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The document was marked with 5 Deletions, 5 Insertions, 0 Moves. 6560 50 P ENVIRONMENTAL PROTECTION AGENCY 40 CFR Part 63 [ OAR 2002 0088, FRL ]

RIN 2060 AM90 National Emission Standards for Hazardous Air Pollutants for Refractory Products Manufacturing AGENCY: Environmental Protection Agency ( EPA).

ACTION: Direct final rule; amendments.

SUMMARY: EPA is taking direct final action on amendments to the national emission standards for hazardous air pollutants ( NESHAP) for new and existing refractory products manufacturing facilities, which were promulgated on April 16, 2003, under section 112( d) of the Clean Air Act ( CAA).

The amendments clarify the testing and monitoring requirements and startup and shutdown requirements for batch processes, make certain technical corrections, and add recent changes to be consistent with the NESHAP General Provisions.

DATES: The direct final rule is effective [ INSERT DATE 90 DAYS AFTER PUBLICATION OF THE DIRECT FINAL RULE IN THE FEDERAL REGISTER] without further notice, unless adverse comments are received by [ INSERT DATE 45 DAYS AFTER PUBLICATION OF THE DIRECT FINAL RULE IN THE FEDERAL REGISTER] or by [ INSERT THE DATE 60 DAYS AFTER PUBLICATION OF THE DIRECT FINAL RULE IN THE FEDERAL REGISTER] if a 3 public hearing is requested. If we receive such comment, we will publish a timely withdrawal in the Federal Register which amendments will become effective and which amendments are being withdrawn due to adverse comment.

ADDRESSES: Submit your comments, identified by Docket ID No. OAR 2002 0088, by one of the following methods:

! Federal eRulemaking Portal:

http:// www. regulations. gov. Follow the on line instructions for submitting comments.

! Agency Website: http:// www. epa. gov/ edocket.

EDOCKET, EPA's electronic public docket and comment system, is EPA's preferred method for receiving comments. Follow the on line instructions for submitting comments.

! E mail: a and r docket@ epa. gov ! Fax: ( 202) 566 1741 ! Mail: EPA Air Docket, Mailcode: 6102T, 1200 Pennsylvania Ave., NW, Washington, DC 20460. Please include a total of two copies.

! Hand Delivery: Air and Radiation Docket, Room B

108, EPA, 1301 Constitution Avenue, NW, Washington,

DC 20460, Attention Docket ID No. OAR 2002 0088.

Such deliveries are only accepted during the Docket's normal hours of operation, and special arrangements should be made for deliveries of boxed information. 4 Instructions: Direct your comments to Docket ID No. OAR

2002 0088. EPA's policy is that all comments received will be included in the public docket without change and may be made available online at http:// www. epa. gov/ edocket,

including any personal information provided, unless the comment includes information claimed to be Confidential Business Information ( CBI) or other information whose disclosure is restricted by statute. Do not submit information that you consider to be CBI or otherwise protected through EDOCKET, regulations. gov, or e mail. The EPA EDOCKET and the federal regulations. gov websites are " anonymous access" systems, which means EPA will not know your identity or contact information unless you provide it in the body of your comment. If you send an e mail comment directly to EPA without going through EDOCKET or regulations. gov, your e mail address will be automatically captured and included as part of the comment that is placed in the public docket and made available on the Internet. If you submit an electronic comment, EPA recommends that you include your name and other contact information in the body of your comment and with any disk or CD ROM you submit. If EPA cannot read your comment due to technical difficulties and cannot contact you for clarification, EPA may not be able to consider your comment. Electronic files should avoid the use of special characters, any form of encryption,

and be free of any defects or viruses. For additional 5 information about EPA's public docket visit EDOCKET on line or see the Federal Register of May 31, 2002 ( 67 FR 38102).

Docket: All documents in the docket are listed in the EDOCKET index at http:// www. epa. gov/ edocket. Although listed in the index, some information is not publicly available, i. e., CBI or other information whose disclosure is restricted by statute. Certain other material, such as copyrighted material, is not placed on the Internet and will be publicly available only in hard copy form. Publicly available docket materials are available either electronically in EDOCKET or in hard copy form at Air and Radiation Docket, EPA/ DC, EPA West, Room B102, 1301 Constitution Ave., NW, Washington, DC. The Public Reading Room is open from 8: 30 a. m. to 4: 30 p. m., Monday through Friday, excluding legal holidays. The telephone number for the Public Reading Room is ( 202) 566 1744, and the telephone number for the Air Docket is ( 202) 566 1742.

FOR FURTHER INFORMATION CONTACT: Susan Fairchild, Emission Standards Division ( C504 05), Office of Air Quality Planning and Standards, EPA, Research Triangle Park, NC 27711;

telephone number ( 919) 541 5167; fax number ( 919) 541 5600;

e mail address: fairchild. susan@ epa. gov.

SUPPLEMENTARY INFORMATION:

Regulated Entities. Categories and entities potentially regulated by this action include those listed in the following table: 6 Category NAICS Examples of regulated entities Industrial 327124 Clay refractories manufacturing plants Industrial 327125 Nonclay refractories manufacturing plants This table is not intended to be exhaustive, but rather provides a guide for readers regarding entities likely to be regulated by this action. To determine whether your facility is regulated by this action, you should examine the applicability criteria in § 63.9782 of the Refractory Products Manufacturing NESHAP. If you have any questions regarding the applicability of this action to a particular entity, consult the person listed in the preceding FOR FURTHER INFORMATION CONTACT section.

Worldwide Web ( WWW). In addition to being available in the docket, an electronic copy of today's document will also be available on the WWW. Following the Administrator's signature, a copy of this action will be posted at www. epa. gov/ ttn/ oarpg on EPA's Technology Transfer Network ( TTN) policy and guidance page for newly proposed or promulgated rules. The TTN provides information and technology exchange in various areas of air pollution control.

Comments. We are publishing the direct final rule without prior proposal because we view the amendments as noncontroversial and do not anticipate adverse comments because the amendments clarify several of the requirements 7 of the NESHAP, bring the NESHAP into consistency with the General Provisions to 40 CFR part 63, and make technical corrections to the NESHAP. However, in the Proposed Rules section of this Federal Register, we are publishing a separate document that will serve as the proposal to amend the NESHAP for refractory products manufacturing facilities if adverse comments are filed.

If we receive adverse comment on one or more distinct amendments, we will publish a timely withdrawal in the Federal Register informing the public which amendments will become effective and which amendments are being withdrawn due to adverse comment. We will address all public comments on withdrawn amendments in a subsequent final rule. We will not institute a second comment period on this action. Any parties interested in commenting must do so at this time.

Judicial Review. Under section 307( b)( 1) of the CAA,

judicial review of the direct final rule amendments is available only by filing a petition for review in the U. S.

Court of Appeals for the District of Columbia Circuit by [ INSERT DATE 90 DAYS AFTER DATE OF PUBLICATION OF THIS DIRECT FINAL RULE IN THE FEDERAL REGISTER]. Under section 307( d)( 7)( B) of the CAA, only an objection to the direct final rule which was raised with reasonable specificity during the period for public comment can be raised during judicial review. Moreover, under section 307( b)( 2) of the CAA, the requirements established by the direct final rule 8 may not be challenged separately in any civil or criminal proceedings brought by EPA to enforce these requirements.

Outline. The information presented in this preamble is organized as follows:

I. Background II. Amendments to 40 CFR Part 63, Subpart SSSSS A. Emission Testing B. Control Device Operation C. Operating Limits D. Monitoring E. Other Changes F. Table 1. Summary of Amendments to Subpart SSSSS III. Statutory and Executive Order Reviews A. Executive Order 12866: Regulatory Planning and Review B. Paperwork Reduction Act C. Regulatory Flexibility Act D. Unfunded Mandates Reform Act E. Executive Order 13132: Federalism F. Executive Order 13175: Consultation and Coordination with Indian Tribal Governments G. Executive Order 13045: Protection of Children from Environmental Health Risks and Safety Risks H. Executive Order 13211: Actions that Significantly Affect Energy Supply, Distribution, or Use I. National Technology Transfer and Advancement Act J. Congressional Review Act I. Background EPA promulgated the NESHAP for new and existing refractory products manufacturing facilities on April 16,

2003 ( 68 FR 18730) as 40 CFR part 63, subpart SSSSS.

Shortly after promulgation of the Refractory Products Manufacturing NESHAP, EPA also promulgated amendments to the General Provisions to 40 CFR part 63 ( 68 FR 32586, May 30,

2003). After reviewing the final amendments to the General Provisions and comparing those to the Refractory Products Manufacturing NESHAP, we discovered discrepancies between sections of the General Provisions as cited in the NESHAP 9 and the newly amended sections of the General Provisions.

We also identified minor technical errors and other specific sections of the Refractory Products Manufacturing NESHAP that needed clarification. Today's action includes amendments to the Refractory Products Manufacturing NESHAP that clarify the requirements for testing, control device operation, operating limits, and monitoring.

II. Amendments to 40 CFR Part 63, Subpart SSSSS A. Emission Testing The Refractory Products Manufacturing NESHAP specify several requirements that pertain to the testing of batch process sources. Because emissions of hazardous air pollutants ( HAP) from a batch process source can vary significantly over the course of a batch cycle, the NESHAP specify emission limits in terms of the peak emissions period. In today's action, we are revising the definition of the peak emissions period in terms of the applicable emission limits to include separate definitions for the 3

hour peak total hydrocarbons ( THC) mass emissions period,

which applies to batch process sources that comply with the THC percentage reduction limit; the 3 hour peak THC emissions concentration period, which applies to batch sources that satisfy the THC emission concentration limit;

and the 3 hour peak hydrogen fluoride ( HF) mass emissions period, which pertains to the emission limits for batch process clay refractory products kilns. All references to 10 the peak emissions period in the tables to 40 CFR part 63,

subpart SSSSS, have been revised for consistency.

The NESHAP include provisions to allow the owner or operator of an affected batch process source to develop an emissions profile and use the profile to limit emissions testing to the peak emissions period. In today's action, we are amending 40 CFR 63.9802 to clarify that emissions profiles for sources subject to the THC emission limits must be developed using data collected at the maximum organic HAP processing rate. This amendment also clarifies that a new emissions profile must be developed if a facility wants to use an emissions profile to limit testing to the peak emissions period at a process, but increases its maximum organic HAP processing rate at that process. In addition,

we are amending 40 CFR 63.9802 to clarify that emissions profiles for batch process clay refractory kilns must be developed using data from when the kiln is processing the clay refractory product with the highest uncalcined clay processing rate.

We are amending 40 CRF 63.9798( a) to eliminate the reference to permit renewal, and stating that subsequent performance tests must be conducted at least every 5 years.

Item 1( b)( i)( 1) of Table 4 to Subpart SSSSS of Part 63 is amended to clarify that a sampling port is also required at the control device inlet if the owner or operator plans to develop an emissions profile or use the provision for 11 reducing the operating temperature of a thermal or catalytic oxidizer on an affected batch process source. In both cases, sampling is required at the control device inlet.

Item 8( a)( i)( 5) of Table 4 to Subpart SSSSS of Part 63 is amended to specify the THC concentration in terms of the outlet of the control device. We also made other minor changes to this provision in Table 4 to simplify the wording.

Item 13 of Table 4 to Subpart SSSSS of Part 63 is amended to eliminate the reference to the THC percentage reduction limit. We have clarified that regardless of which THC emission limit applies to a specific source, the owner or operator of the source must measure not only the THC concentration but also the oxygen concentration at the control device inlet for at least the 1 hour period that immediately follows the temperature reduction. This measurement is necessary for demonstrating that the source is meeting the limit of 20 parts per million dry volume ( ppmvd) THC, corrected to 18 percent oxygen, after the oxidizer temperature has been reduced.

