASTM D1946-90 (Reapproved 2006), Standard Method for Analysis
of Reformed Gas by Gas Chromatography, (Approved June 1, 2006), IBR
approved for Sec.  60.107a(d).
    (79) ASTM D2013-72, Standard Method of Preparing Coal Samples for
Analysis, IBR approved for appendix A-7 to part 60: Method 19, Section
<IP_ADDRESS>.3.
    (80) ASTM D2013-86, Standard Method of Preparing Coal Samples for
Analysis, IBR approved for appendix A-7 to part 60: Method 19, Section
<IP_ADDRESS>.3.
    (81) ASTM D2015-77 (Reapproved 1978), Standard Test Method for
Gross Calorific Value of Solid Fuel by the Adiabatic Bomb Calorimeter,
IBR approved for Sec. Sec.  60.45(f), 60.46(c), and appendix A-7 to
part 60: Method 19, Section <IP_ADDRESS>.3.
    (82) ASTM D2015-96, Standard Test Method for Gross Calorific Value
of Solid Fuel by the Adiabatic Bomb Calorimeter, IBR approved for
Sec. Sec.  60.45(f), 60.46(c), and appendix A-7 to part 60: Method 19,
Section <IP_ADDRESS>.3.
    (83) ASTM D2016-74, Standard Test Methods for Moisture Content of
Wood, IBR approved for appendix A-8 to part 60: Method 28, Section
16.1.1.
    (84) ASTM D2016-83, Standard Test Methods for Moisture Content of
Wood, IBR approved for appendix A-8 to part 60: Method 28, Section
16.1.1.
    (85) ASTM D2234-76, Standard Methods for Collection of a Gross
Sample of Coal, IBR approved for appendix A-7 to part 60: Method 19,
Section <IP_ADDRESS>.1.
    (86) ASTM D2234-96, Standard Methods for Collection of a Gross
Sample of Coal, IBR approved for appendix A-7 to part 60: Method 19,
Section <IP_ADDRESS>.1.
    (87) ASTM D2234-97b, Standard Methods for Collection of a Gross
Sample of Coal, IBR approved for appendix A-7 to part 60: Method 19,
Section <IP_ADDRESS>.1.
    (88) ASTM D2234-98, Standard Methods for Collection of a Gross
Sample of Coal, IBR approved for appendix A-7 to part 60: Method 19,
Section <IP_ADDRESS>.1.
    (89) ASTM D2369-81, Standard Test Method for Volatile Content of
Coatings, IBR approved for appendix A-8 to part 60: Method 24, Section
6.2.
    (90) ASTM D2369-87, Standard Test Method for Volatile Content of
Coatings, IBR approved for appendix A-8 to part 60: Method 24, Section
6.2.
    (91) ASTM D2369-90, Standard Test Method for Volatile Content of
Coatings, IBR approved for appendix A-8 to part 60: Method 24, Section
6.2.
    (92) ASTM D2369-92, Standard Test Method for Volatile Content of
Coatings, IBR approved for appendix A-8 to part 60: Method 24, Section
6.2.
    (93) ASTM D2369-93, Standard Test Method for Volatile Content of
Coatings, IBR approved for appendix A-8 to part 60: Method 24, Section
6.2.
    (94) ASTM D2369-95, Standard Test Method for Volatile Content of
Coatings, IBR approved for appendix A-8 to part 60: Method 24, Section
6.2.
    (95) ASTM D2382-76, Heat of Combustion of Hydrocarbon Fuels by Bomb
Calorimeter (High-Precision Method), IBR approved for Sec. Sec.
60.18(f), 60.485(g), 60.485a(g), 60.564(f), 60.614(e), 60.664(e), and
60.704(d).
    (96) ASTM D2382-88, Heat of Combustion of Hydrocarbon Fuels by Bomb
Calorimeter (High-Precision Method), IBR approved for Sec. Sec.
60.18(f), 60.485(g), 60.485a(g), 60.564(f), 60.614(e), 60.664(e), and
60.704(d).
    (97) ASTM D2504-67, Noncondensable Gases in C3 and Lighter
Hydrocarbon Products by Gas Chromatography, IBR approved for Sec. Sec.
60.485(g) and 60.485a(g).
    (98) ASTM D2504-77, Noncondensable Gases in C3 and Lighter
Hydrocarbon Products by Gas Chromatography, IBR approved for Sec. Sec.
60.485(g) and 60.485a(g).
    (99) ASTM D2504-88 (Reapproved 1993), Noncondensable Gases in C3
and Lighter Hydrocarbon Products by Gas Chromatography, IBR approved
for Sec. Sec.  60.485(g) and 60.485a(g).
    (100) ASTM D2584-68(Reapproved 1985), Standard Test Method for
Ignition Loss of Cured Reinforced Resins, IBR approved for Sec.
60.685(c).
    (101) ASTM D2584-94, Standard Test Method for Ignition Loss of
Cured Reinforced Resins, IBR approved for Sec.  60.685(c).
    (102) ASTM D2597-94 (Reapproved 1999), Standard Test Method for
Analysis of Demethanized Hydrocarbon Liquid Mixtures Containing
Nitrogen and Carbon Dioxide by Gas Chromatography, IBR approved for
Sec.  60.335(b).
    (103) ASTM D2622-87, Standard Test Method for Sulfur in Petroleum
Products by Wavelength Dispersive X-Ray Fluorescence Spectrometry, IBR
approved for Sec. Sec.  60.106(j) and 60.335(b).
    (104) ASTM D2622-94, Standard Test Method for Sulfur in Petroleum
Products by Wavelength Dispersive X-Ray Fluorescence Spectrometry, IBR
approved for Sec. Sec.  60.106(j) and 60.335(b).
    (105) ASTM D2622-98, Standard Test Method for Sulfur in Petroleum
Products by Wavelength Dispersive X-Ray Fluorescence Spectrometry, IBR
approved for Sec. Sec.  60.106(j) and 60.335(b).
    (106) ASTM D2622-05, Standard Test Method for Sulfur in Petroleum
Products by Wavelength Dispersive X-Ray Fluorescence Spectrometry, IBR
approved for Sec.  60.4415(a).
    (107) ASTM D2879-83Test Method for Vapor Pressure-Temperature
Relationship and Initial Decomposition Temperature of Liquids by
Isoteniscope, IBR approved for Sec. Sec.  60.111b(f)(3), 60.116b(e),
60.116b(f), 60.485(e), and 60.485a(e).
    (108) ASTM D2879-96, Test Method for Vapor Pressure-Temperature
Relationship and Initial Decomposition

