 [Federal Register Volume 80, Number 205 (Friday, October 23, 2015)] [Rules and Regulations] [Page 64354] [FR Doc No: C1-2015-26449]

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DEPARTMENT OF HOMELAND SECURITY

Federal Emergency Management Agency

44 CFR Part 64

[Docket ID FEMA-2015-0001; Internal Agency Docket No. FEMA-8405]

Suspension of Community Eligibility

Correction

    In rule document 2015-26449 beginning on page 63130 in the issue of  Monday, October 19, 2015, make the following correction:

Sec.  64.6  [Corrected]

    On page 63131, in the table, in the first column, in the Region VII  entry ``Kansas: 23 Hanover, City of, Washington County'' should read  ``Kansas: Hanover, City of, Washington County''. [FR Doc. C1-2015-26449 Filed 10-22-15; 8:45 am] BILLING CODE 1505-01-D


Steve Whitehead < stevewhitehead@ fsicorp. com> Received Date: 8/ 12/ 03 15: 03 Transmission Date To: Michael Samulski/ AA/ USEPA/ US@ EPA cc: Subject: Resin Data Attached is the resin data I want to discuss with you. At present, we have 2 coatings. One from Ameron, the other from Crosslink Technology Surface area of the bottles are 0.0425 m2 All mass measurements are in grams If cell is highlighted green, the seal was found broken and an attempt was made to reseal the Red text denotes an additional alu seal was required to achieve a seal, and so 0.242 If cell is highlighted yellow, the bottle was extensively damaged as to make retrieval of data For the Ameron coating ( AMC), two layers of Amercoat ( 733: 100), and one layer of Amershie applied to the inside and outside of the bottles following the steps for coating the CRC.

Three bottles from each type of Fluorine treatment and fuel will be coated ( 72 bottles), with t uncoated bottles ( 3), and three uncoated bottles ( 32, UCB) added to the testing for control pu 111 bottles. For the Crosslink Technology coat ( CRC), the ratio is 100: 23. The inside of the bottles will b bottle, then turning the bottle over for five minutes ( subject to change), and putting the bottle cure for at least 24 hrs before permeation testing One coat of resin will be applied to the outside of the bottles with a paint brush, and will be a least 24 hrs the bottle g was subtracted to correct for the additional seal ta impossible hield ( 4: 1) will be h three untreated, l purposes; for a total of ll by coated by filling the ttle upright, allowing it to allowed to cure for at RH 80% RH 98% RH 79% RH 84% RH 96% RH 58%

ID# 07/ 11/ 03 7/ 14/ 03 07/ 17/ 03 7/ 21/ 03 GH NC 01 397.750 386.099 384.113 375.425 366.803 354.584 GH NC 02 392.760 381.982 380.040 371.705 362.932 351.277 GH NC 03 397.637 387.393 385.574 377.919 362.200 359.562 PG NC 01 366.053 355.616 353.558 344.626 335.716 322.829 PG NC 02 381.800 380.680 368.591 359.345 350.237 337.084 PG NC 03 380.544 369.882 367.793 358.482 344.211 336.582 PG OA 06 377.739 361.475 359.011 347.712 335.680 320.300 PG OA 02 381.546 381.404 381.111 381.180 380.887 380.503 PG OB 01 386.000 385.948 385.955 385.943 385.942 385.897 PG OB 02 386.148 381.895 381.833 381.547 381.215 380.767 PG ( GH) OB 09 401.452 400.714 400.689 400.586 400.453 400.303 PG ( GH) OB 07 390.610 390.379 390.266 389.884 389.469 388.966 GH OA 17 395.495 393.450 393.045 391.776 390.713 389.348 GH OB 01 390.126 388.867 388.729 388.131 387.608 386.952 GH OA 02 383.128 380.596 380.181 378.914 377.808 376.259 GH OA 07 398.733 396.390 395.901 394.355 392.985 391.314 PG IA& B 16 388.211 387.598 387.675 387.573 387.455 387.294 Weight after preconditioning Weight before preconditioning 07/ 11/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 30/ 03 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss ID# g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day GH NC 01 46.729 68.141 67.624 71.876 71.118 53.657 GH NC 02 45.694 65.373 68.808 68.559 70.541 52.491 GH NC 03 42.800 60.039 123.286 15.518 61.035 47.835 PG NC 01 48.424 70.055 69.882 75.806 76.506 54.945 PG NC 02 284.447 72.518 71.435 77.371 79.506 56.316 PG NC 03 49.153 73.027 111.929 44.876 78.565 55.667 PG OA 06 57.976 88.620 94.369 90.471 86.165 66.020 PG OA 02 6.894  0.541 2.298 2.259 2.329 1.785 PG OB 01  0.165 0.094 0.008 0.265 0.176 0.195 PG OB 02 1.459 2.243 2.604 2.635 3.024 0.198 PG ( GH) OB 09 0.588 0.808 1.043 0.882 0.835 0.676 PG ( GH) OB 07 2.659 2.996 3.255 2.959 3.635 0.921 GH OA 17 9.529 9.953 8.337 8.029 8.035 6.555 GH OB 01 3.247 4.690 4.102 3.859 4.082 3.334 GH OA 02 9.765 9.937 8.675 9.112 10.024 7.203 GH OA 07 11.506 12.125 10.745 9.829 9.988 8.373 PG IA& B 16  1.812 0.800 0.925 0.947 0.906 0.857 RH 85% RH 83% RH 95% RH 66% RH 79% 0 0 7/ 23/ 03 7/ 30/ 03 8/ 1/ 03 8/ 5/ 03 8/ 8/ 03 1/ 0/ 00 1/ 0/ 00 348.539 332.576 327.463 317.169 309.631 345.281 329.665 324.746 314.556 306.920 354.374 340.143 335.565 326.555 319.918 316.326 299.980 294.821 284.284 276.443 330.326 313.572 308.166 297.263 289.054 329.904 313.343 308.102 297.225 289.289 312.976 293.335 287.210 273.813 263.439 380.305 379.774 379.606 379.286 378.500 385.882 385.824 385.799 385.753 385.727 380.752 380.693 380.179 379.527 367.619 400.232 400.031 399.833 399.545 399.449 388.899 388.625 387.958 387.690 387.449 388.665 386.715 385.975 384.470 383.276 386.605 385.613 385.266 384.576 384.085 375.407 373.264 372.463 370.997 369.959 390.465 387.974 387.150 385.314 383.977 387.217 386.962 386.888 386.752 386.664 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 60.153 60.553 59.122 57.871 59.941 59.890 53.859 53.000 52.055 60.694 61.982 61.498 63.600 64.135 64.384 61.659 63.982 62.243 72.059 78.806 81.365 1.976 1.882 6.165 0.294 0.271 0.204 6.047 3.835 93.396 2.329 1.694 0.753 7.847 1.576 1.890 8.706 8.853 9.365 4.082 4.059 3.851 9.424 8.624 8.141 9.694 10.800 10.486 0.871 0.800 0.690 0 1/ 0/ 00 01/ 00/ 00 Weight loss g/ m2/ day Gasahol RH 80% RH 98%

inside barrier FSI# Coating type 1 F  16 CRC 31.123 36.295 5.172 2 F  17 CRC No longer able to test 3 F  18 CRC 31.330 41.807 10.477 4 F  52 AMC 34.071 66.696 32.625 357.985 356.552 5 F  53 AMC 31.257 68.400 37.143 380.515 6 F  54 AMC 31.405 71.332 39.927 7 F  88 SUP 31.445  31.445 425.768 423.082 8 F  89 SUP 33.675  33.675 394.662 390.770 9 F  90 SUP 31.121  31.121 417.006 414.042 10 F  124 51PC 200 33.593 36.707 3.114 374.489 373.108 11 F  125 51PC 200 33.478 36.606 3.128 378.365 377.136 12 F  126 51PC 200 31.223 35.090 3.867 343.200 342.034 13 F  160 CRT 30.931 36.792 5.861 361.041 361.052 14 F  161 CRT 31.274 38.604 7.330 366.501 365.400 15 F  162 CRT 33.819 42.008 8.189 364.762 363.948 16 F  181 51PC  500 32.720 45.061 12.341 338.831 337.935 17 F  182 51PC  500 31.796 44.638 12.842 348.130 347.334 18 F  183 51PC  500 32.104 44.973 12.869 352.470 351.239 Mass of coating Empty uncoated weight Weight after coat Weight after preconditioning Weight before preconditioning Gasahol 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 inside Weight loss Weight loss Weight loss Weight loss Weight loss barrier FSI# g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 4 F  52 AMC  1.388 0.949 0.933 0.876 0.706 5 F  53AMC 6 F  54AMC 7 F  88 SUP  0.471 0.361 0.439 0.300 0.341 8 F  89 SUP  1.600 2.047 1.757 2.041 2.835 9 F  90 SUP 5.529 3.004 0.729 0.588 4.329 10 F  124 51PC 200  1.459 0.651 0.941 1.618 7.353 11 F  125 51PC 200  0.212 0.282 0.792 0.459 0.482 12 F  126 51PC 200 0.118 0.525 0.533 0.341 0.471 13 F  160 CRT 0.282 0.290 1.286 1.076 1.600 14 F  161 CRT  1.694 0.392 1.169 0.618 0.706 15 F  162 CRT  1.106 2.596 0.690 0.306 0.318 16 F  181 51PC  500  2.071 0.729 1.122 0.682 0.776 17 F  182 51PC  500  2.376 0.580 1.067 0.765 0.824 18 F  183 51PC  500 5.365 1.161 0.996 1.459 2.059 RH 79% RH 84% RH 96% RH 58% RH 85% RH 96% RH 83% RH 95%