Item 13. a. 5 of Table 4 to Subpart SSSSS of Part 63 is amended to clarify that only the THC emissions concentration limit applies following any reduction in the oxidizer temperature. We received comment on the proposed rule ( 67 FR 42108, June 20, 2002) requesting a second emission limit be allowed for sources wanting to meet a percentage 12 reduction limit rather than an emission concentration limit.

The commenter believed that since EPA had promulgated percentage reduction limits for other MACT standards to reduce emissions of THC, and since air pollution control devices are usually rated and installed with a minimum percent reduction achieved by the devices, that emission limit would be simpler to meet. At promulgation of the final rule ( April 16, 2003, 68 FR 18730), we changed the rule to allow regulated sources to meet either the percentage reduction limit or the concentration limit.

In the final rule, we allowed the choice between either the percentage reduction limit or the concentration limit,

but required owners and operators to meet the selected emission limit during all times of operation. We also allowed owners and operators the option to turn off the control device when it was no longer needed. However, for those owners or operators meeting the percentage reduction compliance option, it is not possible to meet that limit if the control device is not in operation. We believe that conserving energy is a beneficial option for all owners and operators, and regardless of the compliance option selected,

all should have the opportunity to benefit from turning off the control device when it is no longer needed. Thus, we are clarifying that whether an owner or operator shows compliance with the percentage reduction limit or the concentration limit, compliance with the rule for a unit 13 with a control device no longer in operation may only be demonstrated by meeting the concentration limit, that is,

when the THC emissions are below 20 ppmvd corrected to 18 percent oxygen from the heated process unit. Owners and operators in this case may choose to meet the percentage reduction limit before turning off the control device and may show compliance with the concentration limit after turning off the control device.

Item 14( a)( i)( 1) of Table 4 to Subpart SSSSS of Part 63 is amended to specify that the performance tests must be performed while processing the clay refractory product with the highest uncalcined clay processing rate.

B. Control Device Operation Refractory products manufacturing plants typically produce a wide range of products, some of which may contain organic HAP binders or additives, while other products may contain only inorganic binders or additives that do not contain or form HAP. Many plants do not have dedicated thermal process units ( e. g., dryers and kilns) for each type of product they manufacture and instead, use the same process units to manufacture products that emit HAP and products that do not contain or emit HAP. Recognizing this situation, we are amending 40 CFR 63.9792 of the NESHAP to clarify that control devices used to comply with the emission limits established by 40 CFR part 63, subpart SSSSS, do not have to be operated when an otherwise affected 14 process unit is processing products that do not contain or release HAP. This amendment applies to sources subject to the THC emission limits as well as the emission limits for HF and hydrochloric acid ( HCl).

Table 3 to Subpart SSSSS of Part 63, which specifies work practice standards, includes several options for controlling emissions of polycyclic organic matter ( POM)

from shape preheaters and pitch working tanks used in the manufacture of pitch impregnated refractory products.

Options include exhausting the affected source to a thermal or catalytic oxidizer that is comparable to a thermal or catalytic oxidizer that is used to meet the emission limits for an affected defumer or coking oven. To clarify what is meant by a " comparable" thermal or catalytic oxidizer, we are amending 40 CFR 63.9824 to include a definition of " comparable control device."

C. Operating Limits The Refractory Products Manufacturing NESHAP refer to the operating limit as the " maximum allowable organic HAP processing rate." We are amending the definition of maximum organic HAP processing rate in 40 CFR 63.9824 to distinguish between the operating limit and the actual processing rate measured during the performance test.

The Refractory Products Manufacturing NESHAP include several operating limits for clay refractory products kilns that are controlled by dry limestone adsorbers ( DLA). We 15 are amending the NESHAP to eliminate the operating limits of maintaining free flowing limestone throughout the DLA because the term " free flowing" may not be appropriate for the grade of limestone used in DLA. The remaining operating limits specified for DLA in the NESHAP are adequate for ensuring compliance with the emission limits for clay refractory products kilns.

As specified in Table 2 ( Requirements for Establishing Operating Limits) of the rule, Subpart SSSSS of Part 63,

owners and operators of certain thermal process sources of organic HAP are required to establish an operating limit for the maximum organic HAP processing rate. The organic HAP processing rate is a function of the amount of organic HAP in the raw materials and the amounts of those raw materials in the refractory product formulation. Because there are minor variations in the content of organic HAP in a specific binder or additive, the operating limit for the maximum organic HAP processing rate can inadvertently be exceeded without changing the product formulation. In today's action, we are amending the procedure for establishing the operating limit and clarifying that minor exceedances of the maximum organic HAP processing rate established during the performance test are not violations of the operating limit.

Specifically, we are amending items 3( b) and 8( b) of Table 4 ( Requirements for Performance Tests) to Subpart SSSSS of Part 63 to be consistent with the requirements in Table 2 16 that reflect a 10 percent allowance when calculating the operating limit.

Today's action amends the procedures for determining minimum temperature operating limits for thermal and catalytic oxidizers that are used to control emissions from certain batch process sources of organic HAP as they pertain to sources that comply with the provisions for reducing the operating temperature of a thermal or catalytic oxidizer.

We are also amending subpart SSSSS to clarify that owners or operators of batch process sources controlled with thermal or catalytic oxidizers must measure the oxidizer operating temperature throughout each entire test run.

D. Monitoring The Refractory Products Manufacturing NESHAP require THC continuous emission monitoring systems ( CEMS) on thermal process sources of organic HAP that use process changes or control devices other than thermal or catalytic oxidizers to meet the THC emission limits. We are amending 40 CFR 63.9800( i)( 1) by adding a reference to sources that use process changes to meet the emission limits.

We are also amending 40 CFR 63.9800( i) to state that such sources must maintain the 3 hour block average THC concentration at or below 20 ppmvd, corrected to 18 percent oxygen.

Today's action amends the definition of " deviation" in 40 CFR 63.9824 to include failure to provide adequate 17 continuous monitoring systems ( CMS) data for demonstrating compliance with any emission limit or other requirement. In addition, we are amending the requirement that the owner or operator of an affected source that is required to use a CMS to meet an operating limit must report any deviations from those operating limits.

E. Other Changes We are amending the Refractory Products Manufacturing NESHAP to include definitions for Shutdown and Startup to preclude unnecessary reporting of batch process source operation.

III. Statutory and Executive Order Reviews A. Executive Order 12866: Regulatory Planning and Review Under Executive Order 12866 ( 58 FR 51735, October 4,

1993), EPA must determine whether the regulatory action is " significant" and, therefore, subject to review by the Office of Management and Budget ( OMB) and the requirements of the Executive Order. The Executive Order defines " significant regulatory action" as one that is likely to result in a rule that may:

( 1) Have an annual effect on the economy of $ 100 million or more or adversely affect in a material way the economy, a sector of the economy, productivity, competition,

jobs, the environment, public health or safety, or State,

local, or tribal governments or communities;

( 2) create a serious inconsistency or otherwise 18 interfere with an action taken or planned by another agency;

( 3) materially alter the budgetary impact of entitlements, grants, user fees, or loan programs, or the rights and obligation of recipients thereof; or ( 4) raise novel legal or policy issues arising out of legal mandates, the President's priorities, or the principles set forth in the Executive Order.

Pursuant to the terms of Executive Order 12866, it has been determined that the direct finalthis rule amendments do not constituteis a " significant regulatory action" because none of the listed criteria apply to this action.

Consequentlyit raises novel legal or policy issues arising out of legal mandates. As such, this action was not submitted to OMB for review under Executive Order 12866.

Changes made in response to OMB suggestions or recommendations will be documented in the public record.

B. Paperwork Reduction Act This action does not impose an information collection burden under the provisions of the Paperwork Reduction Act,

44 U. S. C. 3501 et seq. OMB approved the information collection requests for the NESHAP for refractory products manufacturing pursuant to the provisions of the Paperwork Reduction Act, 44 U. S. C. 3501 et seq. OMB assigned OMB control number 2060 0515 ( EPA ICR No. 2040.01) to these information collection requests. A copy of the Information Collection Request ( ICR) may be obtained from Susan Auby by 19 mail at US EPA, Office of Environmental Information,

Collection Strategies Division ( MD 2822T), 1200 Pennsylvania Ave., NW, Washington, DC 20460; by e mail at auby. susan@ epa. gov; or by calling ( 202) 566 1672. You may also download a copy off the Internet at http:// www. epa. gov/ icr.

Today's action makes clarifying changes to the NESHAP for refractory products manufacturing and imposes no new information collection requirements on the industry.

Because there is no additional burden on the industry as a result of the direct final rule amendments, the ICR has not been revised.

Burden means the total time, effort, or financial resources expended by persons to generate, maintain, retain,

or disclose or provide information to or for a Federal agency. This includes the time needed to review instructions; develop, acquire, install, and utilize technology and systems for the purposes of collecting,

validating, and verifying information, processing and maintaining information, and disclosing and providing information; adjust the existing ways to comply with any previously applicable instructions and requirements; train personnel to be able to respond to a collection of information; search data sources; complete and review the collection of information; and transmit or otherwise disclose the information. 20 An agency may not conduct or sponsor, and a person is not required to respond to, a collection of information unless it displays a current valid OMB control number. The OMB control numbers for EPA's regulations are listed in 40 CFR part 9 and 48 CFR chapter 15.

C. Regulatory Flexibility Act EPA has determined that it is not necessary to prepare a regulatory flexibility analysis in connection with this final rule.

For purposes of assessing the impacts of today's rule on small entities, small entity is defined as: ( 1) a small business as defined by the Small Business Administrations'

regulations at 13 CFR 121.201; ( 2) a small governmental jurisdiction that is a government of a city, county, town,

school district or special district with a population of less than 50,000; and ( 3) a small organization that is any not for profit enterprise which is independently owned and operated and is not dominant in its field.

After considering the economic impacts of today's direct final rule amendments on small entities, EPA has concluded that this action will not have a significant economic impact on a substantial number of small entities ( SISNOSE). At promulgation of the Refractory Products Manufacturing NESHAP, EPA determined that one facility, or 17 percent of all facilities, is owned by a small company and would experience an impact of less than one half of one 21 percent (< 0.50 percent) of company sales. EPA found no SISNOSE for the underlying rule, and the direct final rule amendments are minor corrections and clarifications to that rule that do not add any additional requirements.

Although the direct final rule amendments will not have a significant economic impact on a substantial number of small entities, EPA nonetheless has tried to reduce the impact of the direct final rule amendments on small entities. EPA has limited the amendments to changes that clarify ambiguities of the Refractory Products Manufacturing NESHAP, correct citations to the General Provisions, and clarify the complex batch testing requirements of the Refractory Products Manufacturing NESHAP. EPA believes that the amendments will simplify the NESHAP and will not add additional burden to regulated entities.

D. Unfunded Mandates Reform Act Title II of the Unfunded Mandates Reform Act of 1995 ( UMRA), Public Law No. 104 4, establishes requirements for Federal agencies to assess the effects of their regulatory actions on State, local, and tribal governments and the private sector. Under section 202 of the UMRA, EPA generally must prepare a written statement, including a cost benefit analysis, for proposed and final rules with " Federal mandates" that may result in expenditures by State,

local, and tribal governments, in the aggregate, or by the private sector, of $ 100 million or more in any 1 year. 22 Before promulgating an EPA rule for which a written statement is needed, section 205 of the UMRA generally requires EPA to identify and consider a reasonable number of regulatory alternatives and adopt the least costly, most cost effective, or least burdensome alternative that achieves the objectives of the rule. The provisions of section 205 do not apply when they are inconsistent with applicable law. Moreover, section 205 allows EPA to adopt an alternative other than the least costly, most costeffective or least burdensome alternative if the Administrator publishes with the final rule an explanation why that alternative was not adopted. Before EPA establishes any regulatory requirements that may significantly or uniquely affect small governments,

including tribal governments, it must have developed under section 203 of the UMRA a small government agency plan. The plan must provide for notifying potentially affected small governments, enabling officials of affected small governments to have meaningful and timely input in the development of EPA's regulatory proposals with significant Federal intergovernmental mandates, and informing,

educating, and advising small governments on compliance with the regulatory requirements.