Temperature of Liquids by Isoteniscope, IBR approved for Sec. Sec.
60.111b(f)(3), 60.116b(e), 60.116b(f), 60.485(e), and 60.485a(e).
    (109) ASTM D2879-97, Test Method for Vapor Pressure-Temperature
Relationship and Initial Decomposition Temperature of Liquids by
Isoteniscope, IBR approved for Sec. Sec.  60.111b(f)(3), 60.116b(e),
60.116b(f), 60.485(e), and 60.485a(e).
    (110) ASTM D2880-78, Standard Specification for Gas Turbine Fuel
Oils, IBR approved for Sec. Sec.  60.111(b), 60.111a(b), and 60.335(d).
    (111) ASTM D2880-96, Standard Specification for Gas Turbine Fuel
Oils, IBR approved for Sec. Sec.  60.111(b), 60.111a(b), and 60.335(d).
    (112) ASTM D2908-74, Standard Practice for Measuring Volatile
Organic Matter in Water by Aqueous-Injection Gas Chromatography, IBR
approved for Sec.  60.564(j).
    (113) ASTM D2908-91, Standard Practice for Measuring Volatile
Organic Matter in Water by Aqueous-Injection Gas Chromatography, IBR
approved for Sec.  60.564(j).
    (114) ASTM D2986-71, Standard Method for Evaluation of Air, Assay
Media by the Monodisperse DOP (Dioctyl Phthalate) Smoke Test, IBR
approved for appendix A-3 to part 60: Method 5, Section 7.1.1; appendix
A-5 to part 60: Method 12, Section 7.1.1; and Method 13A, Section
<IP_ADDRESS>.
    (115) ASTM D2986-78, Standard Method for Evaluation of Air, Assay
Media by the Monodisperse DOP (Dioctyl Phthalate) Smoke Test, IBR
approved for appendix A-3 to part 60: Method 5, Section 7.1.1; appendix
A-5 to part 60: Method 12, Section 7.1.1; and Method 13A, Section
<IP_ADDRESS>.
    (116) ASTM D2986-95a, Standard Method for Evaluation of Air, Assay
Media by the Monodisperse DOP (Dioctyl Phthalate) Smoke Test, IBR
approved for appendix A-3 to part 60: Method 5, Section 7.1.1; appendix
A-5 to part 60: Method 12, Section 7.1.1; and Method 13A, Section
<IP_ADDRESS>.
    (117) ASTM D3173-73, Standard Test Method for Moisture in the
Analysis Sample of Coal and Coke, IBR approved for appendix A-7 to part
60: Method 19, Section <IP_ADDRESS>.3.
    (118) ASTM D3173-87, Standard Test Method for Moisture in the
Analysis Sample of Coal and Coke, IBR approved for appendix A-7 to part
60: Method 19, Section <IP_ADDRESS>.3.
    (119) ASTM D3176-74, Standard Method for Ultimate Analysis of Coal
and Coke, IBR approved for Sec.  60.45(f)(5)(i) and appendix A-7 to
part 60: Method 19, Section <IP_ADDRESS>.
    (120) ASTM D3176-89, Standard Method for Ultimate Analysis of Coal
and Coke, IBR approved for Sec.  60.45(f)(5)(i) and appendix A-7 to
part 60: Method 19, Section <IP_ADDRESS>.
    (121) ASTM D3177-75, Standard Test Method for Total Sulfur in the
Analysis Sample of Coal and Coke, IBR approved for appendix A-7 to part
60: Method 19, Section <IP_ADDRESS>.3.
    (122) ASTM D3177-89, Standard Test Method for Total Sulfur in the
Analysis Sample of Coal and Coke, IBR approved for appendix A-7 to part
60: Method 19, Section <IP_ADDRESS>.3.
    (123) ASTM D3178-73 (Reapproved 1979), Standard Test Methods for
Carbon and Hydrogen in the Analysis Sample of Coal and Coke, IBR
approved for Sec.  60.45(f).
    (124) ASTM D3178-89, Standard Test Methods for Carbon and Hydrogen
in the Analysis Sample of Coal and Coke, IBR approved for Sec.
60.45(f).
    (125) ASTM D3246-81, Standard Test Method for Sulfur in Petroleum
Gas by Oxidative Microcoulometry, IBR approved for Sec.  60.335(b).
    (126) ASTM D3246-92, Standard Test Method for Sulfur in Petroleum
Gas by Oxidative Microcoulometry, IBR approved for Sec.  60.335(b).
    (127) ASTM D3246-96, Standard Test Method for Sulfur in Petroleum
Gas by Oxidative Microcoulometry, IBR approved for Sec.  60.335(b).
    (128) ASTM D3246-05, Standard Test Method for Sulfur in Petroleum
Gas by Oxidative Microcoulometry, IBR approved for Sec.  60.4415(a)(1).
    (129) ASTM D3270-73T, Standard Test Methods for Analysis for
Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated
Method), IBR approved for appendix A-5 to part 60: Method 13A, Section
16.1.
    (130) ASTM D3270-80, Standard Test Methods for Analysis for
Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated
Method), IBR approved for appendix A-5 to part 60: Method 13A, Section
16.1.
    (131) ASTM D3270-91, Standard Test Methods for Analysis for
Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated
Method), IBR approved for appendix A-5 to part 60: Method 13A, Section
16.1.
    (132) ASTM D3270-95, Standard Test Methods for Analysis for
Fluoride Content of the Atmosphere and Plant Tissues (Semiautomated
Method), IBR approved for appendix A-5 to part 60: Method 13A, Section
16.1.
    (133) ASTM D3286-85, Standard Test Method for Gross Calorific Value
of Coal and Coke by the Isoperibol Bomb Calorimeter, IBR approved for
appendix A-7 to part 60: Method 19, Section <IP_ADDRESS>.3.
    (134) ASTM D3286-96, Standard Test Method for Gross Calorific Value
of Coal and Coke by the Isoperibol Bomb Calorimeter, IBR approved for
appendix A-7 to part 60: Method 19, Section <IP_ADDRESS>.3.
    (135) ASTM D3370-76, Standard Practices for Sampling Water, IBR
approved for Sec.  60.564(j).
    (136) ASTM D3370-95a, Standard Practices for Sampling Water, IBR
approved for Sec.  60.564(j).
    (137) ASTM D3588-98 (Reapproved 2003), Standard Practice for
Calculating Heat Value, Compressibility Factor, and Relative Density of
Gaseous Fuels, (Approved May 10, 2003), IBR approved for Sec. Sec.
60.107a(d) and 60.5413(d).
    (138) ASTM D3699-08, Standard Specification for Kerosine, including
Appendix X1, (Approved September 1, 2008), IBR approved for Sec. Sec.
60.41b and 60.41c.
    (139) ASTM D3792-79, Standard Test Method for Water Content of
Water-Reducible Paints by Direct Injection into a Gas Chromatograph,
IBR approved for appendix A-7 to part 60: Method 24, Section 6.3.
    (140) ASTM D3792-91, Standard Test Method for Water Content of
Water-Reducible Paints by Direct Injection into a Gas Chromatograph,
IBR approved for appendix A-7 to part 60: Method 24, Section 6.3.
    (141) ASTM D4017-81, Standard Test Method for Water in Paints and
Paint Materials by the Karl Fischer Titration Method, IBR approved for
appendix A-7 to part 60: Method 24, Section 6.4.
    (142) ASTM D4017-90, Standard Test Method for Water in Paints and
Paint Materials by the Karl Fischer Titration Method, IBR approved for
appendix A-7 to part 60: Method 24, Section 6.4.
    (143) ASTM D4017-96a, Standard Test Method for Water in Paints and
Paint Materials by the Karl Fischer Titration Method, IBR approved for
appendix A-7 to part 60: Method 24, Section 6.4.
    (144) ASTM D4057-81, Standard Practice for Manual Sampling of
Petroleum and Petroleum Products, IBR approved for appendix A-7 to part
60: Method 19, Section <IP_ADDRESS>.3.
    (145) ASTM D4057-95, Standard Practice for Manual Sampling of
Petroleum and Petroleum Products, IBR approved for appendix A-7 to part
60: Method 19, Section <IP_ADDRESS>.3.
    (146) ASTM D4057-95 (Reapproved 2000), Standard Practice for Manual
Sampling of Petroleum and Petroleum Products, IBR approved for Sec.
60.4415(a).
    (147) ASTM D4084-82, Standard Test Method for Analysis of Hydrogen