07/ 10/ 03 7/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 356.611 356.490 356.371 356.222 356.162 356.072 355.842 355.826 423.102 423.056 423.000 422.949 422.920 422.892 422.795 422.780 390.838 390.577 390.353 390.006 389.765 389.511 388.915 388.980 414.049 413.666 413.573 413.473 413.105 413.104 412.923 412.804 373.170 373.087 372.967 372.692 372.309 372.241 372.087 371.969 377.145 377.109 377.008 376.930 376.889 376.843 376.689 376.657 342.271 342.204 342.136 342.078 342.038 342.009 341.921 341.851 361.040 361.003 360.839 360.656 360.762 360.685 343.122 282.848 365.472 365.422 365.273 365.168 365.108 365.059 364.931 364.930 363.995 363.906 363.818 363.766 363.739 363.712 363.652 363.651 338.265 338.172 338.029 337.913 337.847 337.791 337.655 337.654 347.435 347.361 347.225 347.095 347.025 346.963 346.790 346.789 351.253 351.105 350.978 350.730 350.797 350.742 350.587 350.572 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 1.059 1.082 0.188 1.076 0.831 0.329 0.456 0.176 0.494 0.471 2.988 2.805 2.082 0.776 0.502 0.012 0.852 1.400 1.741 1.396 0.800 0.725 1.388 1.971 1.388 0.541 0.725 0.376 0.535 0.408 0.341 0.414 0.824 0.647 0.282 0.906 82.649 709.106 90.753 1.000 0.576 0.602 0.012 0.676 0.627 0.318 0.282 0.012 0.241 0.275 0.659 0.640 0.012 0.635 0.557 0.729 0.814 0.012 1.000 1.184 0.647 0.729 0.176 0.853 0.690 RH 66% RH 79%

08/ 05/ 03 08/ 08/ 03 355.643 355.537 422.696 422.636 388.848 388.784 412.508 412.330 371.634 371.457 376.566 376.514 341.741 341.705 267.420 Bottle Cracked 364.815 364.735 363.610 363.575 337.546 337.475 346.619 346.468 350.427 350.339 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 01/ 00/ 00 Weight loss g/ m2/ day Gasahol RH 80% RH 98% RH 79%

inside adhesion FSI# Coating type 07/ 10/ 03 1 F  4 CRC No Longer able to test 2 F  5 CRC 30.735 38.688 7.953 3 F  6 CRC No Longer able to test 4 F  40 AMC 33.391 89.795 56.404 402.993 399.848 399.738 5 F  41 AMC 30.955 65.858 34.903 363.902 360.050 360.631 6 F  42 AMC 33.269 78.612 45.343 410.136 408.167 408.030 7 F 76 SUP 33.494  33.494 403.509 401.746 401.973 8 F 77 SUP 30.611  30.611 412.541 410.362 410.407 9 F 78 SUP 33.375  33.375 10 F  112 51PC 200 30.961 34.601 3.640 359.205 351.954 351.880 11 F  113 51PC 200 33.562 37.054 3.492 390.441 386.206 385.900 12 F  114 51PC 200 33.325 36.916 3.591 302.666 300.520 300.421 13 F  148 CRT 30.549 38.890 8.341 366.151 364.015 364.005 14 F  149 CRT 30.898 37.727 6.829 366.302 364.524 364.520 15 F  150 CRT 33.286 40.813 7.527 379.246 377.667 377.903 16 F  184 51PC  500 33.467 48.817 15.350 351.205 342.849 341.682 17 F  185 51PC  500 33.411 49.097 15.686 298.482 290.570 289.268 18 F  186 51PC  500 30.797 46.354 15.557 356.939 349.546 348.248 Weight after preconditioning Empty uncoated weight Weight after coat Mass of coat Weight before preconditioning Gasahol 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 inside Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss adhesion FSI# Coating type g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 4 F  40 AMC 2.588 6.259 6.439 6.318 6.729 6.965 5 F  41 AMC  13.671 3.984 3.937 4.082 3.988 4.306 6 F  42 AMC 3.224 4.337 3.992 3.994 3.471 4.835 7 F 76 SUP  5.341 0.439 0.737 0.406 0.376 2.412 8 F 77 SUP  1.059 0.627 0.541 0.447 0.082 0.424 9 F 78 SUP 10 F  112 51PC 200 1.741 3.051 2.322 2.206 1.859 2.188 11 F  113 51PC 200 7.200 3.098 2.361 2.229 1.953 1.282 12 F  114 51PC 200 2.329 3.122 2.533 2.294 2.106 2.459 13 F  148 CRT 0.235 0.886 0.871 0.671 0.776 0.906 14 F  149 CRT 0.094 0.808 0.769 0.524 0.588 0.706 15 F  150 CRT  5.553 0.337 0.384 0.124 0.153 0.271 16 F  184 51PC  500 27.459 38.604 37.537 36.053 35.800 38.894 17 F  185 51PC  500 30.635 39.647 38.110 35.165 33.388 36.365 18 F  186 51PC  500 30.541 39.710 38.455 37.306 38.435 39.953 RH 84% RH 96% RH 58% RH 85% RH 96% RH 83% RH 95%

07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 398.940 398.119 397.045 396.473 395.881 394.565 394.008 360.123 359.621 358.927 358.588 358.222 357.343 357.000 407.477 406.968 406.289 405.994 405.583 404.714 404.370 401.917 401.823 401.754 401.722 401.517 401.297 401.185 410.327 410.258 410.182 410.175 410.139 410.110 410.092 351.491 351.195 350.820 350.662 350.476 350.012 349.830 385.505 385.204 384.825 384.659 384.550 383.982 383.794 300.023 299.700 299.310 299.131 298.922 298.410 298.208 363.892 363.781 363.667 363.601 363.524 363.388 363.337 364.417 364.319 364.230 364.180 364.120 364.007 363.950 377.860 377.811 377.790 377.777 377.754 377.721 377.705 336.760 331.974 325.845 322.802 319.496 311.325 308.231 284.213 279.354 273.376 270.538 267.447 260.146 257.479 343.185 338.282 331.940 328.673 325.277 317.105 314.053 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 6.193 6.553 6.082 6.353 4.136 4.035 3.900 4.157 4.089 4.047 3.876 4.000 1.035 1.318 0.771 1.867 0.136 0.212 0.135 0.188 2.184 2.141 1.959 2.173 2.673 2.212 2.329 2.949 2.409 2.376 2.271 2.502 0.640 0.600 0.594 0.549 0.532 0.671 0.518 0.525 0.155 0.188 0.147 0.204 38.452 36.400 34.912 35.741 34.358 31.376 29.841 30.525 38.456 35.906 34.253 35.922 RH 66% RH 79% 0.000 0.000 0.000 0.000 0.000 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 392.974 392.164 356.337 355.807 403.711 403.201 401.054 400.816 410.069 410.045 349.497 349.220 383.398 383.022 297.822 297.503 363.236 363.166 363.862 363.795 377.680 377.654 302.296 297.739 252.406 248.514 308.230 303.650 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 0.000 01/ 00/ 00 01/ 00/ 00 Weight loss g/ m2/ day Gasahol RH 80% RH 98%

inside A& B FSI# Coating type 1 F 28 CRC No Longer able to test 2 F 29 CRC No Longer able to test 3 F 30 CRC 33.950 40.240 6.290 4 F  64 AMC 33.985 74.085 40.100 376.043 370.188 5 F  65 AMC 31.486 73.689 42.203 404.126 168.075 6 F  66 AMC 31.521 67.362 35.841 369.059 367.136 7 F  100 SUP 31.247  31.247 389.153 387.295 8 F  101 SUP 31.004  31.004 382.266 370.865 9 F  102 SUP 30.768  30.768 10 F  136 51PC 200 31.310 35.440 4.130 372.573 371.354 11 F  137 51PC 200 31.193 32.290 1.097 384.949 381.765 12 F  138 51PC 200 31.373 35.514 4.141 355.855 353.687 13 F  172 CRT 31.211 37.342 6.131 369.172 367.816 14 F  173 CRT 33.411 39.630 6.219 379.267 377.920 15 F  174 CRT 33.443 39.689 6.246 356.867 356.704 16 F 187 51PC  500 32.042 45.056 13.014 362.631 360.398 17 F  188 51PC  500 29.237 42.953 13.716 341.620 340.614 18 F  189 51PC  500 29.496 42.533 13.037 386.898 385.275 Weight after preconditioning Empty uncoated weight Weight after coat Mass of coating Weight before preconditioning Gasahol 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 inside Weight loss Weight loss Weight loss Weight loss Weight loss A& B FSI# Coating type g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 4 F  64 AMC 0.071 0.643 0.886 0.865 0.788 5 F  65AMC 6 F  66 AMC 0.376 1.608 4.698 4.735 5.271 7 F  100 SUP 0.047 1.906 4.345 4.265 6.329 8 F  101 SUP  1.247 0.831 1.027 1.047 1.271 9 F  102 SUP 10 F  136 51PC 200 0.965 0.573 0.722 1.324 4.882 11 F  137 51PC 200  0.941 0.878 0.478 0.571 0.482 12 F  138 51PC 200  0.071 0.416 0.494 0.406 0.435 13 F  172 CRT 0.329 0.400 1.294 0.582 1.941 14 F  173 CRT  0.376 2.557 7.145 17.200 7.494 15 F  174 CRT  1.106 2.353 2.769 2.459 2.647 16 F 187 51PC  500  0.376 1.404 0.714 0.612 0.588 17 F  188 51PC  500 0.188 0.996 1.757 1.594 2.141 18 F  189 51PC  500 0.000 0.659 0.714 0.765 0.882 RH 79% RH 84% RH 96% RH 58% RH 85% RH 96% RH 83%