The EPA has determined that today's direct final rule amendments do not contain a Federal mandate that may result in expenditures of $ 100 million or more for State, local, 23 and tribal governments, in the aggregate, or the private sector in any 1 year, nor do the direct final rule amendments significantly or uniquely impact small governments because there are no requirements that apply to such governments or impose obligations upon them.

Therefore, today's direct final rule amendments are not subject to the requirements of sections 202 and 205 of the UMRA.

E. Executive Order 13132: Federalism Executive Order 13132, entitled " Federalism" ( 64 FR 43255, August 10, 1999), requires EPA to develop an accountable process to ensure " meaningful and timely input by State and local officials in the development of regulatory policies that have federalism implications."

" Policies that have federalism implications" is defined in the Executive Order to include regulations that have " substantial direct effects on the States, on the relationship between the national government and the States,

or on the distribution of power and responsibilities among the various levels of government."

The direct final rule amendments do not have federalism implications. They will not have substantial direct effects on the States, on the relationship between the national government and the States, or on the distribution of power and responsibilities among the various levels of government,

as specified in Executive Order 13132. None of the affected 24 facilities are owned or operated by State governments, and the direct final rule amendments will not supercede State regulations that are more stringent. Thus, Executive Order 13132 does not apply to the direct final rule amendments.

F. Executive Order 13175: Consultation and Coordination with Indian Tribal Governments Executive Order 13175, entitled " Consultation and Coordination with Indian Tribal Governments" ( 65 FR 67249,

November 9, 2000), requires EPA to develop an accountable process to ensure " meaningful and timely input by tribal officials in the development of regulatory policies that have tribal implications." The direct final rule amendments do not have tribal implications, as specified in Executive Order 13175. They will not have substantial direct effects on tribal governments, on the relationship between the Federal government and Indian tribes, or on the distribution of power and responsibilities between the Federal government and Indian tribes, as specified in Executive Order 13175.

No tribal governments own or operate refractory products manufacturing facilities. Thus, Executive Order 13175 does not apply to the direct final rule amendments.

G. Executive Order 13045: Protection of Children from Environmental Health Risks and Safety Risks Executive Order 13045 ( 62 FR 19885, April 23, 1997)

applies to any rule that ( 1) is determined to be " economically significant" as defined under Executive Order 25 12866 and ( 2) concerns an environmental health or safety risk that EPA has reason to believe may have a disproportionate effect on children. If the regulatory action meets both criteria, EPA must evaluate the environmental health or safety effects of the planned rule on children and explain why the planned rule is preferable to other potentially effective and reasonably feasible alternatives that EPA considered.

EPA interprets Executive Order 13045 as applying only to those regulatory actions that are based on health or safety risks, such that the analysis required under section 5 501 of the Executive Order has the potential to influence the regulation. Today's direct final rule amendments are not subject to Executive Order 13045 because they are based on technology performance and not on health or safety risks.

In addition, the direct final rule amendments have been determined not to be " economically significant" as defined under Executive Order 12866.

H. Executive Order 13211: Actions Concerning Regulations that Significantly Affect Energy Supply, Distribution, or Use Today's direct final rule amendments are not subject to Executive Order 13211 ( 66 FR 28355, May 22, 2001) because they are not a significant regulatory action under Executive Order 12866.

I. National Technology Transfer and Advancement Act of 1995 Section 12( d) of the National Technology Transfer and Advancement Act ( NTTAA) of 1995 ( Public Law No. 104 113;

15 U. S. C. 272 note) directs EPA to use voluntary consensus standards in their regulatory and procurement activities unless to do so would be inconsistent with applicable law or otherwise impractical. Voluntary consensus standards are technical standards ( e. g., materials specifications, test methods, sampling procedures, business practices) developed or adopted by one or more voluntary consensus bodies. The NTTAA directs EPA to provide Congress, through annual reports to OMB, with explanations when an agency does not use available and applicable voluntary consensus standards.

The direct final rule amendments implement clarifications and corrections to the NESHAP for refractory product manufacturing, but do not change any technical standards.

Therefore, EPA did not consider the use of any voluntary consensus standards.

J. Congressional Review Act The Congressional Review Act, 5 U. S. C. 801 et seq., as added by the Small Business Regulatory Enforcement Fairness Act of 1996, generally provides that before a rule may take effect, the agency promulgating the rule must submit a rule report, which includes a copy of the rule, to each House of the Congress and to the Comptroller General of the United States. EPA will submit a report containing the direct final rule and other required information to the US Senate,

the US House of Representatives, and the Comptroller General 27 of the United States prior to publication of the rule in the Federal Register. This action is not a " major rule" as defined by 5 U. S. C. 804( 2). The direct final rule amendments are effective on [ INSERT DATE 90 DAYS AFTER DATE OF PUBLICATION OF THIS DIRECT FINAL RULE IN THE FEDERAL REGISTER]. NESHAP: Refractory Products Manufacturing Page 28 of 94 28 List of Subjects in 40 CFR Part 63 Environmental protection, Administrative practice and procedure, Air pollution control, Hazardous substances,

Intergovernmental relations, Reporting and recordkeeping requirements.

Dated:

Stephen L. Johnson, Acting Administrator 29 For the reasons stated in the preamble, title 40,

chapter I, part 63 of the Code of Federal Regulations is amended as follows:

PART 63   [ AMENDED]

1. The authority citation for part 63 continues to read as follows:

Authority: 42 U. S. C. 7401, et seq.

SUBPART SSSSS   [ AMENDED]

2. Section 63.9792 is amended as follows:

a. Revising paragraph ( b);

b. Changing the designation of paragraph ( f) to paragraph ( g); and c. Adding a new paragraph ( f).

§ 63.9792 What are my general requirements for complying with this subpart?

* * * * *

( b) Except as specified in paragraphs ( e) and ( f) of this section, you must always operate and maintain your affected source, including air pollution control and monitoring equipment, according to the provisions in § 63.6( e)( 1)( i). During the period between the compliance date specified for your affected source in § 63.9786 and the date upon which continuous monitoring systems have been installed and validated and any applicable operating limits have been established, you must maintain a log detailing the operation and maintenance of the process and emissions 30 control equipment.

* * * * *

( f) For any affected source that is subject to any of the emission limits specified in Table 1 to this subpart,

you do not have to operate the control device on that affected source under the conditions specified in paragraphs ( f)( 1) and ( 2) of this section.

( 1) For any source that is subject to the THC emissions concentration limit or the THC percentage reduction limit, you do not have to operate the control device on that source when none of the refractory products that are being processed by that source contain or form an organic HAP.

( 2) For any new clay refractory products kiln that is subject to the production based mass emission limits or the percentage reduction limits for HF and HCl, you do not have to operate the control device on that kiln when none of the refractory products that are being processed by that kiln are clay refractory products, as defined in § 63.9824.

( g) You must be in compliance with the provisions of subpart A of this part, except as noted in Table 11 to this subpart.

3. Section 63.9798 is amended as follows:

a. Revising paragraph ( a);

b. Revising paragraph ( c) introductory text; and c. Revising paragraphs ( c)( 2) and ( d). 31 § 63.9798 When must I conduct subsequent performance tests?

( a) You must conduct a performance test at least every 5 years following the initial performance test.

* * * * *

( c) If you own or operate a source that is subject to the emission limits specified in items 2 through 9 of Table 1 to this subpart, you must conduct a performance test on the source( s) listed in paragraphs ( c)( 1) and ( 2) of this section before you start production of any refractory product for which the organic HAP processing rate is likely to exceed the maximum allowable organic HAP processing rate,

as defined in items 3( b) and 8( b) of Table 4 to this subpart, established during the most recent performance test on that same source.

* * * * *

( 2) Each affected kiln that follows an affected shape dryer or curing oven in the same process line and is used to process the refractory product with the higher organic HAP processing rate.

( d) If you own or operate a kiln that is subject to the emission limits specified in item 5 or 9 of Table 1 to this subpart, you must conduct a performance test on the affected kiln following any process changes that are likely to increase organic HAP emissions from the kiln ( e. g., a decrease in the curing cycle time for a curing oven that precedes the affected kiln in the same process line). 32 * * * * *

4. Section 63.9800 is amended as follows:

a. Revising paragraph ( g)( 1);

b. Revising paragraph ( g)( 3);

c. Revising paragraph ( i)( 1); and d. Adding paragraphs ( i)( 1)( iv) to ( vi).

§ 63.9800 How do I conduct performance tests and establish operating limits?

* * * * *

( g) * * *

( 1) To determine compliance with the THC emission concentration limit listed in Table 1 to this subpart, you must calculate your emission concentration corrected to 18 percent oxygen for each test run using Equation 1 of this section:

( Eq. 1)

( ) C 2.9 C 20.9 C THC THC O C 2 = ×

Where:

CTHCC = THC concentration, corrected to 18 percent oxygen ppmvd CTHC = THC concentration ( uncorrected), ppmvd CO2 = Oxygen concentration, percent.

* * * * *

( 3) To determine compliance with production based HF and HCl emission limits in Table 1 to this subpart, you must calculate your mass emissions per unit of uncalcined clay 33 processed for each test run using Equation 3 of this section:

( Eq. 3) MP ER P =

Where:

MP = mass emissions of specific HAP ( HF or HCl) per unit of production, kilograms of pollutant per megagram ( pounds per ton) of uncalcined clay processed ER = mass emissions rate of specific HAP ( HF or HCl) during each performance test run, kilograms ( pounds) per hour P = average uncalcined clay processing rate for the performance test, megagrams ( tons) of uncalcined clay processed per hour. * * * * *

( i) * * *

( 1) For sources subject to the THC concentration limit specified in item 3, 4, 7, or 8 of Table 1 to this subpart,

you must satisfy the requirements specified in paragraphs ( i)( 1)( i) through ( vi) of this section.

( i) * * *

( iv) You must meet the data reduction requirements specified in § 63.8( g).

( v) You must maintain the 3 hour block average THC concentration at or below 20 ppmvd, corrected to 18 percent oxygen.

( vi) To calculate the oxygen correction specified in paragraph ( i)( 1)( v) of this section, you may use oxygen concentration measurements concurrent with THC concentration 34 measurements, the average oxygen concentration measured during the most recent performance test on the affected source, or other oxygen concentration measurements that are representative of normal operation for the affected source.

* * * * *

5. Section 63.9802 is revised to read as follows:

§ 63.9802 How do I develop an emissions profile?

( a) If you decide to develop an emissions profile for an affected batch process source, as indicated in item 8( a)( i)( 4) or 17( b)( i)( 4) of Table 4 to this subpart, you must measure and record mass emissions of the applicable pollutant throughout a complete batch cycle of the affected batch process source according to the procedures described in paragraph ( a)( 1) or ( 2) of this section.

( 1) If your affected batch process source is subject to the THC concentration limit specified in item 6( a), 7( a),

8, or 9 of Table 1 to this subpart or the THC percentage reduction limit specified in item 6( b) or 7( b) of Table 1 to this subpart, you must measure and record the THC mass emissions rate at the inlet to the control device using the test methods, averaging periods, and procedures specified in items 10( a) and ( b) of Table 4 to this subpart for each complete hour of the batch process cycle and while the source is processing the product with the maximum organic HAP processing rate.

( 2) If your affected batch process source is subject 35 to the HF and HCl percentage reduction emission limits in item 11 of Table 1 to this subpart, you must measure and record the HF mass emissions rate at the inlet to the control device through a series of 1 hour test runs using one of the test methods specified in item 14( a) of Table 4 to this subpart for each complete hour of the batch process cycle and while the source is processing the product with the highest uncalcined clay processing rate.