Sulfide in Gaseous Fuels (Lead Acetate Reaction Rate Method), IBR
approved for Sec.  60.334(h).
    (148) ASTM D4084-94, Standard Test Method for Analysis of Hydrogen
Sulfide in Gaseous Fuels (Lead Acetate Reaction Rate Method), IBR
approved for Sec.  60.334(h).
    (149) ASTM D4084-05, Standard Test Method for Analysis of Hydrogen
Sulfide in Gaseous Fuels (Lead Acetate Reaction Rate Method), IBR
approved for Sec. Sec.  60.4360 and 60.4415(a).
    (150) ASTM D4177-95, Standard Practice for Automatic Sampling of
Petroleum and Petroleum Products, IBR approved for appendix A-7 to part
60: Method 19, Section <IP_ADDRESS>.1.
    (151) ASTM D4177-95 (Reapproved 2000), Standard Practice for
Automatic Sampling of Petroleum and Petroleum Products, IBR approved
for Sec.  60.4415(a).
    (152) ASTM D4239-85, Standard Test Methods for Sulfur in the
Analysis Sample of Coal and Coke Using High Temperature Tube Furnace
Combustion Methods, IBR approved for appendix A-7 to part 60: Method
19, Section <IP_ADDRESS>.3.
    (153) ASTM D4239-94, Standard Test Methods for Sulfur in the
Analysis Sample of Coal and Coke Using High Temperature Tube Furnace
Combustion Methods, IBR approved for appendix A-7 to part 60: Method
19, Section <IP_ADDRESS>.3.
    (154) ASTM D4239-97, Standard Test Methods for Sulfur in the
Analysis Sample of Coal and Coke Using High Temperature Tube Furnace
Combustion Methods, IBR approved for appendix A-7 to part 60: Method
19, Section <IP_ADDRESS>.3.
    (155) ASTM D4294-02, Standard Test Method for Sulfur in Petroleum
and Petroleum Products by Energy-Dispersive X-Ray Fluorescence
Spectrometry, IBR approved for Sec.  60.335(b).
    (156) ASTM D4294-03, Standard Test Method for Sulfur in Petroleum
and Petroleum Products by Energy-Dispersive X-Ray Fluorescence
Spectrometry, IBR approved for Sec.  60.4415(a).
    (157) ASTM D4442-84, Standard Test Methods for Direct Moisture
Content Measurement in Wood and Wood-base Materials, IBR approved for
appendix A-8 to part 60: Method 28, Section 16.1.1.
    (158) ASTM D4442-92, Standard Test Methods for Direct Moisture
Content Measurement in Wood and Wood-base Materials, IBR approved for
appendix A-8 to part 60: Method 28, Section 16.1.1.
    (159) ASTM D4444-92, Standard Test Methods for Use and Calibration
of Hand-Held Moisture Meters, IBR approved for appendix A-8 to part 60:
Method 28, Section 16.1.1.
    (160) ASTM D4457-85 (Reapproved 1991), Test Method for
Determination of Dichloromethane and 1,1,1-Trichloroethane in Paints
and Coatings by Direct Injection into a Gas Chromatograph, IBR approved
for appendix A-7 to part 60: Method 24, Section 6.5.
    (161) ASTM D4468-85 (Reapproved 2000), Standard Test Method for
Total Sulfur in Gaseous Fuels by Hydrogenolysis and Rateometric
Colorimetry, IBR approved for Sec. Sec.  60.335(b) and 60.4415(a).
    (162) ASTM D4468-85 (Reapproved 2006), Standard Test Method for
Total Sulfur in Gaseous Fuels by Hydrogenolysis and Rateometric
Colorimetry, (Approved June 1, 2006), IBR approved for Sec.
60.107a(e).
    (163) ASTM D4629-02, Standard Test Method for Trace Nitrogen in
Liquid Petroleum Hydrocarbons by Syringe/Inlet Oxidative Combustion and
Chemiluminescence Detection, IBR approved for Sec. Sec.  60.49b(e) and
60.335(b).
    (164) ASTM D4809-95, Standard Test Method for Heat of Combustion of
Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method), IBR
approved for Sec. Sec.  60.18(f), 60.485(g), 60.485a(g), 60.564(f),
60.614(d), 60.664(e), and 60.704(d).
    (165) ASTM D4809-06, Standard Test Method for Heat of Combustion of
Liquid Hydrocarbon Fuels by Bomb Calorimeter (Precision Method),
(Approved December 1, 2006), IBR approved for Sec.  60.107a(d).
    (166) ASTM D4810-88 (Reapproved 1999), Standard Test Method for
Hydrogen Sulfide in Natural Gas Using Length of Stain Detector Tubes,
IBR approved for Sec. Sec.  60.4360 and 60.4415(a).
    (167) ASTM D4891-89 (Reapproved 2006) Standard Test Method for
Heating Value of Gases in Natural Gas Range by Stoichiometric
Combustion, (Approved June 1, 2006), IBR approved for Sec. Sec.
60.107a(d) and 60.5413(d).
    (168) ASTM D5287-97 (Reapproved 2002), Standard Practice for
Automatic Sampling of Gaseous Fuels, IBR approved for Sec.  60.4415(a).
    (169) ASTM D5403-93, Standard Test Methods for Volatile Content of
Radiation Curable Materials, IBR approved for appendix A-7 to part 60:
Method 24, Section 6.6.
    (170) ASTM D5453-00, Standard Test Method for Determination of
Total Sulfur in Light Hydrocarbons, Motor Fuels and Oils by Ultraviolet
Fluorescence, IBR approved for Sec.  60.335(b).
    (171) ASTM D5453-05, Standard Test Method for Determination of
Total Sulfur in Light Hydrocarbons, Motor Fuels and Oils by Ultraviolet
Fluorescence, IBR approved for Sec.  60.4415(a).
    (172) ASTM D5504-01, Standard Test Method for Determination of
Sulfur Compounds in Natural Gas and Gaseous Fuels by Gas Chromatography
and Chemiluminescence, IBR approved for Sec. Sec.  60.334(h) and
60.4360.
    (173) ASTM D5504-08, Standard Test Method for Determination of
Sulfur Compounds in Natural Gas and Gaseous Fuels by Gas Chromatography
and Chemiluminescence, (Approved June 15, 2008), IBR approved for
Sec. Sec.  60.107a(e) and 60.5413(d).
    (174) ASTM D5762-02, Standard Test Method for Nitrogen in Petroleum
and Petroleum Products by Boat-Inlet Chemiluminescence, IBR approved
for Sec.  60.335(b).
    (175) ASTM D5865-98, Standard Test Method for Gross Calorific Value
of Coal and Coke, IBR approved for Sec. Sec.  60.45(f) and 60.46(c),
and appendix A-7 to part 60: Method 19, Section <IP_ADDRESS>.3.
    (176) ASTM D5865-10, Standard Test Method for Gross Calorific Value
of Coal and Coke, (Approved January 1, 2010), IBR approved for
Sec. Sec.  60.45(f), 60.46(c), and appendix A-7 to part 60: Method 19,
section <IP_ADDRESS>.3.
    (177) ASTM D6216-98, Standard Practice for Opacity Monitor
Manufacturers to Certify Conformance with Design and Performance
Specifications, IBR approved for appendix B to part 60: Performance
Specification 1.
    (178) ASTM D6228-98, Standard Test Method for Determination of
Sulfur Compounds in Natural Gas and Gaseous Fuels by Gas Chromatography
and Flame Photometric Detection, IBR approved for Sec.  60.334(h).
    (179) ASTM D6228-98 (Reapproved 2003), Standard Test Method for
Determination of Sulfur Compounds in Natural Gas and Gaseous Fuels by
Gas Chromatography and Flame Photometric Detection, IBR approved for
Sec. Sec.  60.4360 and 60.4415.
    (180) ASTM D6348-03, Standard Test Method for Determination of
Gaseous Compounds by Extractive Direct Interface Fourier Transform
Infrared (FTIR) Spectroscopy, (Approved October 1, 2003), IBR approved
for Sec.  60.73a(b), table 7 to subpart IIII, and table 2 to subpart
JJJJ.
    (181) ASTM D6366-99, Standard Test Method for Total Trace Nitrogen
and Its Derivatives in Liquid Aromatic Hydrocarbons by Oxidative
Combustion and Electrochemical Detection, IBR approved for Sec.
60.335(b)(9).