07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 370.185 370.103 369.990 369.843 369.776 369.700 369.511 168.008 86.141 367.120 366.915 366.558 365.753 365.547 365.214 387.535 387.292 386.980 386.255 385.717 385.449 384.609 370.918 370.812 370.681 370.503 370.395 370.297 370.048 371.555 371.482 371.390 371.165 370.750 370.698 370.533 381.805 381.693 381.632 381.535 381.494 381.447 381.336 353.690 353.637 353.574 353.505 353.468 353.400 353.282 368.044 367.993 367.828 367.729 367.564 367.446 367.287 377.936 377.610 376.941 374.017 373.380 372.887 371.768 356.751 356.451 356.098 355.680 355.697 355.656 355.245 360.414 360.235 360.144 360.040 359.990 359.937 359.796 340.606 340.479 340.255 339.984 340.044 339.961 339.751 385.275 385.191 385.100 384.970 384.895 384.456 384.143 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 0.894 0.889 0.424 0.688 0.604 3.918 1.539 1.253 1.584 3.153 3.953 4.976 11.741 20.110 1.153 1.172 0.906 1.153 1.027 0.612 0.776 0.576 0.682 0.588 0.553 0.522 0.388 1.800 2.706 0.800 0.555 0.459 0.482 0.408 1.388 0.748 1.235 0.771 0.478 5.800 5.266 5.918 14.312 24.361 0.482 1.934 0.541 0.565 0.518 0.624 0.664 0.471 0.559 0.478 0.976 0.988 0.718 1.582 1.592 5.165 1.473 1.671 1.588 1.255 RH 95% RH 66% RH 79% 0.000 0.000 0.000 0.000 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 369.475 369.358 369.281 364.756 364.543 364.341 384.186 382.190 379.626 369.971 369.775 369.644 370.484 370.368 370.293 381.303 380.997 380.652 353.243 353.161 353.109 367.182 367.051 366.990 371.265 368.832 365.726 355.199 355.103 355.037 359.756 359.661 359.600 339.690 339.421 339.218 384.243 383.973 383.813 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 0.000 0.000 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss g/ m2/ day g/ m2/ day Gasahol RH 80% RH 98%

outside barrier FSI# Coating type 1 F 22 CRC 31.182 2 F 23 CRC 34.100 3 F 24 CRC 34.216 4 F  58 AMC 31.433 95.183 63.750 437.902 436.522 5 F  59 AMC 31.483 87.290 55.807 390.304 6 F  60 AMC 31.433 76.964 45.531 419.964 417.819 7 F  94 SUP 34.180 8 F  95 SUP 33.778 56.943 23.165 400.631 9 F  96 SUP 33.981 53.858 19.877 399.784 10 F  130 51PC 200 33.614 40.944 7.330 389.015 387.784 11 F  131 51PC 200 30.843 37.751 6.908 388.236 386.708 12 F  132 51PC 200 31.454 38.667 7.213 384.440 384.145 13 F  166 CRT 31.529 38.864 7.335 365.118 362.197 14 F  167 CRT 33.578 41.245 7.667 340.913 335.717 15 F  168 CRT 33.935 41.277 7.342 350.101 334.191 16 F  190 51PC  500 29.202 43.452 14.250 390.054 389.730 17 F  191 51PC  500 29.652 42.928 13.276 400.793 400.393 18 F  192 51PC  500 29.482 43.538 14.056 382.878 382.037 Weight after preconditioning Empty uncoated weight Weight after coat Mass of coat Weight before preconditioning Gasahol 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 outside Weight loss Weight loss Weight loss Weight loss Weight loss barrier FSI# Coating type g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 4 F  58 AMC 2.047 4.196 3.467 3.212 3.624 5 F  59AMC 6 F  60 AMC 4.518 8.902 7.882 0.359 0.635 7 F  94SUP 8 F  95 SUP  1.012 0.525 0.769 0.853 0.729 9 F  96 SUP 7.294  0.039 0.149 0.024 0.094 10 F  130 51PC 200 0.165 0.447 0.408 0.247 0.388 11 F  131 51PC 200 2.329 0.447 0.502 0.365 0.541 12 F  132 51PC 200 1.318 2.471 2.376 2.371 0.035 13 F  166 CRT  1.482 0.165 0.369 0.494 2.788 14 F  167 CRT 0.000 1.545 1.475 1.882 1.082 15 F  168 CRT 1.459 0.039 0.094 0.059 0.353 16 F  190 51PC  500 0.894 3.082 3.224 2.882 2.918 17 F  191 51PC  500 0.847 3.082 3.231 2.924 2.941 18 F  192 51PC  500 0.776 4.784 4.871 4.300 4.365 RH 79% RH 84% RH 96% RH 58% RH 85% RH 96% RH 83%

07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 436.435 435.900 435.458 434.912 434.846 434.826 417.627 416.492 415.729 415.668 415.614 415.553 415.413 400.674 400.607 400.509 400.364 400.302 400.236 399.979 399.474 399.479 399.460 399.456 399.448 399.182 398.358 387.777 387.720 387.668 387.626 387.593 387.574 387.491 386.851 386.794 386.730 386.668 386.622 386.591 386.176 384.089 383.774 383.471 383.068 383.065 382.817 382.255 362.260 362.239 362.192 362.108 361.871 361.391 360.084 335.717 335.520 335.332 335.012 335.162 335.021 334.636 334.371 334.366 334.354 334.344 334.314 334.138 333.960 389.692 389.299 388.888 388.398 388.150 387.883 387.234 400.357 399.964 399.552 399.055 398.805 398.519 397.880 382.004 381.394 380.773 380.042 379.913 379.843 379.602 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 0.235 0.329 0.282 0.235 0.718 0.659 0.388 0.535 0.604 0.776 1.209 0.976 1.153 1.098 3.129 3.878 3.871 3.871 3.922 0.224 0.391 0.365 0.318 0.329 0.365 1.953 3.141 13.141 6.220 2.918 2.645 5.329 0.747 1.820 5.647 6.151 7.600 2.624 2.282 1.659 1.812 2.635 6.012 4.533 2.071 0.838 0.847 4.824 5.176 3.141 3.054 3.224 3.024 2.949 3.365 3.007 3.282 3.100 2.988 0.824 1.134 2.047 1.547 2.141 RH 95% RH 66% RH 79% 0.000 0.000 0.000 0.000 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 434.728 434.680 434.650 415.380 415.289 415.212 399.896 399.700 399.560 398.029 397.371 396.871 387.460 387.406 387.364 385.909 383.675 382.882 381.802 381.675 381.443 359.680 359.234 358.943 334.412 333.390 332.812 333.888 333.068 332.408 386.960 386.446 386.070 397.601 397.074 396.693 379.428 379.165 378.892 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 0.000 0.000 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss g/ m2/ day g/ m2/ day Gasahol RH 80% RH 98%

outside adhesion FSI# Coating type 1 F  10 CRC 33.868 2 F  11 CRC 30.799 3 F  12 CRC 33.635 4 F  46 AMC 30.760 81.896 51.136 430.624 429.414 5 F  47 AMC 31.188 81.455 50.267 426.621 6 F  48 AMC 30.740 75.696 44.956 421.309 7 F  82 SUP 31.119  31.119 8 F  83 SUP 33.809  33.809 401.600 9 F  84 SUP 33.409  33.409 401.299 10 F  118 51PC 200 33.398 41.147 7.749 383.255 382.643 11 F  119 51PC 200 30.988 38.040 7.052 387.726 386.972 12 F  120 51PC 200 33.378 40.180 6.802 370.388 369.492 13 F  154 CRT 31.042 40.492 9.450 382.522 371.400 14 F  155 CRT 30.762 39.069 8.307 391.355 383.953 15 F  156 CRT 33.382 41.244 7.862 382.378 381.885 16 F  193 51PC  500 30.759 46.005 15.246 392.629 389.833 17 F  194 51PC  500 30.779 46.164 15.385 393.249 390.429 18 F  195 51PC  500 33.680 49.434 15.754 405.583 404.026 Weight after preconditioning Empty uncoated weight Weight after coat Mass of coat Weight before preconditioning Gasahol 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 outside Weight loss Weight loss Weight loss Weight loss Weight loss adhesion FSI# Coating type g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 4 F  46 AMC  1.624 1.749 1.475 1.071 1.247 5 F  47 AMC 6 F  48 AMC 7 F  82 SUP 8 F  83 SUP 9 F  84 SUP 10 F  118 51PC 200 2.800 5.239 5.608 5.682 6.000 11 F  119 51PC 200 3.929 6.925 6.996 7.441 7.329 12 F  120 51PC 200 5.059 7.804 8.306 8.135 7.612 13 F  154 CRT 2.212 0.196 0.196 0.094 0.141 14 F  155 CRT  1.012 0.235 0.180 0.076 0.012 15 F  156 CRT 1.576 2.988 2.690 2.518 0.071 16 F  193 51PC  500 1.224 5.271 6.761 6.659 6.835 17 F  194 51PC  500 8.118 15.616 17.475 16.859 23.894 18 F  195 51PC  500 0.965 4.055 5.137 5.447 5.271 RH 79% RH 84% RH 96% RH 58% RH 85% RH 96% RH 83% RH 95%

07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 429.483 429.260 429.072 428.890 428.784 428.694 428.352 428.247 382.524 381.856 381.141 380.175 379.665 379.172 377.545 376.964 386.805 385.922 385.030 383.765 383.142 382.524 380.588 379.877 369.277 368.282 367.223 365.840 365.193 364.527 362.141 360.158 371.548 371.523 371.498 371.482 371.470 371.453 371.412 371.405 383.996 383.966 383.943 383.930 383.929 383.917 383.344 383.343 381.818 381.437 381.094 380.908 380.902 380.888 380.865 380.860 389.781 389.109 388.247 387.115 386.534 385.912 383.683 382.803 390.084 388.093 385.865 382.999 381.210 380.567 376.622 375.451 403.985 403.468 402.813 401.887 401.439 400.891 399.060 398.410 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 1.059 1.609 1.235 1.353 1.435 5.800 7.656 6.835 6.865 6.996 7.271 9.111 8.365 8.571 8.690 7.835 11.228 23.329 23.912 4.400 0.200 0.193 0.082 0.141 0.141 0.141 0.136 0.012 0.082 0.086 0.165 0.108 0.059 0.082 0.086 7.318 10.489 10.353 9.859 7.655 7.565 18.565 13.776 14.441 14.588 6.447 8.616 7.647 8.747 9.114 RH 66% RH 79% 0.000 0.000 0.000 0.000 0.000 0.000 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 428.017 427.834 375.797 374.905 378.420 377.312 356.335 355.774 371.381 371.363 383.329 383.318 380.846 380.835 381.127 380.151 372.996 371.136 396.923 395.761 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day Gasahol RH 80% RH 98%