( b) You must develop a new emissions profile if you meet all of the conditions specified in paragraphs ( b)( 1)

through ( 3) of this section.

( 1) You own or operate a batch process source that is subject to the emission limits specified in item 6( a), 6( b),

7( a), 7( b), 8, or 9 of Table 1 to this subpart.

( 2) You use an emissions profile to limit emission testing to the 3 hour peak emissions period.

( 3) You begin manufacturing a new refractory product for which the organic HAP processing rate is likely to exceed the maximum allowable organic HAP processing rate established during the most recent performance test on that same source.

6. Section 63.9812 is amended by revising paragraphs ( b) and ( c) as follows:

§ 63.9812 What notifications must I submit and when?

* * * * *

( b) As specified in § 63.9( b)( 2), if you start up your 36 affected source before April 16, 2003, you must submit an Initial Notification not later than 120 calendar days after April 16, 2003.

( c) As specified in § 63.9( b)( 2), if you start up your new or reconstructed affected source on or after April 16,

2003, you must submit an Initial Notification not later than 120 calendar days after you become subject to this subpart.

* * * * *

7. Section 63.9816 is amended by revising paragraph ( c)( 9) as follows:

§ 63.9816 What records must I keep?

* * * * *

( c) * * *

( 1) * * *

( 9) If you operate a source that is subject to the THC emission limits specified in item 2 or 6 of Table 1 to this subpart and is controlled with a catalytic oxidizer, records of annual checks of catalyst activity levels and subsequent corrective actions.

* * * * *

8. Section 63.9824 is amended as follows:

a. Revising paragraph ( 3) and adding paragraph ( 4) to the definition of Deviation;

b. Revising the definitions of Maximum organic HAP processing rate and Peak emissions period; and c. Adding the definitions of Comparable control 37 device, Shutdown, and Startup.

§ 63.9824 What definitions apply to this subpart?

* * * * *

Comparable control device means, subject to paragraphs ( 1),( 2) and ( 3) of this definition, a control device with design and operating parameters that are comparable to the reference control device.

( 1) For a thermal oxidizer, a comparable control device is either:

( i) A thermal oxidizer with a residence time at least as long as, and a combustion chamber operating temperature at least as high as the reference thermal oxidizer; or ( ii) A control device that has been demonstrated to control emissions to a level that is comparable to or better than the level of emissions control achieved by the reference thermal oxidizer.

( 2) For a catalytic oxidizer, a comparable control device is either:

( i) A catalytic oxidizer with a space velocity no greater than, and a catalyst bed inlet temperature at least as high as the reference catalytic oxidizer; or ( ii) A control device that has been demonstrated to control emissions to a level that is comparable to or better than the level of emissions control achieved by the reference catalytic oxidizer.

( 3) For other control devices, a comparable control 38 device is one that has been demonstrated either through engineering calculations or emission testing to control emissions to a level that is comparable to or better than the level of control achieved by the reference control device.

* * * * *

Deviation * * *

( 3) Fails to meet any emission limitation ( emission limit, operating limit, or work practice standard) in this subpart during startup, shutdown, or malfunction, regardless of whether or not such failure is permitted by this subpart;

or ( 4) Fails to provide adequate monitoring data for demonstrating compliance with any emission limitation ( emission limit, operating limit, or work practice standard)

or other applicable requirement established by this subpart due to a malfunction or failure of any CMS required by this subpart.

* * * * *

Maximum organic HAP processing rate means the maximum rate at which the mass of organic HAP materials in refractory shapes are processed in an affected process unit.

( See also the definition of organic HAP processing rate.)

* * * * *

Peak emissions period means the period of consecutive hourly average emissions of the applicable pollutant that is 39 greater than any other period of consecutive hourly average emissions for the same pollutant over the course of a specified batch process cycle, as defined in paragraphs ( 1)

through ( 3) of this definition. The peak emissions period is a function of the rate at which the temperature of the refractory shapes is increased, the mass and loading configuration of the shapes in the process unit, the constituents of the refractory mix, and the type of pollutants emitted.

( 1) The 3 hour peak THC mass emissions period is the period of 3 consecutive hours over which the sum of the uncontrolled hourly THC mass emissions rates is greater than the sum of the uncontrolled hourly THC mass emissions rates for any other period of 3 consecutive hours during the same batch process cycle.

( 2) The 3 hour peak THC emissions concentration period is the period of 3 consecutive hours over which the sum of the THC concentrations, corrected to 18 percent oxygen, is greater than the sum of the THC concentrations at the same sampling location, corrected to 18 percent oxygen, for any other period of 3 consecutive hours during the same batch process cycle.

( 3) The 3 hour peak HF mass emissions period is the period of 3 consecutive hours over which the sum of the uncontrolled hourly HF mass emissions rates is greater than the sum of the uncontrolled hourly HF mass emissions rates 40 for any other period of 3 consecutive hours during the same batch process cycle.

* * * * *

Shutdown means the cessation of operation of an affected source. For an affected batch process source,

shutdown means the cessation of operation during a batch cycle. Shutdown does not include normal periods between batch cycles when the batch process source is not in operation.

Startup means the setting into operation of an affected source. For an affected batch process source, startup means the initial startup of the source or the startup of the source following maintenance, replacement of equipment, or equipment repairs. Startup does not include routine recharging of a batch process source at the start of a batch cycle.

* * * * *

9. Table 1 to subpart SSSSS is amended as follows:

a. Revising items 6. a and b;

b. Revising items 7. a and b;

c. Revising item 8;

d. Revising item 9; and e. Revising items 11. a and b.

Table 1 to Subpart SSSSS of Part 63 Emission Limits As stated in § 63.9788, you must comply with the emission limits for affected sources in the following table: 41 For .... You must meet the following emission limits...

* * * * * * *

6. Batch process units that are controlled with a thermal or catalytic oxidizer. a. The 2 run block average THC concentration for the 3 hour peak THC emissions concentration period must not exceed 20 ppmvd, corrected to 18 percent oxygen, at the outlet of the control device; OR b. The 2 run block average THC mass emissions rate for the 3 hour peak THC mass emissions period must be reduced by at least 95 percent.

7. Batch process units that are equipped with a control device other than a thermal or catalytic oxidizer. a. The 2 run block average THC concentration for the 3 hour peak THC emissions concentration period must not exceed 20 ppmvd, corrected to 18 percent oxygen, at the outlet of the control device; OR b. The 2 run block average THC mass emissions rate for the 3 hour peak THC mass emissions period must be reduced by at least 95 percent.

8. Batch process units that use process changes to reduce organic HAP emissions. The 2 run block average THC concentration for the 3 hour peak THC emissions concentration period must not exceed 20 ppmvd, corrected to 18 percent oxygen, at the outlet of the process gas stream.

9. Batch process kilns that are not equipped with a control device. The 2 run block average THC concentration for the 3 hour peak THC emissions concentration period must not exceed 20 ppmvd, corrected to 18 percent oxygen, at the outlet of the process gas stream.

* * * * * * * 11. Each new batch process kiln that is used to produce clay refractory products. a. The 2 run block average HF mass emissions rate for the 3 hour peak HF mass emissions period must be reduced by at least 90 percent; AND b. The 2 run block average HCl mass emissions rate for the 3 hour peak HF mass emissions period must be reduced by at least 30 percent.

10. Table 2 to subpart SSSSS is amended as follows:

a. Revising item 1. c;

b. Revising item 4;

c. Revising 7;

d. Revising items 8. a and b and adding items 8. c through e;

e. Revising items 9. a and b, and adding new items 9. d through f; and f. Deleting item 11. b and renumbering items 11. c and d as items 11. b and c, respectively.

Table 2 to Subpart SSSSS of Part 63 Operating Limits As stated in § 63.9788, you must comply with the operating limits for affected sources in the following table:

For... You must...

1. Each affected source listed in Table 1 to this subpart. a. Operate all affected sources according to the requirements to this subpart on and after the date on which the initial performance test is conducted or required to be conducted, whichever date is earlier; AND b. Capture emissions and vent them through a closed system; AND c. Operate each control device that is required to comply with this subpart on each affected source during all periods that the 43 source is operating, except where specified in § 63.9792( e) and ( f), item 2 of this table, and item 13 of Table 4 to this subpart; AND d. Record all operating parameters specified in Table 8 to this subpart for the affected source; AND e. Prepare and implement a written OM& M plan as specified in § 63.9792( d).

* * * * * * *

4. Each affected continuous process unit. Maintain the 3 hour block average organic HAP processing rate ( pounds per hour) at or below the maximum allowable organic HAP processing rate established during the most recent performance test.

* * * * * * *

7. Each affected batch process unit. For each batch cycle, maintain the organic HAP processing rate ( pounds per batch) at or below the maximum allowable organic HAP processing rate established during the most recent performance test.

8. Batch process units that are equipped with a thermal oxidizer. a. Except as specified in item 8. b. of this table, maintain throughout the entire batch cycle the hourly average operating temperature in the thermal oxidizer combustion chamber at or above the minimum allowable operating temperature established during the most recent performance test, as determined according to item 11 of Table 4 to this subpart; AND b. If complying with the provisions for reducing the thermal oxidizer operating temperature, as specified in item 13 of Table 4 to this subpart, satisfy the requirements of items 8. c. through 8. e. of this table; c. From the start of the batch cycle until the batch process unit 44 reaches its maximum temperature, maintain the thermal oxidizer combustion chamber temperature at or above the minimum allowable temperature established during the most recent performance test, as determined according to item 11 of Table 4 to this subpart; d. From the time when the batch process unit reaches its maximum temperature, maintain the thermal oxidizer combustion chamber temperature at or above the minimum allowable temperature established during the most recent performance test, as determined according to item 11 of Table 4 to this subpart, for a length of time that equals or exceeds the length of time between the process unit reaching its maximum temperature and the start of the thermal oxidizer temperature reduction during the most recent performance test; e. For the remainder of the batch process cycle, maintain the thermal oxidizer combustion chamber temperature at or above the reduced thermal oxidizer temperature established during the most recent performance test, as specified in item 13 of Table 4 to this subpart.

9. Batch process units that are equipped with a catalytic oxidizer. a. Except as specified in item 9. b. of this table, maintain throughout the entire batch cycle the hourly average operating temperature at the inlet of the catalyst bed at or above the minimum allowable operating temperature established during the most recent performance test, as determined according to item 12 of Table 4 to this subpart; AND b. If complying with the provisions for reducing the catalytic oxidizer operating temperature, as specified in item 13 of Table 4 to this subpart, satisfy the requirements of items 45 9. d through 9. f of this table; AND c. Check the activity level of the catalyst at least every 12 months. d. From the start of the batch cycle until the batch process unit reaches its maximum temperature, maintain the temperature at the inlet of the catalyst bed at or above the minimum allowable temperature established during the most recent performance test, as determined according to item 12 of Table 4 to this subpart; e. From the time when the batch process unit reaches its maximum temperature, maintain the temperature at the inlet of the catalyst bed at or above the minimum allowable temperature established during the most recent performance test, as determined according to item 12 of Table 4 to this subpart, for a length of time that equals or exceeds the length of time between the process unit reaching its maximum temperature and the start of the catalytic oxidizer temperature reduction during the most recent performance test; f. For the remainder of the batch process cycle, maintain the temperature at the inlet of the catalyst bed at or above the reduced catalyst bed inlet temperature established during the most recent performance test, as specified in item 13 of Table 4 to this subpart.

* * * * * * *

11. Each affected kiln that is equipped with a DLA. a. Maintain the 3 hour block average pressure drop across the DLA at or above the minimum levels established during the most recent performance test; AND b. Maintain the limestone feeder at or above the level established 46 during the most recent performance test; AND c. Use the same grade of limestone from the same source as was used during the most recent performance test and maintain records of the source and type of limestone used.