    (182) ASTM D6420-99 (Reapproved 2004), Standard Test Method for
Determination of Gaseous Organic Compounds by Direct Interface Gas
Chromatography-Mass Spectrometry, (Approved October 1, 2004), IBR
approved for Sec.  60.107a(d) and table 2 to subpart JJJJ.
    (183) ASTM D6522-00, Standard Test Method for Determination of
Nitrogen Oxides, Carbon Monoxide, and Oxygen Concentrations in
Emissions from Natural Gas-Fired Reciprocating Engines, Combustion
Turbines, Boilers, and Process Heaters Using Portable Analyzers, IBR
approved for Sec.  60.335(a).
    (184) ASTM D6522-00 (Reapproved 2005), Standard Test Method for
Determination of Nitrogen Oxides, Carbon Monoxide, and Oxygen
Concentrations in Emissions from Natural Gas-Fired Reciprocating
Engines, Combustion Turbines, Boilers, and Process Heaters Using
Portable Analyzers, (Approved October 1, 2005), IBR approved for table
2 to subpart JJJJ, and Sec. Sec.  60.5413(b) and (d).
    (185) ASTM D6667-01, Standard Test Method for Determination of
Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum
Gases by Ultraviolet Fluorescence, IBR approved for Sec.  60.335(b).
    (186) ASTM D6667-04, Standard Test Method for Determination of
Total Volatile Sulfur in Gaseous Hydrocarbons and Liquefied Petroleum
Gases by Ultraviolet Fluorescence, IBR approved for Sec.  60.4415(a).
    (187) ASTM D6751-11b, Standard Specification for Biodiesel Fuel
Blend Stock (B100) for Middle Distillate Fuels, including Appendices X1
through X3, (Approved July 15, 2011), IBR approved for Sec. Sec.
60.41b and 60.41c.
    (188) ASTM D6784-02, Standard Test Method for Elemental, Oxidized,
Particle-Bound and Total Mercury in Flue Gas Generated from Coal-Fired
Stationary Sources (Ontario Hydro Method), IBR approved for Sec.
60.56c(b) and appendix B to part 60: Performance Specification 12A,
Section 8.6.2.
    (189) ASTM D6784-02 (Reapproved 2008) Standard Test Method for
Elemental, Oxidized, Particle-Bound and Total Mercury in Flue Gas
Generated from Coal-Fired Stationary Sources (Ontario Hydro Method),
(Approved April 1, 2008), IBR approved for Sec. Sec.  60.2165(j) and
60.2730(j), tables 1, 5, 6 and 8 to subpart CCCC, and tables 2, 6, 7,
and 9 to subpart DDDD, Sec. Sec.  60.4900(b), 60.5220(b), tables 1 and
2 to subpart LLLL, and tables 2 and 3 to subpart MMMM.
    (190) ASTM D7467-10, Standard Specification for Diesel Fuel Oil,
Biodiesel Blend (B6 to B20), including Appendices X1 through X3,
(Approved August 1, 2010), IBR approved for Sec. Sec.  60.41b and
60.41c.
    (191) ASTM E168-67, General Techniques of Infrared Quantitative
Analysis, IBR approved for Sec. Sec.  60.485a(d), 60.593(b),
60.593a(b), and 60.632(f).
    (192) ASTM E168-77, General Techniques of Infrared Quantitative
Analysis, IBR approved for Sec. Sec.  60.485a(d), 60.593(b),
60.593a(b), and 60.632(f).
    (193) ASTM E168-92, General Techniques of Infrared Quantitative
Analysis, IBR approved for Sec. Sec.  60.485a(d)(1), 60.593(b)(2),
60.593a(b)(2), 60.632(f), and 60.5400.
    (194) ASTM E169-63, General Techniques of Ultraviolet Quantitative
Analysis, IBR approved for Sec. Sec.  60.485a(d), 60.593(b),
60.593a(b), and 60.632(f) .
    (195) ASTM E169-77, General Techniques of Ultraviolet Quantitative
Analysis, IBR approved for Sec. Sec.  60.485a(d), 60.593(b), and
60.593a(b), 60.632(f).
    (196) ASTM E169-93, General Techniques of Ultraviolet Quantitative
Analysis, (Approved May 15, 1993), IBR approved for Sec. Sec.
60.485a(d), 60.593(b), 60.593a(b), 60.632(f), and 60.5400(f).
    (197) ASTM E260-73, General Gas Chromatography Procedures, IBR