outside A& B FSI# Coating type 1 F  34 CRC 31.643 2 F  35 CRC 31.785 3 F  36 CRC 31.578 4 F  70 AMC 31.102 72.440 41.338 422.250 405.363 5 F  71 AMC 34.044 71.203 37.159 407.162 421.911 6 F  72 AMC 33.731 73.415 39.684 415.068 414.761 7 F  106 SUP 31.340 54.704 23.364 390.358 388.557 8 F  107 SUP 33.844 55.593 21.749 390.576 388.975 9 F  108 SUP 31.172 55.027 23.855 402.082 400.158 10 F  142 51PC 200 33.622 39.786 6.164 382.952 382.607 11 F  143 51PC 200 33.837 40.738 6.901 369.519 368.860 12 F  144 51PC 200 33.622 40.859 7.237 368.976 363.910 13 F  178 CRT 33.890 40.464 6.574 387.630 385.699 14 F  179 CRT 33.668 40.164 6.496 370.018 368.330 15 F  180 CRT 31.149 39.302 8.153 374.864 372.763 16 F  196 51PC  500 29.175 43.964 14.789 388.170 385.604 17 F  197 51PC  500 32.069 47.149 15.080 405.082 404.633 18 F  198 51PC  500 32.138 47.556 15.418 392.481 390.642 Weight after preconditioning Empty uncoated weight Weight after coat Mass of coat Weight before preconditioning Gasahol 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 outside Weight loss Weight loss Weight loss Weight loss Weight loss A& B FSI# Coating type g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 4 F  70 AMC  1.600 0.925 0.525 0.506 0.318 5 F  71 AMC  0.494 6 F  72 AMC  2.024 1.969 2.667 0.229 0.106 7 F  106 SUP  1.247 2.541 0.329 0.229 0.553 8 F  107 SUP  2.282 0.141 0.267 11.065 2.565 9 F  108 SUP  1.953 0.173 0.133 0.194 0.200 10 F  142 51PC 200 0.871 2.714 2.525 2.671 2.706 11 F  143 51PC 200  2.706 0.714 0.447 0.594 0.529 12 F  144 51PC 200  0.800 0.337 0.235 0.271 0.271 13 F  178 CRT  0.659 0.125 0.047 0.176 0.306 14 F  179 CRT  1.271 1.278 1.475 1.412 0.094 15 F  180 CRT  0.800 0.165 0.125 0.324 0.329 16 F  196 51PC  500  1.341 1.969 0.455 0.718 0.765 17 F  197 51PC  500  0.306 3.890 2.376 2.629 2.788 18 F  198 51PC  500 3.388 0.878 0.416 0.559 0.424 RH 79% RH 84% RH 96% RH 58% RH 85% RH 96% RH 83%

07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 405.431 405.313 405.246 405.160 405.133 405.077 404.975 421.932 Dropped and shattered, producing leaks 414.847 414.838 414.498 414.459 414.450 414.411 414.360 388.610 388.528 388.486 388.447 388.400 388.342 388.265 389.072 389.054 389.020 387.381 387.163 386.737 385.809 400.241 400.219 400.202 400.169 400.152 400.121 400.062 382.570 382.224 381.902 381.448 381.218 380.956 380.346 368.975 368.884 368.827 368.726 368.681 368.617 368.505 363.944 363.901 363.871 363.825 363.802 363.771 363.706 385.727 385.711 385.705 385.675 385.649 385.467 384.913 368.384 368.463 368.275 368.035 368.269 368.245 368.200 372.797 372.776 372.760 372.705 372.677 372.633 372.460 385.661 385.652 385.594 385.472 385.407 385.267 385.120 404.646 404.150 403.847 403.400 403.405 403.356 402.954 390.740 390.628 390.575 390.480 390.444 390.386 390.278 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 0.659 0.480 0.459 0.412 0.596 0.459 0.240 0.329 0.276 1.725 0.682 0.362 2.141 2.253 2.753 5.012 4.367 5.600 7.429 9.929 0.365 0.278 0.353 0.324 0.573 3.082 2.871 3.576 0.353 0.416 0.753 0.527 0.541 0.512 0.722 0.365 0.306 0.353 0.271 0.620 2.141 2.607 4.494 1.224 1.482 0.282 0.212 0.259 0.218 0.259 0.518 0.814 4.118 1.224 3.153 1.647 0.692 2.082 1.141 2.110 0.576 1.892 6.776 3.176 5.490 0.682 0.508 0.576 0.476 0.596 RH 95% RH 66% RH 79% 0.000 0.000 0.000 0.000 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 404.936 404.866 404.790 414.332 414.285 414.065 388.083 387.700 387.349 385.333 384.070 382.804 400.032 399.977 399.904 380.284 380.224 380.171 368.459 368.372 368.280 363.676 363.630 363.551 384.773 384.565 384.376 368.178 368.141 368.108 372.352 372.144 371.742 384.943 384.749 384.480 402.620 402.080 401.380 390.229 390.148 390.072 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 0.000 0.000 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss g/ m2/ day g/ m2/ day Pure Gas RH 80% RH 98%

inside barrier FSI# Coating type 1 F  13 CRC 34.155 49.022 2 F  14 CRC 34.105 43.621 3 F  15 CRC No Longer able to test 4 F  49 AMC 31.264 82.157 50.893 394.253 393.826 5 F  50 AMC 31.318 89.902 58.584 405.763 405.056 6 F  51 AMC 30.933 75.760 44.827 372.211 371.295 7 F  85 SUP 30.913  30.913 412.489 411.748 8 F  86 SUP 31.039  31.039 410.031 409.214 9 F  87 SUP 33.954  33.954 386.821 385.332 10 F  121 51PC 200 33.494  33.494 377.624 376.792 11 F  122 51PC 200 31.102  31.102 369.591 368.456 12 F  123 51PC 200 30.964  30.964 389.100 388.048 13 F  157 CRT 33.609 39.955 6.346 387.530 386.648 14 F  158 CRT 31.301 37.429 6.128 380.679 379.840 15 F  159 CRT 33.709 41.227 7.518 388.545 387.519 16 F  199 51PC  500 29.598 43.080 13.482 384.746 373.797 17 F  200 51PC  500 29.269 42.315 13.046 370.605 369.086 18 F  201 51PC  500 32.080 47.234 15.154 383.802 382.656 Empty uncoated weight Weight after coat Weight before preconditioning Weight after preconditioning Pure Gas 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 inside Weight loss Weight loss Weight loss Weight loss Weight loss barrier FSI# Coating type g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 4 F  49 AMC  0.353 0.290 0.400 0.412 0.447 5 F  50 AMC  0.094 1.082 1.224 1.271 1.259 6 F  51 AMC  0.494 0.808 0.792 1.153 0.141 7 F  85 SUP 0.400 3.224 2.941 2.847 2.447 8 F  86 SUP  0.024 0.110 0.173 0.100 0.118 9 F  87 SUP 47.271  14.580 0.651 0.641 1.082 10 F  121 51PC 200 0.047 0.063 0.063 0.065 0.012 11 F  122 51PC 200 0.871 0.000 0.118 0.100 0.012 12 F  123 51PC 200  0.118 0.173 0.227 0.329 0.341 13 F  157 CRT  0.353 0.447 0.416 0.453 0.471 14 F  158 CRT  0.518 0.204 0.251 0.241 0.341 15 F  159 CRT  0.494 0.227 0.133 0.147 0.224 16 F  199 51PC  500 0.024 0.125 0.110 0.624 2.400 17 F  200 51PC  500 0.141 0.243 0.243 0.488 1.106 18 F  201 51PC  500  0.188 0.220 0.227 0.118 0.165 RH 79% RH 84% RH 96% RH 58% RH 85% RH 96% RH 83% RH 95%

07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 393.841 393.804 393.753 393.683 393.645 393.608 393.503 393.462 405.302 405.164 405.008 404.792 404.685 404.568 404.233 404.099 371.316 371.213 371.112 370.916 370.904 370.831 370.642 370.566 411.731 411.320 410.945 410.461 410.495 410.428 410.356 410.331 409.215 409.201 409.179 409.162 409.152 409.131 409.096 409.084 383.323 385.182 385.099 384.990 385.140 385.026 384.821 384.665 376.790 376.782 376.774 376.763 376.762 376.751 376.730 376.720 368.419 368.419 368.404 368.387 368.386 368.348 368.303 368.291 388.053 388.031 388.002 387.946 387.917 387.596 387.315 387.380 386.663 386.606 386.553 386.476 386.436 386.389 386.268 386.210 379.862 379.836 379.804 379.763 379.734 379.700 379.575 379.456 387.540 387.511 387.494 387.469 387.450 387.438 387.406 387.385 373.796 373.780 373.766 373.660 373.456 373.452 373.424 373.411 369.080 369.049 369.018 368.935 368.841 368.620 368.075 367.992 382.664 382.636 382.849 382.829 382.815 382.803 382.768 382.744 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 0.435 0.494 0.482 0.441 0.439 1.376 1.576 1.576 1.524 1.514 0.859 0.889 0.894 0.824 0.871 0.788 0.339 0.294 0.329 0.282 0.247 0.165 0.141 0.135 0.118 1.341 0.965 1.835 1.041 0.941 0.129 0.099 0.118 0.376 0.196 0.447 0.212 0.141 0.135 0.165 3.776 1.322 2.082 0.047 0.125 0.553 0.569 0.682 0.529 0.588 0.400 0.588 1.400 0.941 0.925 0.141 0.151 0.247 0.082 0.180 0.047 0.132 0.153 0.171 0.141 2.600 2.565 3.824 0.794 1.035 0.141 0.165 0.282 0.147 0.196 RH 66% RH 79% 0.000 0.000 0.000 0.000 0.000 0.000 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 393.387 393.331 403.840 403.647 370.426 370.315 410.275 410.239 409.061 409.046 384.488 384.368 376.656 376.631 368.268 368.247 387.372 387.356 386.120 386.045 379.296 379.178 387.371 387.348 373.382 373.364 367.857 367.725 382.719 382.694 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day Pure Gas RH 80% RH 98%