* * * * * * *

11. Table 4 to subpart SSSSS is amended to read as follows:

Table 4 to Subpart SSSSS to Part 63 Requirements for Performance Tests As stated in § 63.9800, you must comply with the requirements for performance tests for affected sources in the following table:

For... You must... Using... According to the following requirements...

1. Each affected source listed in Table 1 to this subpart. a. Conduct performance tests. i. The requirement s of the general provisions in subpart A of this part and the requirement s to this subpart. ( 1) Record the date of the test; AND ( 2) Identify the emission source that is tested; AND ( 3) Collect and record the corresponding operating parameter and emission test data listed in this table for each run of the performance test; AND ( 4) Repeat the performance test at least every 5 years; AND ( 5) Repeat the performance test before changing the parameter value for 47 any operating limit specified in your OM& M plan; AND ( 6) If complying with the THC concentration or THC percentage reduction limits specified in items 2 through 9 of Table 1 to this subpart, repeat the performance test under the conditions specified in items 2. a. 2. and 2. a. 3. of this table; AND ( 7) If complying with the emission limits for new clay refractory products kilns specified in items 10 and 11 of Table 1 to this subpart, repeat the performance test under the conditions specified in items 14. a. i. 4. and 17. a. i. 4. of this table.

b. Select the locations of sampling ports and the number of traverse points. i. Method 1 or 1A of 40 CFR, part 60, appendix A. ( 1) To demonstrate compliance with the percentage reduction limits specified in items 2. b., 3. b., 6. b., 7. b., 10, and 11 of Table 1 to this subpart, OR to develop an emissions profile, OR to satisfy the requirements of item 13. a. of this table, locate 48 sampling sites at the inlet of the control device and at either the outlet of the control device or at the stack prior to any releases to the atmosphere; AND ( 2) To demonstrate compliance with any other emission limit specified in Table 1 to this subpart, locate all sampling sites at the outlet of the control device or at the stack prior to any releases to the atmosphere.

c. Determine gas velocity and volumetric flow rate. Method 2, 2A, 2C, 2D, 2F, or 2G of 40 CFR part 60, appendix A. Measure gas velocities and volumetric flow rates at 1 hr intervals throughout each test run.

d. Conduct gas molecular weight analysis. ( i) Method 3, 3A, or 3B of 40 CFR part 60, appendix A; OR As specified in the applicable test method.

( ii) ASME PTC 19.10 1981 Part 10. You may use ASME PTC 19.10 1981 Part 10 ( available for purchase from Three Park Avenue, New York, NY 10016 5990) as an alternative to EPA Method 3B.

e. Measure gas moisture Method 4 of 40 CFR part 60, As specified in the applicable test method. 49 content. appendix A.

2. Each new or existing curing oven, shape dryer, and kiln that is used to process refractory products that use organic HAP; each new or existing coking oven and defumer that is used to produce pitchimpregnated refractory products; each new shape preheater that is used to produce pitchimpregnated refractory products; AND each new or existing process unit that is exhausted to a thermal or catalytic oxidizer that also controls emissions from an a. Conduct performance tests. ( 1) Conduct the performance test while the source is operating at the maximum organic HAP processing rate, as defined in § 63.9824, reasonably expected to occur; AND ( 2) Repeat the performance test before starting production of any product for which the organic HAP processing rate is likely to exceed the maximum allowable organic HAP processing rate established during the most recent performance test, as specified in § 63.9798( c); AND ( 3) Repeat the performance test on any affected uncontrolled kiln following process changes ( e. g., shorter curing oven cycle time) that could increase organic HAP emissions from the affected kiln, as specified in § 63.9798( d). 50 affected shape preheater or pitch working tank.

b. Satisfy the applicable requirement s listed in items 3 through 13 of this table.

3. Each affected continuous process unit. a. Perform a minimum of 3 test runs. The appropriate test methods specified in items 1, 4, and 5 of this table. Each test run must be at least 1 hour in duration.

b. Establish the operating limit for the maximum organic HAP processing rate. i. Method 311 of 40 CFR part 63, appendix A, OR material safety data sheets ( MSDS), OR product labels to determine the mass fraction of organic HAP in each resin, binder, or additive; AND ii. Product formulation data that specify the mass fraction of ( 1) Calculate and record the organic HAP content of all refractory shapes that are processed during the performance test, based on the mass fraction of organic HAP in the resins, binders, or additives; the mass fraction of each resin, binder, or additive, in the product; and the process feed rate; AND ( 2) Calculate and record the organic HAP processing rate ( pounds per hour) for each test run; AND ( 3) Calculate and record the maximum 51 each resin, binder, and additive in the products that are processed during the performance test; AND iii. Process feed rate data ( tons per hour). allowable organic HAP processing rate as 110% of the average of the organic HAP processing rates for the three test runs.

c. Record the operating temperature of the affected source. Process data. During each test run and at least once per hour, record the operating temperature in the highest temperature zone of the affected source.

4. Each continuous process unit that is subject to the THC emission limit listed in item 2. a., 3. a., 4, or 5 of Table 1 to this subpart. a. Measure THC concentrati ons at the outlet of the control device or in the stack. i. Method 25A of 40 CFR part 60, appendix A. ( 1) Each minute, measure and record the concentrations of THC in the exhaust stream; AND ( 2) Provide at least 50 1 minute measurements for each valid hourly average THC concentration.

b. Measure oxygen concentrati ons at the outlet of the control device or in the stack. i. Method 3A of 40 CFR part 60, appendix A. ( 1) Each minute, measure and record the concentrations of oxygen in the exhaust stream; AND ( 2) Provide at least 50 1 minute measurements for each valid hourly 52 average oxygen concentration.

c. Determine the hourly average THC concentrati on, corrected to 18 percent oxygen. i. Equation 1 of § 63.9800( g) ( 1); AND ii. The 1 minute THC and oxygen concentrati on data. ( 1) Calculate the hourly average THC concentration for each hour of the performance test as the average of the 1 minute THC measurements; AND ( 2) Calculate the hourly average oxygen concentration for each hour of the performance test as the average of the 1 minute oxygen measurements; AND ( 3) Correct the hourly average THC concentrations to 18 percent oxygen using Equation 1 of § 63.9800( g)( 1).

d. Determine the 3 hour block average THC emission concentrati on, corrected to 18 percent oxygen. The hourly average concentrati on of THC, corrected to 18 percent oxygen, for each test run. Calculate the 3 hour block average THC emission concentration, corrected to 18 percent oxygen, as the average of the hourly average THC emission concentrations, corrected to 18 percent oxygen.

5. Each continuous process unit that is subject to the THC percentage reduction limit listed in a. Measure THC concentrati ons at the inlet and outlet of the control device. i. Method 25A of 40 CFR part 60, appendix A. ( 1) Each minute, measure and record the concentrations of THC at the inlet and outlet of the control device; AND ( 2) Provide at least 50 1 minute measurements for 53 item 2. b. or 3. b. of Table 1 to this subpart. each valid hourly average THC concentration at the control device inlet and outlet.

b. Determine the hourly THC mass emissions rates at the inlet and outlet of the control device. i. The 1 minute THC concentrati on data at the control device inlet and outlet; AND ii. The volumetric flow rates at the control device inlet and outlet. Calculate the hourly THC mass emissions rates at the control device inlet and outlet for each hour of the performance test.

c. Determine the 3 hour block average THC percentage reduction. i. The hourly THC mass emissions rates at the inlet and outlet of the control device. ( 1) Calculate the hourly THC percentage reduction for each hour of the performance test using Equation 2 of § 63.9800( g)( 1); AND ( 2) Calculate the 3 hour block average THC percentage reduction.

6. Each continuous process unit that is equipped with a thermal oxidizer. a. Establish the operating limit for the minimum allowable thermal oxidizer combustion chamber temperature . i. Continuous recording of the output of the combustion chamber temperature measurement device. ( 1) At least every 15 minutes, measure and record the thermal oxidizer combustion chamber temperature; AND ( 2) Provide at least one measurement during at least three 15 minute periods per hour of testing; 54 AND ( 3) Calculate the hourly average thermal oxidizer combustion chamber temperature for each hour of the performance test; AND ( 4) Calculate the minimum allowable combustion chamber temperature as the average of the combustion chamber temperatures for the three test runs, minus 14

C ( 25

F).

7. Each continuous process unit that is equipped with a catalytic oxidizer. a. Establish the operating limit for the minimum allowable temperature at the inlet of the catalyst bed. i. Continuous recording of the output of the temperature measurement device. ( 1) At least every 15 minutes, measure and record the temperature at the inlet of the catalyst bed; AND ( 2) Provide at least one catalyst bed inlet temperature measurement during at least three 15 minute periods per hour of testing; AND ( 3) Calculate the hourly average catalyst bed inlet temperature for each hour of the performance test; AND ( 4) Calculate the minimum allowable catalyst bed inlet temperature as the average of the catalyst bed inlet temperatures for the three test 55 runs, minus 14

C ( 25

F).

8. Each affected batch process unit. a. Perform a minimum of 2 test runs. i. The appropriate test methods specified in items 1, 9, and 10 of this table. ( 1) Each test run must be conducted over a separate batch cycle unless you satisfy the requirements of § 63.9800( f)( 3) and ( 4); AND ( 2) Each test run must begin with the start of a batch cycle, except as specified in item 8. a. i. 4. of this table; AND ( 3) Each test run must continue until the end of the batch cycle, except as specified in items 8. a. i. 4. and 8. a. i. 5. of this table; AND ( 4) If you develop an emissions profile, as described in § 63.9802( a)( 1), you can limit each test run to the 3 hour peak THC mass emissions period; AND ( 5) If you do not develop an emissions profile, a test run can be stopped, and the results of that run considered complete, if either of the following provisions are met: i) you measure emissions 56 continuously until at least 3 hours after the affected process unit has reached maximum temperature, AND the hourly average THC mass emissions rate at the outlet of the control device or in the stack has not increased during the 3 hour period since maximum process temperature was reached, AND the applicable emission limit specified in items 6 through 9 of Table 1 to this subpart was met during each of the 3 hours since maximum process temperature was reached, OR, ii) for sources equipped with a thermal or catalytic oxidizer, at least 1 hour has passed since any reduction in the operating temperature of the oxidizer, as specified in item 13 of this table.

b. Establish the operating limit for the maximum organic HAP processing rate. i. Method 311 of 40 CFR part 63, appendix A, OR MSDS, OR product labels to determine the mass ( 1) Calculate and record the organic HAP content of all refractory shapes that are processed during the performance test, based on the mass fraction of organic HAP in the resins, 57 fraction of organic HAP in each resin, binder, or additive; AND ii. Product formulation data that specify the mass fraction of each resin, binder, and additive in the products that are processed during the performance test; AND iii. Batch weight ( tons). binders, or additives; the mass fraction of each resin, binder, or additive, in the product, and the batch weight prior to processing; AND ( 2) Calculate and record the organic HAP processing rate ( pounds per batch) for each test run; AND ( 3) Calculate and record the maximum allowable organic HAP processing rate as 110% of the average of the organic HAP processing rates for the two test runs.

c. Record the batch cycle time. Process data. Record the total elapsed time from the start to the completion of the batch cycle.

d. Record the operating temperature of the affected source. Process data. Record the operating temperature of the affected source at least once every hour from the start to the completion of the batch cycle. 58 9. Each batch process unit that is subject to the THC emission limit listed in item 6. a., 7. a., 8, or 9 of Table 1 to this subpart. a. Measure THC concentrati ons at the outlet of the control device or in the stack. i. Method 25A of 40 CFR part 60, appendix A. ( 1) Each minute, measure and record the concentrations of THC in the exhaust stream; AND ( 2) Provide at least 50 1 minute measurements for each valid hourly average THC concentration.

b. Measure oxygen concentrati ons at the outlet of the control device or in the stack. i. Method 3A of 40 CFR part 60, appendix A. ( 1) Each minute, measure and record the concentrations of oxygen in the exhaust stream; AND ( 2) Provide at least 50 1 minute measurements for each valid hourly average oxygen concentration.