approved for Sec. Sec.  60.485a(d), 60.593(b), 60.593a(b), and
60.632(f).
    (198) ASTM E260-91, General Gas Chromatography Procedures, (IBR
approved for Sec. Sec.  60.485a(d), 60.593(b), 60.593a(b), and
60.632(f).
    (199) ASTM E260-96, General Gas Chromatography Procedures,
(Approved April 10, 1996), IBR approved for Sec. Sec.  60.485a(d),
60.593(b), 60.593a(b), 60.632(f), 60.5400(f), and 60.5406(b).
    (200) ASTM E1584-11, Standard Test Method for Assay of Nitric Acid,
(Approved August 1, 2011), IBR approved for Sec.  60.73a(c).
    (201) ASTM UOP539-97, Refinery Gas Analysis by Gas Chromatography,
(Copyright 1997), IBR approved for Sec.  60.107a(d).
    (h) Association of Official Analytical Chemists, 1111 North 19th
Street, Suite 210, Arlington, VA 22209.
    (1) AOAC Method 9, Official Methods of Analysis of the Association
of Official Analytical Chemists (AOAC), 11th edition, 1970, pp. 11-12,
IBR approved for Sec. Sec.  60.204(b), 60.214(b), 60.224(b), and
60.234(b).
    (2) [Reserved]
    (i) U.S. Environmental Protection Agency, 1200 Pennsylvania Avenue
NW., Washington, DC 20460,<PHONE_NUMBER>, http://www.epa.gov.
    (1) EPA-454/R-98-015, Office of Air Quality Planning and Standards
(OAQPS) Fabric Filter Bag Leak Detection Guidance, September 1997, IBR
approved for Sec. Sec.  60.2145(r), 60.2710(r), 60.4905(b), and
60.5225(b).
    (2) [Reserved]
    (j) The Gas Processors Association, 6526 East 60th Street, Tulsa,
OK 74145; also available through Information Handling Services, 15
Inverness Way East, PO Box 1154, Englewood, CO 80150-1154. You may
inspect a copy at the EPA's Air and Radiation Docket and Information
Center, Room 3334, 1301 Constitution Ave. NW., Washington, DC 20460.
    (1) Gas Processors Association Standard 2172-09, Calculation of
Gross Heating Value, Relative Density, Compressibility and Theoretical
Hydrocarbon Liquid Content for Natural Gas Mixtures for Custody
Transfer (2009), IBR approved for Sec.  60.107a(d).
    (2) Gas Processors Association Standard 2261-00, Analysis for
Natural Gas and Similar Gaseous Mixtures by Gas Chromatography (2000),
IBR approved for Sec.  60.107a(d).
    (3) Gas Processors Association Standard 2377-86, Test for Hydrogen
Sulfide and Carbon Dioxide in Natural Gas Using Length of Stain Tubes,
1986 Revision, IBR approved for Sec. Sec.  60.105(b), 60.107a(b),
60.334(h), 60.4360, and 60.4415(a).
    (k) International Organization for Standardization (ISO) available
through IHS Inc., 15 Inverness Way East, Englewood, CO 80112.
    (1) ISO 8178-4: 1996(E), Reciprocating Internal Combustion
Engines--Exhaust Emission Measurement--part 4: Test Cycles for
Different Engine Applications, IBR approved for Sec.  60.4241(b).
    (2) [Reserved]
    (l) International Organization for Standardization (ISO), 1, ch. de
la Voie-Creuse, Case postale 56, CH-1211 Geneva 20, Switzerland, +41 22
749 01 11, http://www.iso.org/iso/home.htm.
    (1) ISO 8316: Measurement of Liquid Flow in Closed Conduits--Method
by Collection of the Liquid in a Volumetric Tank (1987-10-01)--First
Edition, IBR approved for Sec.  60.107a(d).
    (2) [Reserved]
    (m) This material is available for purchase from the National
Technical Information Services (NTIS), 5285 Port Royal Road,
Springfield, Virginia 22161. You may inspect a copy at the EPA's Air
and Radiation Docket and Information Center (Docket A-91-61, Item IV-J-
125), Room M-1500, 1200 Pennsylvania Ave. NW., Washington, DC 20460.
    (1) OMB Bulletin No. 93-17: Revised Statistical Definitions for
Metropolitan Areas. Office of Management and