inside adhesion FSI# Coating type 1 F  1 CRC 33.472 40.338 6.866 2 F  2 CRC 33.264 40.281 7.017 3 F  3 CRC 31.067 40.223 9.156 4 F  37 AMC 33.374 76.776 43.402 383.143 382.032 5 F  38 AMC 33.383 76.704 43.321 418.729 6 F  39 AMC 33.252 69.444 36.192 391.610 389.920 7 F  73 SUP 31.000  31.000 427.071 424.120 8 F  74 SUP 30.803  30.803 414.138 410.034 9 F  75 SUP 31.054  31.054 405.580 405.546 10 F  109 51PC 200 33.463 36.995 3.532 378.927 378.080 11 F  110 51PC 200 33.650 37.222 3.572 388.696 387.278 12 F  111 51PC 200 33.623 36.162 2.539 388.848 387.713 13 F  145 CRT 33.530 40.721 7.191 380.513 379.786 14 F  146 CRT 33.305 39.742 6.437 365.821 364.874 15 F  147 CRT 33.695 40.989 7.294 399.949 397.746 16 F  202 51PC  500 33.596 49.995 16.399 365.141 363.683 17 F  203 51PC  500 30.879 49.662 18.783 364.169 362.430 18 F  204 51PC  500 33.714 50.435 16.721 391.583 390.002 Weight after preconditioning Empty uncoated weight Weight after coat Mass of coat Weight before preconditioning Pure Gas 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 inside Weight loss Weight loss Weight loss Weight loss Weight loss adhesion FSI# Coating type g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 4 F  37 AMC 1.129 2.486 2.384 2.435 2.435 5 F  38 AMC  9780.000 2.949 3.027 3.000 2.976 6 F  39 AMC 11.694 4.251 4.337 3.294 3.012 7 F  73 SUP  0.541 1.616 0.886 1.359 1.529 8 F  74 SUP 4.424 2.439 1.035 1.894 1.729 9 F  75 SUP 0.094 0.416 0.369 0.394 0.306 10 F  109 51PC 200 0.000 0.102 0.118 0.112 0.106 11 F  110 51PC 200  0.259 0.439 0.227 0.206 0.259 12 F  111 51PC 200  0.094 0.549 0.329 0.265 0.212 13 F  145 CRT  0.588 0.282 0.157 0.188 0.059 14 F  146 CRT 0.659 1.937 1.584 1.471 4.106 15 F  147 CRT 0.400 0.204 0.149 0.165 0.082 16 F  202 51PC  500 3.106 5.380 5.718 5.394 5.082 17 F  203 51PC  500 3.553 5.396 5.961 5.929 5.624 18 F  204 51PC  500 4.118 6.275 6.949 6.759 6.188 RH 79% RH 84% RH 96% RH 58% RH 85% RH 96% RH 83% RH 95%

07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 381.984 381.667 381.363 380.949 380.742 380.509 379.973 379.762 415.650 415.274 414.888 414.378 414.125 413.852 413.174 412.907 389.423 388.881 388.328 387.768 387.512 387.141 386.480 386.235 424.143 423.937 423.824 423.593 423.705 423.689 423.648 423.634 410.088 409.777 409.645 409.323 409.176 408.748 408.144 408.054 405.542 405.489 405.442 405.375 405.349 405.309 405.236 405.203 378.080 378.067 378.052 378.033 378.024 378.015 377.994 377.984 387.289 387.233 387.204 387.169 387.147 387.129 386.949 386.780 387.717 387.647 387.605 387.560 387.542 387.519 387.462 387.448 379.811 379.775 379.755 379.723 379.718 379.701 379.672 379.663 364.846 364.599 364.397 364.147 364.040 364.019 363.971 363.957 397.729 397.703 397.684 397.656 397.649 397.636 397.598 397.592 363.551 362.865 362.136 361.219 360.787 360.374 359.194 358.771 362.279 361.591 360.831 359.823 359.345 358.877 357.550 357.086 389.827 389.027 388.141 386.992 386.466 385.935 384.448 383.916 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 2.741 2.522 2.482 2.335 2.541 3.212 3.191 3.141 2.935 3.114 4.365 3.111 2.882 2.241 2.416 0.188 0.193 0.165 0.147 0.196 7.882 2.842 1.059 1.053 1.051 0.471 0.344 0.388 0.324 0.376 0.106 0.099 0.118 0.100 0.408 0.212 0.847 1.988 0.906 1.459 0.271 0.268 0.165 0.212 0.243 0.200 0.136 0.106 0.135 0.141 0.247 0.226 0.165 0.271 0.267 0.153 0.179 0.071 0.141 0.086 4.859 5.553 4.976 5.329 5.388 5.506 6.245 5.459 5.724 5.859 6.247 6.998 6.259 6.488 7.341 RH 66% RH 79% 0.000 0.000 0.000 0.000 0.000 0.000 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 379.365 379.041 412.408 412.011 385.854 385.546 423.609 423.584 407.875 407.741 405.148 405.100 377.967 377.915 386.626 386.440 387.412 387.381 379.640 379.622 363.911 363.877 397.568 397.557 357.865 357.178 356.113 355.366 382.813 381.877 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day Pure Gas RH 80% RH 98%

inside A& B FSI# Coating type 1 F  25 CRC 31.500 42.837 2 F  26 CRC No Longer able to test 3 F  27 SUP 31.388 38.391 7.003 415.830 415.392 4 F  61 AMC 34.107 74.000 39.893 377.169 5 F  62 AMC 31.572 6 F  63 AMC 34.007 69.296 35.289 371.621 371.069 7 F  97 SUP 31.098 8 F  98 SUP 31.417  31.417 396.969 396.377 9 F  99 SUP 33.871 10 F  133 51PC 200 33.640 37.508 3.868 393.732 392.986 11 F  134 51PC 200 33.684 37.113 3.429 379.810 378.214 12 F  135 51PC 200 31.168 34.352 3.184 383.695 382.575 13 F  169 CRT 30.975 37.228 6.253 395.256 395.106 14 F  170 CRT 33.455 39.772 6.317 395.051 394.874 15 F  171 CRT 33.552 39.667 6.115 404.519 404.206 16 F  205 51PC  500 32.056 N/ A 17 F  206 51PC  500 29.501 46.598 17.097 390.198 390.168 18 F  207 51PC  500 29.542 43.885 14.343 388.017 388.001 Weight after preconditioning Empty uncoated weight Weight after coat Mass of coat Weight before preconditioning Pure Gas 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 inside Weight loss Weight loss Weight loss Weight loss Weight loss A& B FSI# Coating type g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 3 F  27 SUP  0.612  0.275 0.557 0.265 0.118 5 F  62 AMC 6 F  63 AMC 2.447 6.204 7.373 9.647 10.318 7 F  97 SUP 8 F  98 SUP  0.235  0.039 0.400 0.194 0.224 9 F  99 SUP 10 F  133 51PC 200 0.141  0.565 0.463 0.171 0.224 11 F  134 51PC 200  0.565  0.431 0.604 0.206 0.247 12 F  135 51PC 200 0.447  0.431 0.282 0.147 0.212 13 F  169 CRT 5.294 0.290 1.914 4.471  5.365 14 F  170 CRT  3.976 1.200 0.651 0.294 0.282 15 F  171 CRT  0.612 0.165 0.408 0.247 0.365 16 F  205 51PC  500 17 F  206 51PC  500 1.906 2.008 2.212 2.100 3.118 18 F  207 51PC  500 1.882 2.400 7.843 0.147 0.329 RH 79% RH 84% RH 96% RH 58% RH 85% RH 96% RH 83% RH 95%

07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 415.418 415.453 415.382 415.337 415.327 415.297 415.250 415.234 370.965 370.174 369.234 367.594 366.959 364.574 362.166 361.290 396.387 396.392 396.341 396.308 396.289 396.273 396.234 396.216 392.980 393.052 392.993 392.964 392.945 392.930 392.898 392.884 378.238 378.293 378.216 378.181 378.160 378.149 378.098 377.969 382.556 382.611 382.575 382.550 382.532 382.509 382.397 382.351 394.881 394.844 394.842 394.082 394.780 394.767 394.727 394.713 395.043 394.890 394.807 394.757 394.733 394.713 394.653 394.635 404.232 404.211 404.159 404.117 404.086 404.070 404.012 403.990 390.087 389.831 389.549 389.192 389.169 389.150 389.121 389.105 387.921 387.615 386.857 386.832 386.804 386.792 386.752 386.733 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 0.353 0.221 0.188 0.200 0.165 28.059 11.332 10.306 16.753 10.824 0.188 0.184 0.212 0.147 0.149 0.176 0.151 0.165 0.276 0.118 0.129 0.240 1.518 0.924 1.012 0.271 0.527 0.541 1.329 1.820 0.153 0.188 0.165 0.182 0.149 0.235 0.282 0.212 0.276 0.290 0.188 0.273 0.259 0.253 0.235 0.224 0.136 0.188 0.176 0.102 0.141 0.188 0.224 0.165 0.188 RH 66% RH 79% 0.000 0.000 0.000 0.000 0.000 0.000 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 415.200 415.179 358.442 357.062 396.191 396.172 392.837 392.822 377.812 377.683 382.125 381.893 394.682 394.663 394.588 394.551 403.947 403.917 389.075 389.062 386.705 386.681 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day Pure Gas RH 80% RH 98%

outside barrier FSI# Coating type 1 F  19 CRC 31.264  31.264 2 F  20 CRC 31.467  31.467 3 F  21 CRC 33.720  33.720 4 F  55 AMC 31.124 60.713 29.589 403.666 403.094 5 F  56 AMC 31.452 56.179 24.727 397.824 397.406 6 F  57 AMC 31.150 58.521 27.371 397.619 397.084 7 F  91 SUP 33.555 56.140 22.585 402.721 401.946 8 F  92 SUP 33.694 58.194 24.500 408.552 407.860 9 F  93 SUP 30.823 10 F  127 51PC 200 30.872 38.056 7.184 360.463 359.868 11 F  128 51PC 200 33.548 40.327 6.779 374.975 374.416 12 F  129 51PC 200 33.630 13 F  163 CRT 33.627 39.968 6.341 391.636 390.466 14 F  164 CRT 33.779 41.433 7.654 406.766 404.940 15 F  165 CRT 33.516 40.307 6.791 392.798 392.197 16 F  208 51PC  500 32.026 46.096 14.070 391.307 391.053 17 F  209 51PC  500 32.094 46.609 14.515 344.755 344.500 18 F  210 51PC  500 31.884 45.938 14.054 359.583 359.338 Weight after preconditioning Empty uncoated weight Weight after coat Mass of coat Weight before preconditioning Pure Gas 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 outside Weight loss Weight loss Weight loss Weight loss Weight loss barrier FSI# Coating type g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 4 F  55 AMC 2.753 296.729 60.173 3.471 52.329 5 F  56 AMC  0.706 1.153 1.976 1.629 1.741 6 F  57 AMC 0.918 4.220 3.757 4.018 3.929 7 F  91 SUP  1.153 0.016 0.047 0.071 0.012 8 F  92 SUP  0.329 0.173 0.102 0.065 0.012 9 F  93 SUP 10 F  127 51PC 200 0.000 0.125 0.267 0.282 0.235 11 F  128 51PC 200 0.000 0.314 0.055 0.129 0.012 12 F  129 51PC 200 13 F  163 CRT 1.929 1.929 3.184 0.082 0.035 14 F  164 CRT  0.141 0.518 2.063 0.165 0.071 15 F  165 CRT 13.859 4.392 1.663 0.676 2.176 16 F  208 51PC  500  1.482 0.392 0.071 0.624 1.024 17 F  209 51PC  500  1.271 0.298 0.024 0.424 0.200 18 F  210 51PC  500  1.082 0.282 0.102 0.235 0.012 RH 79% RH 84% RH 96% RH 58% RH 85% RH 96% RH 83% RH 95%