c. Determine the hourly average THC concentrati on, corrected to 18 percent oxygen. i. Equation 1 of § 63.9800( g) ( 1); AND ii. The 1 minute THC and oxygen concentrati on data. ( 1) Calculate the hourly average THC concentration for each hour of the performance test as the average of the 1 minute THC measurements; AND ( 2) Calculate the hourly average oxygen concentration for each hour of the performance test as the average of the 1 minute oxygen measurements; AND ( 3) Correct the hourly average THC concentrations to 18 percent oxygen using Equation 1 of § 63.9800( g)( 1). 59 d. Determine the 3 hour peak THC emissions concentrati on period for each test run. The hourly average THC concentrati ons, corrected to 18 percent oxygen. Select the period of 3 consecutive hours over which the sum of the hourly average THC concentrations, corrected to 18 percent oxygen, at the control device outlet or in the stack is greater than the sum of the hourly average THC emission concentrations, corrected to 18 percent oxygen, at the control device outlet or in the stack for any other period of 3 consecutive hours during the test run.

e. Determine the average THC concentrati on, corrected to 18 percent oxygen, for each test run. The hourly average THC emission concentrati ons, corrected to 18 percent oxygen, for the 3 hour peak THC emissions concentrati on period. Calculate the average of the hourly average THC concentrations, corrected to 18 percent oxygen, for the 3 hours of the peak THC emissions concentration period for each test run.

f. Determine the 2 run block average THC concentrati on, corrected to 18 percent oxygen, for The average THC concentrati on, corrected to 18 percent oxygen, for each test run. Calculate the average of the average THC concentrations, corrected to 18 percent oxygen, for the two test runs. 60 the emission test.

10. Each batch process unit that is subject to the THC percentage reduction limit listed in item 6. b. or 7. b. of Table 1 to this subpart. a. Measure THC concentrati ons at the inlet and outlet of the control device. i. Method 25A of 40 CFR part 60, appendix A. ( 1) Each minute, measure and record the concentrations of THC at the control device inlet and outlet; AND ( 2) Provide at least 50 1 minute measurements for each valid hourly average THC concentration at the control device inlet and outlet.

b. Determine the hourly THC mass emissions rates at the control device inlet and outlet. i. The 1 minute THC concentrati on data at the control device inlet and outlet; AND ii. The volumetric flow rates at the control device inlet and outlet. ( 1) Calculate the hourly THC mass emissions rates at the control device inlet and outlet for each hour of the performance test.

c. Determine the 3 hour peak THC mass emissions period for each test run. The hourly THC mass emissions rates at the control device inlet. Select the period of 3 consecutive hours over which the sum of the hourly THC mass emissions rates at the control device inlet is greater than the sum of the hourly THC mass emissions rates at the control device inlet for any other period of 3 61 consecutive hours during the test run.

d. Determine the average THC percentage reduction for each test run. i. Equation 2 of § 63.9800( g) ( 2); AND ii. The hourly THC mass emissions rates at the control device inlet and outlet for the 3 hour peak THC mass emissions period. Calculate the average THC percentage reduction for each test run using Equation 2 of § 63.9800( g)( 2).

e. Determine the 2 run block average THC percentage reduction for the emission test. The average THC percentage reduction for each test run. Calculate the average of the average THC percentage reductions for the two test runs.

f. If complying with the provisions for reducing the thermal oxidizer operating temperature , as specified in item 13 of Table 4 to this subpart, measure the i. Method 3A of 40 CFR part 60, appendix A. ( 1) Each minute, measure and record the concentrations of oxygen in the exhaust stream; AND ( 2) Calculate each hourly average oxygen concentration using at least 50 1 minute measurements for each valid hourly average oxygen concentration. 62 oxygen concentrati on at the inlet to the control device.

11. Each batch process unit that is equipped with a thermal oxidizer. a. Establish the operating limit for the minimum thermal oxidizer combustion chamber temperature . i. Continuous recording of the output of the combustion chamber temperature measurement device. ( 1) At least every 15 minutes of each entire test run, measure and record the thermal oxidizer combustion chamber temperature; AND ( 2) Provide at least one temperature measurement during at least three 15 minute periods per hour of testing; AND ( 3) For each test run, calculate the hourly average combustion chamber temperature for each hour of the 3 hour peak THC emissions concentration period or the 3 hour peak THC mass emissions period, as defined in § 63.9824, whichever applies; AND ( 4) Calculate the average combustion chamber temperature for the applicable 3 hour peak emissions period for each test run using the average hourly combustion chamber temperatures for 63 the applicable 3 hour peak emissions period; AND ( 5) Calculate the minimum allowable thermal oxidizer combustion chamber operating temperature as the average of the average combustion chamber temperatures for the applicable 3 hour peak emissions period for the two test runs, minus 14

C ( 25

F).

12. Each batch process unit that is equipped with a catalytic oxidizer. a. Establish the operating limit for the minimum allowable temperature at the inlet of the catalyst bed. i. Continuous recording of the output of the temperature measurement device. ( 1) At least every 15 minutes of each entire test run, measure and record the temperature at the inlet of the catalyst bed; AND ( 2) Provide at least one catalyst bed inlet temperature measurement during at least three 15 minute periods per hour of testing; AND ( 3) For each test run, calculate the hourly average catalyst bed inlet temperature for each hour of the 3 hour peak THC emissions concentration period or the 3 hour peak THC mass emissions period, as defined in § 63.9824, whichever 64 applies; AND ( 4) Calculate the average catalyst bed inlet temperature for the applicable 3 hour peak emissions period for each test run using the average hourly catalyst bed inlet temperatures for the applicable 3 hour peak emissions period; AND ( 5) Calculate the minimum allowable catalyst bed inlet operating temperature as the average of the average catalyst bed inlet temperatures for the applicable 3 hour peak emissions period for the two test runs, minus 14

C ( 25

F).

13. Each batch process unit that is equipped with a thermal or catalytic oxidizer. a. During each test run, maintain the applicable operating temperature of the oxidizer until emission levels allow the oxidizer to be shut off or the operating temperature ( 1) The oxidizer can be shut off or the oxidizer operating temperature can be reduced if you do not use an emissions profile to limit testing to the 3 hour peak THC mass emissions period, as specified in item 8. a. i. 4. of this table; AND ( 2) At least 3 hours have passed since the affected 65 of the oxidizer to be reduced. process unit reached maximum temperature; AND ( 3) The applicable emission limit specified in item 6. a. or 6. b. of Table 1 to this subpart was met during each of the previous three 1 hour periods; AND ( 4) The hourly average THC mass emissions rate at the control device inlet did not increase during the 3 hour period that immediately preceded the oxidizer temperature reduction; AND ( 5) The THC concentration at the oxidizer inlet did not exceed 20 ppmvd, corrected to 18 percent oxygen, during each of the four 15 minute periods immediately following the oxidizer temperature reduction; AND ( 6) If the THC concentration exceeded 20 ppmvd, corrected to 18 percent oxygen, during any of the four 15 minute periods immediately following the oxidizer 66 temperature reduction, you must return the oxidizer to its normal operating temperature as soon as possible and maintain that temperature for at least 1 hour; AND ( 7) Continue the test run until the THC concentration at the oxidizer inlet is no more than 20 ppmvd, corrected to 18 percent oxygen, for at least four consecutive 15 minute periods that immediately follow the oxidizer temperature reduction.

14. Each new continuous kiln that is used to process clay refractory products. a. Measure emissions of HF and HCl. i. Method 26A of 40 CFR part 60, appendix A; OR ii. Method 26 of 40 CFR part 60, appendix A; OR iii. Method 320 of 40 CFR part 63, appendix A. ( 1) Conduct the test while the kiln is operating at the maximum production level and is processing the refractory product with the highest uncalcined clay processing rate, as specified in item 15. a. of this table; AND ( 2) You may use Method 26 of 40 CFR part 60, appendix A, only if no acid PM ( e. g., HF or HCl dissolved in water droplets emitted by sources controlled by a wet scrubber) is present; 67 AND ( 3) If you use Method 320 of 40 CFR part 63, appendix A, you must follow the analyte spiking procedures of Section 13 of Method 320 unless you can demonstrate that the complete spiking procedure has been conducted at a similar source; AND ( 4) Repeat the performance test if the affected source is controlled with a DLA and you change the source of the limestone used in the DLA.

b. Perform a minimum of 3 test runs. The appropriate test methods specified in items 1 and 14. a. of this table. Each test run must be at least 1 hour in duration.

15. Each new continuous kiln that is subject to the productionbased HF and HCl emission limits specified in items 10. a. and 10. b. of a. Record the uncalcined clay processing rate. i. Production data; AND ii. Product formulation data that specify the mass fraction of uncalcined clay in the products that are processed ( 1) Record the production rate ( tons per hour of fired product); AND ( 2) Calculate and record the average rate at which uncalcined clay is processed ( tons per hour) for each test run. 68 Table 1 to this subpart. during the performance test.

b. Determine the HF mass emissions rate at the outlet of the control device or in the stack. i. Method 26A of 40 CFR part 60, appendix A; OR ii. Method 26 of 40 CFR part 60, appendix A; OR iii. Method 320 of 40 CFR part 63, appendix A. Calculate the HF mass emissions rate for each test run.

c. Determine the 3 hour block average productionbased HF emissions rate. i. The HF mass emissions rate for each test run; AND ii. The average uncalcined clay processing rate. ( 1) Calculate the hourly productionbased HF emissions rate for each test run using Equation 3 of § 63.9800( g)( 3); AND ( 2) Calculate the 3 hour block average productionbased HF emissions rate as the average of the hourly production based HF emissions rates for each test run.

d. Determine the HCl mass emissions rate at the outlet of the control device or in the stack. i. Method 26A of 40 CFR part 60, appendix A; OR ii. Method 26 of 40 CFR part 60, appendix A; OR Calculate the HCl mass emissions rate for each test run. 69 iii. Method 320 of 40 CFR part 63, appendix A.

e. Determine the 3 hour block average productionbased HCl emissions rate. i. The HCl mass emissions rate for each test run; AND ii. The average uncalcined clay processing rate. ( 1) Calculate the hourly productionbased HCl emissions rate for each test run using Equation 3 of § 63.9800( g)( 3); AND ( 2) Calculate the 3 hour block average productionbased HCl emissions rate as the average of the productionbased HCl emissions rates for each test run.

16. Each new continuous kiln that is subject to the HF and HCl percentage reduction limits specified in items 10. a. and 10. b. of Table 1 to this subpart. a. Measure the HF mass emissions rates at the inlet and outlet of the control device. i. Method 26A of 40 CFR part 60, appendix A; OR ii. Method 26 of 40 CFR part 60, appendix A; OR iii. Method 320 of 40 CFR part 63, appendix A. Calculate the HF mass emissions rates at the control device inlet and outlet for each test run.

b. Determine the 3 hour block average HF percentage reduction. i. The HF mass emissions rates at the inlet and outlet of the control device for each test ( 1) Calculate the hourly HF percentage reduction using Equation 2 of § 63.9800( g)( 2); AND ( 2) Calculate the 3 hour block average HF 70 run. percentage reduction as the average of the HF percentage reductions for each test run.

c. Measure the HCl mass emissions rates at the inlet and outlet of the control device. i. Method 26A of 40 CFR part 60, appendix A; OR ii. Method 26 of 40 CFR part 60, appendix A; OR iii. Method 320 of 40 CFR part 63, appendix A. Calculate the HCl mass emissions rates at the control device inlet and outlet for each test run.

d. Determine the 3 hour block average HCl percentage reduction. i. The HCl mass emissions rates at the inlet and outlet of the control device for each test run. ( 1) Calculate the hourly HCl percentage reduction using Equation 2 of § 63.9800( g)( 2); AND ( 2) Calculate the 3 hour block average HCl percentage reduction as the average of HCl percentage reductions for each test run.