Budget, June 30, 1993. NTIS No. PB 93-192-664. IBR approved for Sec.
60.31e.
    (2) [Reserved]
    (n) North American Electric Reliability Corporation, 1325 G Street
NW., Suite 600, Washington, DC 20005-3801, http://www.nerc.com.
    (1) North American Electric Reliability Corporation Reliability
Standard EOP-002-3, Capacity and Energy Emergencies, updated November
19, 2012, IBR approved for Sec. Sec.  60.4211(f) and 60.4243(d). Also
available online: http://www.nerc.com/files/EOP-002-3_1.pdf.
    (2) [Reserved]
    (o) Technical Association of the Pulp and Paper Industry (TAPPI),
Dunwoody Park, Atlanta, GA 30341.
    (1) TAPPI Method T624 os-68, IBR approved for Sec.  60.285(d).
    (2) [Reserved]
    (p) Underwriter's Laboratories, Inc. (UL), 333 Pfingsten Road,
Northbrook, IL 60062.
    (1) UL 103, Sixth Edition revised as of September 3, 1986, Standard
for Chimneys, Factory-built, Residential Type and Building Heating
Appliance, IBR approved for Appendix A-8 to part 60.
    (2) [Reserved]
    (q) Water Pollution Control Federation (WPCF), 2626 Pennsylvania
Avenue NW., Washington, DC 20037.
    (1) Method 209A, Total Residue Dried at 103-105 [deg]C, in Standard
Methods for the Examination of Water and Wastewater, 15th Edition,
1980, IBR approved for Sec.  60.683(b).
    (2) [Reserved]
    (r) West Coast Lumber Inspection Bureau, 6980 SW. Barnes Road,
Portland, OR 97223.
    (1) West Coast Lumber Standard Grading Rules No. 16, pages 5-21, 90
and 91, September 3, 1970, revised 1984, IBR approved for Appendix A-8
to part 60.
    (2) [Reserved]