07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 402.977 365.144 357.472 356.882 352.434 352.113 351.970 351.873 397.436 397.289 397.037 396.760 396.612 396.466 395.952 397.045 396.507 396.028 395.345 395.011 394.695 393.553 401.995 401.993 401.987 401.975 401.974 401.947 401.915 401.909 407.874 407.852 407.839 407.828 407.827 407.812 407.792 407.787 359.868 359.852 359.818 359.770 359.750 359.712 359.626 359.535 374.416 374.376 374.369 374.347 374.346 374.326 374.314 374.313 390.384 390.138 389.974 389.960 389.957 389.940 389.917 389.884 404.946 404.880 404.859 404.831 404.825 404.803 404.766 404.756 391.850 391.290 391.078 390.963 390.778 390.756 390.731 390.721 391.116 391.066 391.057 390.951 391.106 391.083 391.053 391.052 344.554 344.516 344.513 344.441 344.424 344.390 344.298 344.280 359.384 359.348 359.335 359.295 359.294 359.285 359.251 359.250 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 3.776 0.673 1.141 3.994 0.400 1.718 1.715 1.728 1.588 1.631 3.718 3.755 3.839 3.759 3.773 0.318 0.151 0.071 0.206 0.212 0.176 0.094 0.059 0.047 0.086 0.447 0.405 1.071 2.047 1.969 0.235 0.056 0.012 0.041 0.008 0.200 0.108 0.388 1.729 8.486 0.259 0.174 0.118 0.165 0.157 0.259 0.118 0.118 0.147 0.204 0.271 0.141 0.012 1.953 2.902 0.400 0.433 0.212 0.347 0.259 0.106 0.160 0.012 0.041 0.055 RH 66% RH 79% 0.000 0.000 0.000 0.000 0.000 0.000 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 351.194 351.143 395.682 395.474 392.914 392.433 401.874 401.847 407.779 407.768 359.187 358.936 374.306 374.305 389.590 388.508 404.728 404.708 390.696 390.670 390.720 390.350 344.221 344.188 359.243 359.236 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day Pure Gas RH 80% RH 98%

outside adhesion FSI# Coating type 1 F  7 CRC 34.113  34.113 2 F  8 CRC 33.902  33.902 3 F  9 CRC 34.030  34.030 4 F  43 AMC 31.795 63.472 31.677 395.805 395.549 5 F  44 AMC 34.165 66.569 32.404 399.594 398.383 6 F  45 AMC 34.126 80.355 46.229 428.294 426.680 7 F  79 SUP 32.398 58.345 25.947 410.474 409.775 8 F  80 SUP 29.751 55.016 25.265 392.329 391.563 9 F  81 SUP 32.183 57.090 24.907 407.520 406.798 10 F  115 51PC 200 32.195 38.989 6.794 382.416 381.774 11 F  116 51PC 200 32.234 38.668 6.434 385.109 384.092 12 F  117 51PC 200 32.131 38.378 6.247 389.281 387.534 13 F  151 CRT 29.000 38.539 9.539 387.994 387.235 14 F  152 CRT 29.019 37.839 8.820 399.391 398.834 15 F  153 CRT 29.928 37.989 8.061 397.632 397.098 16 F  211 51PC  500 29.904 44.445 14.541 343.796 343.557 17 F  212 51PC  500 32.415 46.803 14.388 347.335 346.480 18 F  213 51PC  500 32.317 46.570 14.253 368.114 364.282 Weight after preconditioning Empty uncoated weight Weight after coat Mass of coat Weight before preconditioning Pure Gas 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 outside Weight loss Weight loss Weight loss Weight loss Weight loss adhesion FSI# Coating type g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 4 F  43 AMC  1.506 3.169 3.208 2.953 3.012 5 F  44 AMC  5.318 2.965 0.690 0.388 0.353 6 F  45 AMC  1.953  1.388 1.961 0.812 0.765 7 F  79 SUP  0.612 0.016 0.063 0.035 0.012 8 F  80 SUP  1.247 0.016 0.141 0.041 0.094 9 F  81 SUP  0.376 0.110 0.275 1.535 1.635 10 F  115 51PC 200  0.141 3.176 4.439 1.935 2.741 11 F  116 51PC 200  1.200 0.400 0.525 0.482 0.506 12 F  117 51PC 200  1.153 0.259 0.204 0.324 0.106 13 F  151 CRT 0.329 1.537 1.467 1.588 1.518 14 F  152 CRT  1.082 0.251 0.204 0.188 0.165 15 F  153 CRT  0.706 0.306 0.329 0.671 0.424 16 F  211 51PC  500  1.482 0.424 0.306 0.476 0.576 17 F  212 51PC  500  4.141 1.380 0.478 0.665 0.553 18 F  213 51PC  500  2.376 0.463 0.384 0.506 0.353 RH 79% RH 84% RH 96% RH 58% RH 85% RH 96% RH 83% RH 95%

07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 395.613 395.209 394.800 394.298 394.042 393.825 393.208 393.268 398.609 398.231 398.385 398.319 398.289 398.258 398.161 398.145 426.763 426.940 426.690 426.552 426.487 426.437 426.270 426.230 409.801 409.799 409.791 409.785 409.784 409.774 409.750 409.748 391.616 391.614 391.596 391.589 391.581 391.566 391.535 391.350 406.814 406.800 406.765 406.504 406.607 406.510 406.336 406.266 381.780 381.375 381.051 380.722 380.489 380.023 378.507 378.075 384.143 384.092 384.025 383.943 383.900 383.846 383.708 383.655 387.583 387.550 387.524 387.469 387.460 387.399 387.309 387.277 387.221 387.025 387.080 386.810 386.681 386.549 386.204 386.081 398.880 398.848 398.822 398.790 398.776 398.747 398.696 398.680 397.128 397.089 397.047 396.933 396.897 396.836 396.674 396.613 343.620 343.566 343.527 343.446 343.397 343.355 343.222 343.188 346.656 346.480 346.419 346.306 346.259 346.188 346.014 345.977 364.383 364.324 364.275 364.189 364.159 364.087 363.962 363.938 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 2.553 2.904 2.141 0.365 0.322 0.365 0.456 0.188 0.347 0.392 0.588 0.786 0.471 0.624 0.557 0.118 0.113 0.024 0.071 0.008 0.176 0.146 2.176 29.135 2.549 1.141 0.819 0.824 0.706 0.667 5.482 7.134 5.082 1.588 1.812 0.635 0.649 0.624 0.706 0.714 0.718 0.424 0.376 0.488 0.533 1.553 1.624 1.447 1.606 1.545 0.341 0.240 0.188 0.265 0.220 0.718 0.762 0.718 0.618 0.871 0.494 0.626 0.400 0.671 0.557 0.835 0.819 0.435 0.918 0.753 0.847 0.588 0.282 0.665 0.486 RH 66% RH 79% 0.000 0.000 0.000 0.000 0.000 0.000 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 393.206 393.165 398.086 398.036 426.124 426.053 409.736 409.735 386.397 386.072 406.146 406.061 377.805 377.574 383.535 383.444 387.194 387.126 385.808 385.611 398.635 398.607 396.508 396.397 343.074 343.003 345.821 345.725 363.825 363.763 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day Pure Gas RH 80% RH 98%

outside A& B FSI# Coating type 1 F  31 CRC 32.071  32.071 2 F  32 CRC 31.743  31.743 3 F  33 CRC 32.417  32.417 4 F  67 AMC 31.092 58.676 27.584 403.411 403.162 5 F  68 AMC 30.967 61.036 30.069 380.401 380.145 6 F  69 AMC 31.927 60.429 28.502 381.906 381.443 7 F  103 SUP 34.245 47.914 13.669 398.573 397.571 8 F  104 SUP 33.770 60.592 26.822 399.861 399.169 9 F  105 SUP 31.247 55.921 24.674 399.312 398.616 10 F  139 51PC 200 30.840 37.917 7.077 380.297 379.569 11 F  140 51PC 200 34.155 40.970 6.815 386.315 385.399 12 F  141 51PC 200 34.170 41.012 6.842 390.883 389.657 13 F  175 CRT 31.516 42.629 11.113 404.174 402.789 14 F  176 CRT 31.571 41.633 10.062 391.762 391.683 15 F  177 CRT 33.946 43.767 9.821 406.286 405.734 16 F  214 51PC  500 29.694 44.578 14.884 342.251 341.977 17 F  215 51PC  500 29.116 43.804 14.688 370.780 369.646 18 F  216 51PC  500 29.101 43.871 14.770 383.736 383.275 Weight after preconditioning Empty uncoated weight Weight after coat Mass of coat Weight before preconditioning Pure Gas 07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 outside Weight loss Weight loss Weight loss Weight loss Weight loss A& B FSI# Coating type g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 4 F  67 AMC  2.376 0.212 0.024 0.165 0.012 5 F  68 AMC  1.788 0.478 0.353 0.524 0.376 6 F  69 AMC 0.071 2.384 2.337 2.459 2.424 7 F  103 SUP  2.988  10.016 10.227 0.076 0.035 8 F  104 SUP  0.447 3.984 0.008 2.682 3.882 9 F  105 SUP  0.847 0.039 0.000 0.065 0.012 10 F  139 51PC 200  1.247 0.227 0.133 0.300 0.753 11 F  140 51PC 200  0.988 0.133 0.110 0.135 0.118 12 F  141 51PC 200  0.894 0.149 0.000 0.153 0.247 13 F  175 CRT 4.494 0.329 0.298 0.282 0.318 14 F  176 CRT  0.753 0.157 0.078 0.112 0.071 15 F  177 CRT  0.965 0.180 0.094 0.106 0.082 16 F  214 51PC  500  1.788 0.447 0.008 0.171 0.035 17 F  215 51PC  500  2.376 0.400 0.008 0.300 0.412 18 F  216 51PC  500  1.624 2.337 7.702 0.259 0.094 RH 79% RH 84% RH 96% RH 58% RH 85% RH 96% RH 83% RH 95%