17. Each new batch process kiln that is used to process clay refractory products. a. Measure emissions of HF and HCl at the inlet and outlet of the control device. i. Method 26A of 40 CFR part 60, appendix A; OR ii. Method 26 of 40 CFR part 60, ( 1) Conduct the test while the kiln is operating at the maximum production level and is processing the refractory product with the highest uncalcined clay processing rate, as 71 appendix A; OR iii. Method 320 of 40 CFR part 63, appendix A. specified in item 15. a. of this table; AND ( 2) You may use Method 26 of 40 CFR part 60, appendix A, only if no acid PM ( e. g., HF or HCl dissolved in water droplets emitted by sources controlled by a wet scrubber) is present; AND ( 3) If you use Method 320 of 40 CFR part 63, appendix A, you must follow the analyte spiking procedures of Section 13 of Method 320 unless you can demonstrate that the complete spiking procedure has been conducted at a similar source; AND ( 4) Repeat the performance test if the affected source is controlled with a DLA and you change the source of the limestone used in the DLA.

b. Perform a minimum of 2 test runs. i. The appropriate test methods specified in items 1 and 17. a. of this table. ( 1) Each test run must be conducted over a separate batch cycle unless you satisfy the requirements of § 63.9800( f)( 3) and ( 4); AND ( 2) Each test run must consist of a 72 series of 1 hour runs at the inlet and outlet of the control device, beginning with the start of a batch cycle, except as specified in item 17. b. i. 4. of this table; AND ( 3) Each test run must continue until the end of the batch cycle, except as specified in item 17. b. i. 4. of this table; AND ( 4) If you develop an emissions profile, as described in § 63.9802( a)( 2), you can limit each test run to the 3 hour peak HF mass emissions period.

c. Determine the hourly HF and HCl mass emissions rates at the inlet and outlet of the control device i. The appropriate test methods specified in items 1 and 17. a. of this table. Determine the hourly mass HF and HCl emissions rates at the inlet and outlet of the control device for each hour of each test run.

d. Determine the 3 hour peak HF mass emissions period. The hourly HF mass emissions rates at the inlet of the control device. Select the period of 3 consecutive hours over which the sum of the hourly HF mass emissions rates at the control device inlet is greater than the sum of the 73 hourly HF mass emissions rates at the control device inlet for any other period of 3 consecutive hours during the test run.

e. Determine the 2 run block average HF percentage reduction for the emissions test. i. The hourly average HF emissions rates at the inlet and outlet of the control device. ( 1) Calculate the HF percentage reduction for each hour of the 3 hour peak HF mass emissions period using Equation 2 of § 63.9800( g)( 2); AND ( 2) Calculate the average HF percentage reduction for each test run as the average of the hourly HF percentage reductions for the 3 hour peak HF mass emissions period for that run; AND ( 3) Calculate the 2 run block average HF percentage reduction for the emission test as the average of the average HF percentage reductions for the two test runs.

f. Determine the 2 run block average HCl percentage reduction for the emission i. The hourly average HCl emissions rates at the inlet and outlet of the control ( 1) Calculate the HCl percentage reduction for each hour of the 3 hour peak HF mass emissions period using Equation 2 of § 63.9800( g)( 2); AND 74 test. device. ( 2) Calculate the average HCl percentage reduction for each test run as the average of the hourly HCl percentage reductions for the 3 hour peak HF mass emissions period for that run; AND AND ( 3) Calculate the 2 run block average HCl percentage reduction for the emission test as the average of the average HCl percentage reductions for the two test runs.

18. Each new kiln that is used to process clay refractory products and is equipped with a DLA. a. Establish the operating limit for the minimum pressure drop across the DLA. i. Data from the pressure drop measurement device during the performance test. ( 1) At least every 15 minutes, measure the pressure drop across the DLA; AND ( 2) Provide at least one pressure drop measurement during at least three 15 minute periods per hour of testing; AND ( 3) Calculate the hourly average pressure drop across the DLA for each hour of the performance test; AND ( 4) Calculate and record the minimum pressure drop as the average of the hourly average pressure drops 75 across the DLA for the two or three test runs, whichever applies.

b. Establish the operating limit for the limestone feeder setting. i. Data from the limestone feeder during the performance test. ( 1) Establish the limestone feeder setting 1 week prior to the performance test; AND ( 2) Record and maintain the feeder setting for the 1 week period that precedes the performance test and during the performance test.

19. Each new kiln that is used to process clay refractory products and is equipped with a DIFF or DLS/ FF. a. Document conformance with specificati ons and requirement s of the bag leak detection system. Data from the installatio n and calibration of the bag leak detection system. Submit analyses and supporting documentation demonstrating conformance with EPA guidance and specifications for bag leak detection systems as part of the Notification of Compliance Status.

b. Establish the operating limit for the lime feeder setting. i. Data from the lime feeder during the performance test. ( 1) For continuous lime injection systems, ensure that lime in the feed hopper or silo is free flowing at all times during the performance test; AND ( 2) Record the feeder setting for the two or three runs, whichever applies. ( 3) If the feed rate setting varies during the three test runs, 76 calculate and record the average feed rate for the two or three test runs, whichever applies.

19. Each new kiln that is used to process clay refractory products and is equipped with a WS. a. Establish the operating limit for the minimum scrubber pressure drop. i. Data from the pressure drop measurement device during the performance test. ( 1) At least every 15 minutes, measure the pressure drop across the scrubber; AND ( 2) Provide at least one pressure drop measurement during at least three 15 minute periods per hour of testing; AND ( 3) Calculate the hourly average pressure drop across the scrubber for each hour of the performance test; AND ( 4) Calculate and record the minimum pressure drop as the average of the hourly average pressure drops across the scrubber for the two or three test runs, whichever applies.

b. Establish the operating limit for the minimum scrubber liquid pH. i. Data from the pH measurement device during the performance test. ( 1) At least every 15 minutes, measure scrubber liquid pH; AND ( 2) Provide at least one pH measurement during at least three 15 minute periods per hour of testing; AND 77 ( 3) Calculate the hourly average pH values for each hour of the performance test; AND ( 4) Calculate and record the minimum liquid pH as the average of the hourly average pH measurements for the two or three test runs, whichever applies.

c. Establish the operating limit for the minimum scrubber liquid flow rate. i. Data from the flow rate measurement device during the performance test. ( 1) At least every 15 minutes, measure the scrubber liquid flow rate; AND ( 2) Provide at least one flow rate measurement during at least three 15 minute periods per hour of testing; AND ( 3) Calculate the hourly average liquid flow rate for each hour of the performance test; AND ( 4) Calculate and record the minimum liquid flow rate as the average of the hourly average liquid flow rates for the two or three test runs, whichever applies.

d. If chemicals are added to the scrubber liquid, i. Data from the chemical feed rate measurement device ( 1) At least every 15 minutes, measure the scrubber chemical feed rate; AND ( 2) Provide at 78 establish the operating limit for the minimum scrubber chemical feed rate. during the performance test. least one chemical feed rate measurement during at least three 15 minute periods per hour of testing; AND ( 3) Calculate the hourly average chemical feed rate for each hour of the performance test; AND ( 4) Calculate and record the minimum chemical feed rate as the average of the hourly average chemical feed rates for the two or three test runs, whichever applies.

12. Table 5 to subpart SSSSS is amended as follows:

a. Revising items 5 and 6; and b. Revising items 10. a and b.

Table 5 to Subpart SSSSS of Part 63 Initial Compliance with Emission Limits As stated in § 63.9806, you must show initial compliance with the emission limits for affected sources according to the following table:

For ... For the following emission limit... You have demonstrated initial compliance if...

* * * * * * *

5. Each affected batch process unit that is subject to the THC emission concentration limit listed in The average THC concentration must not exceed 20 ppmvd, corrected to The 2 run block average THC emission concentration for the 3 hour peak THC emissions concentration period measured during the 79 item 6. a., 7. a., 8, or 9 of Table 1 to this subpart. 18 percent oxygen. performance test using Methods 25A and 3A is equal to or less than 20 ppmvd, corrected to 18 percent oxygen.

6. Each affected batch process unit that is subject to the THC percentage reduction limit listed in item 6. b. or 7. b. of Table 1 to this subpart. The average THC percentage reduction must equal or exceed 95 percent. The 2 run block average THC percentage reduction for the 3 hour peak THC mass emissions period measured during the performance test using Method 25A is equal to or greater than 95 percent.

* * * * * * *

10. Each new batch process kiln that is used to process clay refractory products. a. The average uncontrolled HF emissions must be reduced by at least 90 percent. The 2 run block average HF emission reduction for the 3 hour peak HF mass emissions period measured during the performance test is equal to or greater than 90 percent.

b. The average uncontrolled HCl emissions must be reduced by at least 30 percent. The 2 run block average HCl emissions reduction for the 3 hour peak HF mass emissions period measured during the performance test is equal to or greater than 30 percent.

13. Table 7 to subpart SSSSS is amended as follows:

a. Revising item 2;

b. Revising item 4 by labeling the entry in column 3 as item i and adding item 4. ii;

c. Revising item 5 by labeling the entry in column 3 as item i and adding item 5. ii; and d. Deleting item 9. a. ii and renumbering items 9. a. iii 80 and iv as items 9. a. ii and iii, respectively.

Table 7 to Subpart SSSSS to Part 63 Continuous Compliance with Emission Limits As stated in § 63.9810, you must show continuous compliance with the emission limits for affected sources according to the following table:

For .... For the following emission limit... You must demonstrate continuous compliance by...

* * * * * * *

2. Each new or existing curing oven, shape dryer, and kiln that is used to process refractory products that use organic HAP; each new or existing coking oven and defumer that is used to produce pitchimpregnated refractory products; each new shape preheater that is used to produce pitchimpregnated refractory products; AND each new or existing process unit that is exhausted to a thermal or catalytic oxidizer that also controls emissions from an affected As specified in items 3 through 7 of this table. Satisfying the applicable requirements specified in items 3 through 7 of this table. 81 shape preheater or pitch working tank.

* * * * * * *

4. Each affected process unit that is equipped with a control device other than a thermal or catalytic oxidizer The average THC concentration must not exceed 20 ppmvd, corrected to 18 percent oxygen; OR the average THC percentage reduction must equal or exceed 95 percent. i. Operating and maintaining a THC CEMS at the outlet of the control device or in the stack of the affected source, according to the requirements of Procedure 1 of 40 CFR part 60, appendix F; AND ii. Maintaining the 3 hour block average THC concentration at or below 20 ppmvd, corrected to 18 percent oxygen.

5. Each affected process unit that uses process changes to meet the applicable emission limit. The average THC concentration must not exceed 20 ppmvd, corrected to 18 percent oxygen. i. Operating and maintaining a THC CEMS at the outlet of the control device or in the stack of the affected source, according to the requirements of Procedure 1 of 40 CFR part 60, appendix F; AND ii. Maintaining the 3 hour block average THC concentration at or below 20 ppmvd, corrected to 18 percent oxygen.

* * * * * * *

9. Each affected kiln that is equipped with a DLA a. The average HF emissions must not exceed 0.019 kg/ Mg ( 0.038 lb/ ton) of uncalcined clay processed, OR the average i. Maintaining the pressure drop across the DLA at or above the minimum levels established during the most recent performance test; AND 82 uncontrolled HF emissions must be reduced by at least 90 percent; AND b. The average HCl emissions must not exceed 0.091 kg/ Mg ( 0.18 lb/ ton) of uncalcined clay processed, OR the average uncontrolled HCl emissions must be reduced by at least 30 percent. ii. Recording the limestone feeder setting daily to verify that the feeder setting is at or above the level established during the most recent performance test; AND iii. Using the same grade of limestone as was used during the most recent performance test and maintaining records of the source and grade of limestone.