Subpart Db--[Amended]

0
7. Amend Sec.  60.46b by revising paragraphs (f)(1)(ii) and (h)(1) and
(h)(2) to read as follows:

Sec.  60.46b  Compliance and performance test methods and procedures
for particulate matter and nitrogen oxides.

* * * * *
    (f) * * *
    (1) * * *
    (ii) Method 7E of appendix A of this part or Method 320 of appendix
A of part 63 shall be used to determine the NOX
concentrations. Method 3A or 3B of appendix A of this part shall be
used to determine O2 concentration.
* * * * *
    (h) * * *
    (1) Conduct an initial performance test as required under Sec.
60.8 over a minimum of 24 consecutive steam generating unit operating
hours at maximum heat input capacity to demonstrate compliance with the
NOX emission standards under Sec.  60.44b using Method 7,
7A, or 7E of appendix A of this part, Method 320 of appendix A of part
63 of this chapter, or other approved reference methods; and
    (2) Conduct subsequent performance tests once per calendar year or
every 400 hours of operation (whichever comes first) to demonstrate
compliance with the NOX emission standards under Sec.
60.44b over a minimum of 3 consecutive steam generating unit operating
hours at maximum heat input capacity using Method 7, 7A, or 7E of
appendix A of this part, Method 320 of appendix A of part 63, or other
approved reference methods.
* * * * *

0
8. Amend Sec.  60.47b by revising paragraph (b)(2) to read as follows:

Sec.  60.47b  Emission monitoring for sulfur dioxide.

* * * * *
    (b) * * *
    (2) Measuring SO2 according to Method 6B of appendix A
of this part at the inlet or outlet to the SO2 control
system. An initial stratification test is required to verify the
adequacy of the sampling location for Method 6B of appendix A of this
part. The stratification test shall consist of three paired runs of a
suitable SO2 and CO2 measurement train operated
at the candidate location and a second similar train operated according
to the procedures in Section 3.2 and the applicable procedures in
Section 7 of Performance Specification 2. Method 6B of appendix A of
this part, Method 6A of appendix A of this part, or a combination of
Methods 6 and 3 or 3B of appendix A of this part or Methods 6C or
Method 320 of appendix A of part 63 of this chapter and 3A of appendix
A of this part are suitable measurement techniques. If Method 6B of
appendix A of this part is used for the second train, sampling time and
timer operation may be adjusted for the stratification test as long as
an adequate sample volume is collected; however, both sampling trains
are to be operated similarly. For the location to be adequate for
Method 6B of appendix A of this part, 24-hour tests, the mean of the
absolute difference between the three paired runs must be less than 10
percent.
* * * * *

Subpart Ec--[Amended]

0
9. Amend Sec.  60.51c by revising the definition of ``Medical/
infectious waste'' to read as follows:

Sec.  60.51c  Definitions.

* * * * *
    Medical/infectious waste means any waste generated in the
diagnosis, treatment, or immunization of human beings or animals, in
research pertaining thereto, or in the production or testing of
biologicals that are listed in paragraphs (1) through (7) of this
definition. The definition of medical/infectious waste does not include
hazardous waste identified or listed under the regulations in part 261
of this chapter; household waste, as defined in Sec.  261.4(b)(1) of
this chapter; ash from incineration of medical/infectious waste, once
the incineration process has been completed; human corpses, remains,
and anatomical parts that are intended for interment or cremation; and
domestic sewage materials identified in Sec.  261.4(a)(1) of this
chapter.
    (1) Cultures and stocks of infectious agents and associated
biologicals, including: Cultures from medical and pathological
laboratories; cultures and stocks of infectious agents from research
and industrial laboratories; wastes from the production of biologicals;
discarded live and attenuated vaccines; and culture dishes and devices
used to transfer, inoculate, and mix cultures.
    (2) Human pathological waste, including tissues, organs, and body
parts and body fluids that are removed during surgery or autopsy, or
other medical procedures, and specimens of body fluids and their
containers.
    (3) Human blood and blood products including:
    (i) Liquid waste human blood;
    (ii) Products of blood;
    (iii) Items saturated and/or dripping with human blood; or
    (iv) Items that were saturated and/or dripping with human blood
that are now caked with dried human blood; including serum, plasma, and
other blood components, and their containers, which were used or
intended for use in either patient care, testing and laboratory
analysis or the development of pharmaceuticals. Intravenous bags are
also included in this category.
    (4) Sharps that have been used in animal or human patient care or
treatment or in medical, research, or industrial laboratories,
including hypodermic needles, syringes (with or without the attached
needle), pasteur pipettes, scalpel blades, blood vials, needles with
attached tubing, and