07/ 10/ 03 07/ 14/ 03 07/ 17/ 03 07/ 21/ 03 07/ 23/ 03 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 403.263 403.236 403.233 403.205 403.204 403.183 403.161 403.159 380.221 380.160 380.115 380.026 379.994 379.944 379.845 379.813 381.440 381.136 380.838 380.420 380.456 380.434 380.398 380.387 397.698 398.975 397.671 397.658 397.655 397.636 397.590 397.442 399.188 398.680 398.679 398.223 397.893 397.656 396.829 396.465 398.652 398.647 398.647 398.636 398.635 398.621 398.610 398.600 379.622 379.593 379.576 379.525 379.461 379.402 379.199 379.030 385.441 385.424 385.410 385.387 385.377 385.354 385.288 385.190 389.695 389.676 389.676 389.650 389.629 389.588 389.229 388.985 402.598 402.556 402.518 402.470 402.443 402.409 402.283 402.222 391.715 391.695 391.685 391.666 391.660 391.641 391.620 391.607 405.775 405.752 405.740 405.722 405.715 405.698 405.670 405.651 342.053 341.996 341.995 341.966 341.963 341.944 341.927 341.915 369.747 369.696 369.695 369.644 369.609 369.559 369.345 369.018 383.344 383.046 382.306 382.262 382.254 382.228 382.091 381.873 07/ 25/ 03 07/ 30/ 03 08/ 01/ 03 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day 0.247 0.104 0.024 0.024 0.141 0.588 0.466 0.376 0.359 0.510 0.259 0.169 0.129 0.100 0.259 0.224 0.216 1.741 1.288 1.780 2.788 3.892 4.282 4.959 7.035 0.165 0.052 0.118 0.006 0.094 0.694 0.955 1.988 3.276 4.573 0.271 0.311 1.153 1.188 2.125 0.482 1.689 5.718 0.365 1.404 0.400 0.593 0.718 0.641 0.894 0.224 0.099 0.153 0.835 0.431 0.200 0.132 0.224 0.118 0.298 0.224 0.080 0.141 0.006 0.110 0.588 1.007 3.847 4.118 1.561 0.306 0.645 2.565 1.471 2.573 RH 66% RH 79% 0.000 0.000 0.000 0.000 0.000 0.000 08/ 05/ 03 08/ 08/ 03 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 403.155 403.137 379.752 379.687 380.370 380.337 397.223 396.996 395.622 394.725 398.599 398.587 378.473 377.890 384.988 384.717 388.923 388.744 402.113 401.999 391.465 391.410 405.631 405.593 341.914 341.900 368.318 368.119 381.623 381.295 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 01/ 00/ 00 Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss Weight loss g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day g/ m2/ day


[Federal Register Volume 87, Number 62 (Thursday, March 31, 2022)]
[Rules and Regulations]
[Pages 18694-18696]
[FR Doc No: 2022-06620]

=======================================================================
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DEPARTMENT OF TRANSPORTATION

Federal Aviation Administration

14 CFR Part 39

[Docket No. FAA-2022-0024; Project Identifier MCAI-2021-00994-R;
Amendment 39-21999; AD 2022-07-11]
RIN 2120-AA64

Airworthiness Directives; Leonardo S.p.a. Helicopters

AGENCY: Federal Aviation Administration (FAA), DOT.

ACTION: Final rule.

-----------------------------------------------------------------------

SUMMARY: The FAA is superseding Airworthiness Directive (AD) 2021-17-
18, which applied to all Leonardo S.p.a. Model A109C, A109K2, A109E,
A109S, and AW109SP helicopters. AD 2021-17-18 required an inspection of
certain tail rotor (TR) sleeve assemblies for discrepancies, an
inspection of certain TR shaft assemblies for discrepancies, a
repetitive measurement of the position of the bushing of the TR sleeve
assembly in relation to the pitch change slider assembly, and
corrective actions if necessary. This AD retains the requirements of AD
2021-17-18, and also requires repetitive inspections of the TR sleeve
assemblies, and corrective actions if necessary, as specified in a
European Union Aviation Safety Agency (EASA) AD, which is incorporated
by reference. This AD was prompted by a determination that additional
actions are required to address the unsafe condition. This AD was also
prompted by a report of a crack on the TR mast. The FAA is issuing this
AD to address the unsafe condition on these products.

DATES: This AD is effective May 5, 2022.
    The Director of the Federal Register approved the incorporation by
reference of a certain publication listed in this AD as of September 7,
2021 (86 FR 46766, August 20, 2021).

ADDRESSES: For material incorporated by reference (IBR) in this AD,
contact the EASA, Konrad-Adenauer-Ufer 3, 50668 Cologne, Germany;
phone: +49 221 8999 000; email: [email protected]; internet:
www.easa.europa.eu. You may find this material on the EASA website at
https://ad.easa.europa.eu. You may view this material at the FAA,
Office of the Regional Counsel, Southwest Region, 10101 Hillwood Pkwy.,
Room 6N-321, Fort Worth, TX 76177. For information on the availability
of this material at the FAA, call<PHONE_NUMBER>. It is also available in
the AD docket on the internet at https://www.regulations.gov by
searching for and locating Docket No. FAA-2022-0024.

Examining the AD Docket

    You may examine the AD docket on the internet at https://www.regulations.gov by searching for and locating Docket No. FAA-2022-
0024; or in person at Docket Operations between 9 a.m. and 5 p.m.,
Monday through Friday, except Federal holidays. The AD docket contains
this final rule, any comments received, and other information. The
address for Docket Operations is U.S. Department of Transportation,
Docket Operations, M-30, West Building Ground Floor, Room W12-140, 1200
New Jersey Avenue SE, Washington, DC 20590.

FOR FURTHER INFORMATION CONTACT: Andrea Jimenez, Aerospace Engineer,
COS Program Management Section, Operational Safety Branch, FAA, 1600
Stewart Ave., Suite 410, Westbury, NY 11590; phone:<PHONE_NUMBER>;
email: [email protected].

SUPPLEMENTARY INFORMATION:

Background

    The EASA, which is the Technical Agent for the Member States of the
European Union, has issued EASA AD 2021-0144, dated June 17, 2021 (EASA
AD 2021-0144). (also referred to as the Mandatory Continuing
Airworthiness Information, or the MCAI), to correct an unsafe condition
for all Leonardo S.p.a. (formerly Finmeccanica S.p.A, AgustaWestland
S.p.A., Agusta S.p.A.) Model A109C, A109K2, A109E, A109S, and AW109SP
helicopters.
    The FAA issued a notice of proposed rulemaking (NPRM) to amend 14
CFR part 39 to supersede AD 2021-17-18, Amendment 39-21701 (86 FR
46766, August 20, 2021) (AD 2021-17-18). AD 2021-17-18 applied to all
Leonardo S.p.a. Model A109C, A109K2, A109E, A109S, and AW109SP
helicopters. The NPRM published in the Federal Register on February 3,
2022 (87 FR 6091). The NPRM was prompted by a determination that
additional actions are required to address the unsafe condition. The
NPRM was also prompted by a report of a crack on the TR mast. The NPRM
proposed to continue to require an inspection of certain TR sleeve
assemblies for discrepancies, an inspection of certain TR shaft
assemblies for discrepancies, a repetitive measurement of the position
of the bushing of the TR sleeve assembly in relation to the pitch
change slider assembly, and corrective actions if necessary, as
specified in an EASA AD. The NPRM also proposed to require repetitive
inspections of the TR sleeve assemblies, and corrective actions if
necessary, as specified in an EASA AD.
    The FAA is issuing this AD to address cracking on the TR mast,
which could lead to failure of the TR mast, with consequent loss of
control of the helicopter. See the MCAI for additional background
information.

Discussion of Final Airworthiness Directive

Comments

    The FAA gave the public the opportunity to participate in
developing this final rule. The FAA received no comments on the NPRM or
on the determination of the cost to the public.

Conclusion

    The FAA reviewed the relevant data and determined that air safety
and the public interest require adopting this final rule as proposed,
except for minor editorial changes. The FAA has determined that these
minor changes:
     Are consistent with the intent that was proposed in the
NPRM for addressing the unsafe condition; and
     Do not add any additional burden upon the public than was
already proposed in the NPRM.

Related Service Information Under 1 CFR Part 51

    This AD requires EASA AD 2021-0144, which the Director of the
Federal Register approved for incorporation by reference as of
September 7, 2021 (86 FR 46766, August 20, 2021). This material is
reasonably available because the interested parties have access to it
through their normal course of business or by the means identified in
the ADDRESSES section.

Differences Between this AD and the MCAI

    Paragraph (1) of EASA AD 2021-0144 specifies the inspection must be
done within 25 flight hours or 3 months, whichever occurs first.
However, this AD requires the inspection to be done within 25 hours
time-in-service after September 7, 2021 (the effective date of AD 2021-
17-18).

Interim Action

    The FAA considers this AD interim action. The inspection reports
that are required by this AD will enable the manufacturer to obtain
better insight into the nature, cause, and extent of the cracking, and
eventually to develop final action to address the unsafe condition.
Once final action has been identified, the FAA might consider further
rulemaking.

Costs of Compliance

    The FAA estimates that this AD affects 133 helicopters of U.S.
registry. The FAA estimates the following costs to comply with this AD:

                                      Estimated Costs for Required Actions
----------------------------------------------------------------------------------------------------------------
                                                                                Cost on U.S.
              Action                    Labor cost        Parts cost      Cost per product        operators
----------------------------------------------------------------------------------------------------------------
Retained Inspections/from AD 2021- Up to 6 work-hours               $0  Up to $510 per       Up to $67,830 per
 17-18.                             x $85 per hour =                     inspection/          inspection/
                                    $510 per                             measurement cycle.   measurement cycle.
                                    inspection/
                                    measurement cycle.
New Repetitive Inspections.......  Up to 1 work-hour x               0  Up to $85 per        Up to $11,305 per
                                    $85 per hour = $85                   inspection cycle.    inspection cycle.
                                    per inspection
                                    cycle.
----------------------------------------------------------------------------------------------------------------

    The FAA estimates the following costs to do any necessary on-
condition actions (replacements, repairs, and reporting) that would be
required based on the results of any required actions. The FAA has no
way of determining the number of helicopters that might need these on-
condition actions:

                                    Estimated Costs of On-Condition Actions *
----------------------------------------------------------------------------------------------------------------
                 Action                           Labor cost            Parts cost         Cost per product
----------------------------------------------------------------------------------------------------------------
Retained Replacements...................  19 work-hours x $85 per            $88,760  Up to $90,375.
                                           hour = $1,615.
Retained Reporting......................  1 work-hour x $85 per hour              $0  $85.
                                           = $85.
----------------------------------------------------------------------------------------------------------------
* The FAA has received no definitive data on which to base the cost estimates for the on-condition repairs
  specified in this proposed AD.