* * * * * * *

14. Table 8 to subpart SSSSS is amended as follows:

a. Revising item 4. iii and adding item 4. iv;

b. Revising item 7. iv and adding item 7. v;

c. Revising items 8 and 8. i through v and adding items 8. vi through viii;

d. Revising items 9 and 9. i through iv, renumbering items 9. v and vi as items 9. viii and ix, respectively, and adding items 9. v. through vii;

e. Revising items 11. a. ii and iii, adding item 11. a. iv, deleting item 11. b, and renumbering items 11. c and d as items 11. b and c, respectively; and f. Revising items 13. a. ii and iii, 13. b. ii and iii,

13. c. ii and iii, and 13. d. ii and iii, and adding items 13. a. iv, 13. b. iv, 13. c. iv, and 13. d. iv. 83 Table 8 to Subpart SSSSS of Part 63 Continuous Compliance with Operating Limits As stated in § 63.9810, you must show continuous compliance with the operating limits for affected sources according to the following table:

For... For the following operating limit... You must demonstrate continuous compliance by...

* * * * * * *

4. Each affected continuous process unit. a. Maintain process operating parameters within the limits established during the most recent performance test. i. Recording the organic HAP processing rate ( pounds per hour); AND ii. Recording the operating temperature of the affected source at least hourly; AND iii. Maintaining the 3 hour block average organic HAP processing rate at or below the maximum allowable organic HAP processing rate established during the most recent performance test; AND iv. Reporting, in accordance with § 63.9814( e), any 3 hour block average organic HAP processing rate that exceeds the maximum allowable organic HAP processing rate established during the most recent performance test.

* * * * * * *

7. Each affected batch process unit. a. Maintain process operating parameters within the limits i. Recording the organic HAP processing rate ( pounds per batch); AND ii. Recording the hourly average operating 84 established during the most recent performance test. temperature of the affected source; AND iii. Recording the process cycle time for each batch cycle; AND iv. Maintaining the organic HAP processing rate at or below the maximum allowable organic HAP processing rate established during the most recent performance test; AND v. Reporting, in accordance with § 63.9814( e), any organic HAP processing rate that exceeds the maximum allowable organic HAP processing rate established during the most recent performance test.

8. Batch process units that are equipped with a thermal oxidizer. Maintain the hourly average temperature in the thermal oxidizer combustion chamber at or above the minimum allowable operating temperature established during the most recent performance test. i. Measuring and recording the thermal oxidizer combustion chamber temperature at least every 15 minutes throughout any period during which the thermal oxidizer is required to be in operation; AND ii. Calculating the hourly average thermal oxidizer combustion chamber temperature for any period during which the thermal oxidizer is required to be in operation; AND iii. Except as permitted by item 8. iv of this table, maintaining throughout the entire batch cycle the hourly 85 average operating temperature in the thermal oxidizer combustion chamber at or above the minimum allowable operating temperature established during the most recent performance test; AND iv. If complying with the provisions for reducing the thermal oxidizer operating temperature, as specified in item 13 of Table 4 to this subpart, satisfying the requirements of items 8. vi. through 8. viii. of this table; AND v. Reporting, in accordance with § 63.9814( e), any temperature measurements below the minimum allowable thermal oxidizer combustion chamber temperature established during the most recent performance test. vi. From the start of the batch cycle until the batch process unit reaches its maximum temperature, maintaining the thermal oxidizer combustion chamber temperature at or above the minimum allowable temperature established during the most recent performance test, as determined according to item 11 of Table 4 to this subpart; vii. From the time when the batch process unit reaches its maximum temperature, maintaining 86 the thermal oxidizer combustion chamber temperature at or above the minimum allowable temperature established during the most recent performance test, as determined according to item 11 of Table 4 to this subpart, for a length of time that equals or exceeds the length of time between the process unit reaching its maximum temperature and the start of the thermal oxidizer temperature reduction during the most recent performance test; viii. For the remainder of the batch process cycle, maintaining the thermal oxidizer combustion chamber temperature at or above the reduced thermal oxidizer temperature established during the most recent performance test, as specified in item 13 of Table 4 to this subpart.

9. Batch process units that are equipped with a catalytic oxidizer. Maintain the hourly average temperature at the inlet of the catalyst bed at or above the minimum allowable operating temperature established during the most recent performance test. i. Measuring and recording the temperature at the inlet of the catalyst bed at least every 15 minutes throughout any period during which the catalytic oxidizer is required to be in operation; AND ii. Calculating the hourly average temperature at the catalyst bed inlet for any period during which the catalytic oxidizer is 87 required to be in operation; AND iii. Except as specified in items 9. a. iv through 9. a. vii of this table, maintaining throughout the entire batch cycle the hourly average operating temperature at the catalyst bed inlet at or above the minimum allowable operating temperature established during the most recent performance test; AND iv. If complying with the provisions for reducing the catalytic oxidizer operating temperature, as specified in item 13 of Table 4 to this subpart, satisfying the requirements of items 9. a. v. through 9. a. vii. of this table; AND v. From the start of the batch cycle until the batch process unit reaches its maximum temperature, maintaining the temperature at the inlet of the catalyst bed at or above the minimum allowable temperature established during the most recent performance test, as determined according to item 12 of Table 4 to this subpart; AND vi. From the time when the batch process unit reaches its maximum temperature, maintaining the temperature at the inlet of the catalyst bed at or above the minimum allowable temperature 88 established during the most recent performance test, as determined according to item 12 of Table 4 to this subpart, for a length of time that equals or exceeds the length of time between the process unit reaching its maximum temperature and the start of the catalytic oxidizer temperature reduction during the most recent performance test; AND vii. For the remainder of the batch process cycle, maintaining the temperature at the inlet of the catalyst bed at or above the reduced catalyst bed inlet temperature established during the most recent performance test, as specified in item 13 of Table 4 to this subpart; AND viii. Reporting, in accordance with § 63.9814( e), any temperature measurements below the minimum allowable catalyst bed inlet temperature established during the most recent performance test; AND ix. Checking the activity level of the catalyst at least every 12 months and taking any necessary corrective action, such as replacing the catalyst, to ensure that the catalyst is performing as designed.

* * * * * * * 89 11. Each new kiln that is equipped with a DLA. a. Maintain the average pressure drop across the DLA for each 3 hour block period at or above the minimum pressure drop established during the most recent performance test. i. Collecting the DLA pressure drop data, as specified in item 18. a. of Table 4 to this subpart; AND ii. Calculating the hourly average pressure drop across the DLA; AND iii. Maintaining the 3 hour block average pressure drop across the DLA at or above the minimum pressure drop established during the most recent performance test; AND iv. Reporting, in accordance with § 63.9814( e), any 3 hour block average pressure drop across the DLA below the minimum pressure drop established during the most recent performance test.

b. Maintain the limestone feeder setting at or above the level established during the most recent performance test. Verifying at least daily that the feeder setting is being maintained at or above the level established during the most recent performance test, and recording the feeder setting for each verification.

c. Use the same grade of limestone from the same source as was used during the most recent performance test. Using the same grade of limestone as was used during the most recent performance test and maintaining records of the source and grade of limestone.

* * * * * * * 90 13. Each new kiln that is used to process clay refractory products and is equipped with a wet scrubber. a. Maintain the average pressure drop across the scrubber for each 3 hour block period at or above the minimum pressure drop established during the most recent performance test. i. Collecting the scrubber pressure drop data, as specified in item 20. a. of Table 4 to this subpart; AND ii. Calculating the hourly average pressure drop across the scrubber; AND iii. Maintaining the 3 hour block average scrubber pressure drop at or above the minimum pressure drop established during the most recent performance test; AND iv. Reporting, in accordance with § 63.9814( e), any 3 hour block average pressure drop across the scrubber below the minimum pressure drop established during the most recent performance test.

b. Maintain the average scrubber liquid pH for each 3 hour block period at or above the minimum scrubber liquid pH established during the most recent performance test. i. Collecting the scrubber liquid pH data, as specified in item 20. b. of Table 4 to this subpart; AND ii. Calculating the hourly average scrubber liquid pH; AND iii. Maintaining the 3 hour block average scrubber liquid pH at or above the minimum scrubber liquid pH established during the most recent performance test; AND iv. Reporting, in accordance with § 63.9814( e), any 3 hour block average scrubber 91 liquid pH below the minimum liquid pH established during the most recent performance test.

c. Maintain the average scrubber liquid flow rate for each 3 hour block period at or above the minimum scrubber liquid flow rate established during the most recent performance test. i. Collecting the scrubber liquid flow rate data, as specified in item 20. c. of Table 4 to this subpart; AND ii. Calculating the hourly average scrubber liquid flow rate; AND iii. Maintaining the 3 hour block average scrubber liquid flow rate at or above the minimum scrubber liquid flow rate established during the most recent performance test; AND iv. Reporting, in accordance with § 63.9814( e), any 3 hour block average scrubber liquid flow rate below the minimum liquid flow rate established during the most recent performance test.

d. If chemicals are added to the scrubber liquid, maintain the average scrubber chemical feed rate for each 3 hour block period at or above the minimum scrubber chemical feed rate i. Collecting the scrubber chemical feed rate data, as specified in item 20. d. of Table 4 to this subpart; AND ii. Calculating the hourly average scrubber chemical feed rate; AND iii. Maintaining the 3 hour block average scrubber chemical feed rate at or above the minimum scrubber chemical feed rate established 92 established during the most recent performance test. during the most recent performance test; AND iv. Reporting, in accordance with § 63.9814( e), any 3 hour block average scrubber chemical feed rate below the minimum chemical feed rate established during the most recent performance test.

15. Table 10 to subpart SSSSS is amended by revising item 1 to read as follows:

Table 10 to Subpart SSSSS of Part 63 Requirements for Reports As stated in § 63.9814, you must comply with the requirements for reports in the following table:

You must submit a( n)... The report must contain... You must submit the report...

1. Compliance report The information in § 63.9814( a) through ( f). Semiannually according to the requirements in § 63.9814( b).

* * * * * * *

16. Table 11 to subpart SSSSS is amended as follows:

a. Revising citation § 63.4;

b. Adding citations § 63.6( i)( 15) and ( 16);

c. Revising citation § 63.7( b)( 2);

d. Revising citation § 63.7( e)( 3); and e. Revising citations § 63.8( c)( 1)( i), ( ii), and ( iii).

 Table 11 to Subpart SSSSS of Part 63 Applicability of General Provisions to Subpart SSSSS 93 As stated in § 63.9820, you must comply with the applicable General Provisions requirements according to the following table:

Citatio n Subject Brief Description Applies to Subpart SSSSS * * * * * * *

§ 63.4 Prohibited Activities. Compliance date; circumvention; fragmentation. Yes.

* * * * * * *

§ 63.6( i ) ( 15) [ Reserved]

§ 63.6( i ) ( 16) Administrator ' s authority. Granting extension does not abrogate Administrator's authority. Yes.

* * * * * * *

§ 63.7( b ) ( 2) Notification of Rescheduling. Must notify Administrator as soon as is practicable and provide rescheduled date. Yes.

* * * * * * *

§ 63.7( e ) ( 3) Test Run Duration. Must have three test runs for at least the time specified in the relevant standard; compliance is based on arithmetic mean of three runs; specifies conditions when data from an additional test run can be used. Yes; Yes, except where specified in § 63.9800 for batch process sources; Yes.

* * * * * * * 94 § 63.8( c ) ( 1)( i) Operation and Maintenance of CMS. Must maintain CMS in accordance with § 63.6( e)( 1). Yes.

§ 63.8( c ) ( 1)( ii) Spare Parts for CMS. Must maintain spare parts for routine CMS repairs. Yes.

§ 63.8( c ) ( 1)( iii ) SSMP for CMS. Must develop and implement SSMP for CMS. Yes.

* * * * * * *