culture dishes (regardless of presence of infectious agents). Also
included are other types of broken or unbroken glassware that were in
contact with infectious agents, such as used slides and cover slips.
    (5) Animal waste including contaminated animal carcasses, body
parts, and bedding of animals that were known to have been exposed to
infectious agents during research (including research in veterinary
hospitals), production of biologicals or testing of pharmaceuticals.
    (6) Isolation wastes including biological waste and discarded
materials contaminated with blood, excretions, exudates, or secretions
from humans who are isolated to protect others from certain highly
communicable diseases, or isolated animals known to be infected with
highly communicable diseases.
    (7) Unused sharps including the following unused, discarded sharps:
hypodermic needles, suture needles, syringes, and scalpel blades.
* * * * *

Subpart H--[Amended]

0
10. Amend Sec.  60.84 by revising the equation in paragraph (d) to read
as follows:

Sec.  60.84  Emission monitoring.

* * * * *
    (d) * * *
Es = (Cs S)/[0.265 - (0.0126 %O2) - (A
%CO2)]
* * * * *

Subpart O--[Amended]

0
11. Amend Sec.  60.154 by revising the introductory text to paragraph
(b)(5) to read as follows:

Sec.  60.154  Test methods and procedures.

* * * * *
    (b) * * *
    (5) Samples of the sludge charged to the incinerator shall be
collected in nonporous jars at the beginning of each run and at
approximately 1-hour intervals thereafter until the test ends; and
``2540 G. Total, Fixed, and Volatile Solids in Solid and Semisolid
Samples, in Standard Methods for the Examination of Water and
Wastewater, 20th Edition, 1998'' (incorporated by reference--see Sec.
60.17) shall be used to determine dry sludge content of each sample
(total solids residue), except that:
* * * * *

Subpart BB--[Amended]

0
12. Amend Sec.  60.284 by revising the equation in paragraph (c)(3) to
read as follows:

Sec.  60.284  Monitoring of emissions and operations.

* * * * *
    (c) * * *
    (3) * * *
    Ccorr = C meas x (21- X)/(21- Y)
    * * *
* * * * *

Subpart GG--[Amended]

0
13. Amend Sec.  60.335 by revising the terms Pr and
Po for the equation in paragraph (b)(1) to read as follows:

Sec.  60.335  Test methods and procedures.

* * * * *
    (b) * * *
    (1) * * *
    Pr = reference combustor inlet absolute pressure at
101.3 kilopascals ambient pressure. Alternatively, you may use 760 mm
Hg (29.92 in Hg),
    Po = observed combustor inlet absolute pressure at test,
mm Hg. Alternatively, you may use the barometric pressure for the date
of the test,
* * * * *

Subpart KK--[Amended]

0
14. Amend Sec.  60.374 by revising paragraphs (b)(1), (b)(2), and
(c)(2) to read as follows:

Sec.  60.374  Test methods and procedures.

* * * * *
    (b) * * *
    (1) Method 12 or Method 29 shall be used to determine the lead
concentration (CPb) and, if applicable, the volumetric flow
rate (Qsda) of the effluent gas. The sampling time and
sample volume for each run shall be at least 60 minutes and 0.85 dscm
(30 dscf).
    (2) When different operations in a three-process operation facility
are ducted to separate control devices, the lead emission concentration
(C) from the facility shall be determined as follows:
[GRAPHIC] [TIFF OMITTED] TR27FE14.006

Where:

C = concentration of lead emissions for the entire facility, mg/dscm
(gr/dscf).
Ca = concentration of lead emissions from facility ``a'',
mg/dscm (gr/dscf).
Qsda = volumetric flow rate of effluent gas from facility
``a'', dscm/hr (dscf/hr).
N = total number of control devices to which separate operations in
the facility are ducted.
* * * * *
    (c) * * *
    (2) Method 12 or Method 29 shall be used to determine the lead
concentration (CPb) and the volumetric flow rate
(Qsd) of the effluent gas. The sampling time and sample
volume for each run shall be at least 60 minutes and 0.85 dscm (30
dscf).
* * * * *

Subpart LL--[Amended]

0
15. Amend Sec.  60.382 by revising paragraph (a)(1) to read as follows:

Sec.  60.382  Standard for particulate matter.

    (a) * * *
    (1) Contain particulate matter in excess of 0.05 grams per dry
standard cubic meter (0.05 g/dscm).
* * * * *

0
16. Amend Sec.  60.386 by revising paragraph (b)(2) to read as follows:

Sec.  60.386  Test methods and procedures.

* * * * *
    (b) * * *
    (2) Method 9 and the procedures in Sec.  60.11 shall be used to
determine opacity from stack emissions and process fugitive emissions.
The observer shall read opacity only when emissions are clearly
identified as emanating solely from the affected facility being
observed. A single visible emission observer may conduct visible
emission observations for up to three fugitive, stack, or vent emission
points within a 15-second interval. This option is subject to the
following limitations:
    (i) No more than three emission points are read concurrently;
    (ii) All three emission points must be within a 70[deg] viewing
sector or angle in front of the observer such that the proper sun