    According to the manufacturer, some or all of the costs of this AD
may be covered under warranty, thereby reducing the cost impact on
affected operators. The FAA does not control warranty coverage for
affected operators. As a result, the FAA has included all known costs
in the cost estimate.

Paperwork Reduction Act

    A federal agency may not conduct or sponsor, and a person is not
required to respond to, nor shall a person be subject to penalty for
failure to comply with a collection of information subject to the
requirements of the Paperwork Reduction Act unless that collection of
information displays a current valid OMB control number. The control
number for the collection of information required by this AD is 2120-
0056. The paperwork cost associated with this AD has been detailed in
the Costs of Compliance section of this document and includes time for
reviewing instructions, as well as completing and reviewing the
collection of information. Therefore, all reporting associated with
this AD is mandatory. Comments concerning the accuracy of this burden
and suggestions for reducing the burden should be directed to
Information Collection Clearance Officer, Federal Aviation
Administration, 10101 Hillwood Pkwy., Fort Worth, TX 76177-1524.

Authority for This Rulemaking

    Title 49 of the United States Code specifies the FAA's authority to
issue rules on aviation safety. Subtitle I, section 106, describes the
authority of the FAA Administrator. Subtitle VII: Aviation Programs,
describes in more detail the scope of the Agency's authority.
    The FAA is issuing this rulemaking under the authority described in
Subtitle VII, Part A, Subpart III, Section 44701: General requirements.
Under that section, Congress charges the FAA with promoting safe flight
of civil aircraft in air commerce by prescribing regulations for
practices, methods, and procedures the Administrator finds necessary
for safety in air commerce. This regulation is within the scope of that
authority because it addresses an unsafe condition that is likely to
exist or develop on products identified in this rulemaking action.

Regulatory Findings

    This AD will not have federalism implications under Executive Order
13132. This AD will not have a substantial direct effect on the States,
on the relationship between the national government and the States, or
on the distribution of power and responsibilities among the various
levels of government.
    For the reasons discussed above, I certify that this AD:
    (1) Is not a ``significant regulatory action'' under Executive
Order 12866,
    (2) Will not affect intrastate aviation in Alaska, and
    (3) Will not have a significant economic impact, positive or
negative, on a substantial number of small entities under the criteria
of the Regulatory Flexibility Act.

List of Subjects in 14 CFR Part 39

    Air transportation, Aircraft, Aviation safety, Incorporation by
reference, Safety.

The Amendment

    Accordingly, under the authority delegated to me by the
Administrator, the FAA amends 14 CFR part 39 as follows:

PART 39--AIRWORTHINESS DIRECTIVES

0
1. The authority citation for part 39 continues to read as follows:

    Authority:  49 U.S.C. 106(g), 40113, 44701.

Sec.  39.13  [Amended]

0
2. The FAA amends Sec.  39.13 by:
0
a. Removing Airworthiness Directive (AD) 2021-17-18, Amendment 39-21701
(86 FR 46766, August 20, 2021); and
0
b. Adding the following new AD:

2022-07-11 Leonardo S.p.a.: Amendment 39-21999; Docket No. FAA-2022-
0024; Project Identifier MCAI-2021-00994-R.

(a) Effective Date

    This airworthiness directive (AD) is effective May 5, 2022.

(b) Affected ADs

    This AD replaces AD 2021-17-18, Amendment 39-21701 (86 FR 46766,
August 20, 2021) (AD 2021-17-18).

(c) Applicability

    This AD applies to all Leonardo S.p.a. Model A109C, A109K2,
A109E, A109S, and AW109SP helicopters, certificated in any category.

(d) Subject

    Joint Aircraft System Component (JASC) Code 6400, Tail Rotor
System.

(e) Unsafe Condition

    This AD was prompted by a report of a crack on the tail rotor
(TR) mast. The FAA is issuing this AD to address cracking on the TR
mast, which could lead to failure of the TR mast, with consequent
loss of control of the helicopter.

(f) Compliance

    Comply with this AD within the compliance times specified,
unless already done.

(g) Requirements

    Except as specified in paragraph (h) of this AD: Comply with all
required actions and compliance times specified in, and in
accordance with, European Union Aviation Safety Agency (EASA) AD
2021-0144, dated June 17, 2021 (EASA AD 2021-0144).

(h) Exceptions to EASA AD 2021-0144

    (1) Where EASA AD 2021-0144 refers to its effective date, this
AD requires using September 7, 2021 (the effective date of AD 2021-
17-18).
    (2) The ``Remarks'' section of EASA AD 2021-0144 does not apply
to this AD.
    (3) Where EASA AD 2021-0144 refers to flight hours (FH), this AD
requires using hours time-in-service.
    (4) Where paragraph (1) of EASA AD 2021-0144 specifies a
compliance time of 25 FH or 3 months, whichever occurs first, this
AD requires compliance within 25 hours time-in-service after
September 7, 2021 (the effective date of AD 2021-17-18).
    (5) Where Note 1 of EASA AD 2021-0144 specifies a tolerance of
30 FH, this AD does not allow a tolerance.
    (6) The initial compliance time for the inspection specified in
paragraph (5) of EASA AD 2021-0144 is at the compliance time
specified in paragraph (5) of EASA AD 2021-0144, or within 30 days
after the effective date of this AD, whichever occurs later.
    (7) Where paragraph (6) of EASA AD 2021-0144 states the term
``discrepancies,'' for the purposes of this AD discrepancies include
dents, corrosion, elongation, scratches, wear, excessive wear (web
visible), fretting, or stepping.
    (8) Where paragraph (7) of EASA AD 2021-0144 states the term
``discrepancies,'' for the purposes of this AD discrepancies include
abnormal wear condition, corrosion, fretting, crack, or damage
(including dents, elongation, scratches, or stepping).
    (9) Where EASA AD 2021-0144 defines ``serviceable part,'' and
that definition specifies instructions that are ``approved under
Leonardo Design Organization Approval (DOA) or by EASA,'' for this
AD, the repair must be accomplished using a method approved by the
Manager, General Aviation and Rotorcraft Section, International
Validation Branch, FAA; or EASA; or Leonardo S.p.a.'s EASA DOA. If
approved by the DOA, the approval must include the DOA-authorized
signature.
    (10) Where Note 2 and paragraph (7) of EASA AD 2021-0144 specify
instructions that are ``approved under Leonardo DOA or by EASA,''
for this AD, the repair must be accomplished using a method approved
by the Manager, General Aviation and Rotorcraft Section,
International Validation Branch, FAA; or EASA; or Leonardo S.p.a.'s
EASA DOA. If approved by the DOA, the approval must include the DOA-
authorized signature.
    (11) Where the service information referenced in EASA AD 2021-
0144 specifies to contact the manufacturer for corrective action,
this AD requires the repair to be done in accordance with a method
approved by the Manager, General Aviation and Rotorcraft Section,
International Validation Branch, FAA; or EASA; or Leonardo S.p.a.'s
EASA DOA. If approved by the DOA, the approval must include the DOA-
authorized signature.
    (12) Where the service information referenced in EASA AD 2021-
0144 specifies to discard a certain part, this AD requires removing
that part from service.

(i) Special Flight Permit

    Special flight permits may be issued in accordance with 14 CFR
21.197 and 21.199 to operate the helicopter to a location where the
actions of this AD can be performed, provided no passengers are
onboard.

(j) Alternative Methods of Compliance (AMOCs)

    (1) The Manager, International Validation Branch, FAA, has the
authority to approve AMOCs for this AD, if requested using the
procedures found in 14 CFR 39.19. In accordance with 14 CFR 39.19,
send your request to your principal inspector or local Flight
Standards District Office, as appropriate. If sending information
directly to the manager of the International Validation Branch, send
it to the attention of the person identified in paragraph (k) of
this AD. Information may be emailed to: [email protected].
    (2) Before using any approved AMOC, notify your appropriate
principal inspector, or lacking a principal inspector, the manager
of the local flight standards district office/certificate holding
district office.

(k) Related Information

    For more information about this AD, contact Andrea Jimenez,
Aerospace Engineer, COS Program Management Section, Operational
Safety Branch, FAA, 1600 Stewart Ave., Suite 410, Westbury, NY
11590; phone:<PHONE_NUMBER>; email: [email protected].

(l) Material Incorporated by Reference

    (1) The Director of the Federal Register approved the
incorporation by reference (IBR) of the service information listed
in this paragraph under 5 U.S.C. 552(a) and 1 CFR part 51.
    (2) You must use this service information as applicable to do
the actions required by this AD, unless this AD specifies otherwise.
    (3) The following service information was approved for IBR on
September 7, 2021 (86 FR 46766, August 20, 2021).
    (i) European Union Aviation Safety Agency (EASA) AD 2021-0144,
dated June 17, 2021.
    (ii) [Reserved]
    (4) For EASA AD 2021-0144, contact the EASA, Konrad-Adenauer-
Ufer 3, 50668 Cologne, Germany; phone: +49 221 8999 000; email:
[email protected]; Internet: www.easa.europa.eu. You may find this
EASA AD on the EASA website at https://ad.easa.europa.eu.
    (5) You may view this service information at the FAA, Office of
the Regional Counsel, Southwest Region, 10101 Hillwood Pkwy., Room
6N-321, Fort Worth, TX 76177. For information on the availability of
this material at the FAA, call<PHONE_NUMBER>. This material may be
found in the AD docket on the internet at https://www.regulations.gov by searching for and locating Docket No. FAA-
2022-0024.
    (6) You may view this material that is incorporated by reference
at the National Archives and Records Administration (NARA). For
information on the availability of this material at NARA, email
[email protected], or go to: https://www.archives.gov/federal-register/cfr/ibr-locations.html.

    Issued on March 24, 2022.
Lance T. Gant,
Director, Compliance & Airworthiness Division, Aircraft Certification
Service.
[FR Doc. 2022-06620 Filed 3-30-22; 8:45 am]
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